IP Library Granted Patent US 11,404,180
Granted Patent B2
US 11,404,180 · App. 16/155,134 · Granted Aug 2, 2022

Method for producing collimators and other components from neutron absorbing materials using additive manufacturing

Inventors: David C. Anderson (Knoxville, TN); Anibal J. Ramirez-Cuesta (Knoxville, TN); Matthew B. Stone (Oak Ridge, TN); Amelia M. Elliott (Cleveland, TN); Derek H. Siddel (Knoxville, TN)
Assignee: UT-Battelle, LLC
G21K1/046B29C64/153G21C11/028G21F1/00G21G4/02B33Y10/00
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Quick Facts
Patent No.
US 11,404,180
App. No.
16/155,134
Granted
Aug 2, 2022
Kind
B2
Abstract

Collimators and other components for use in neutron scattering experiments or to provide neutron shielding in nuclear reactors or accelerator based neutron sources are produced by additive manufacturing from neutron absorbing material, such as boron carbide (B 4 C) or isotopically enriched boron carbide ( 10 B).

Claims (29)

1. A method of additively manufacturing a neutron collimator component with a binder jet printer, the method comprising:

loading neutron absorbing powder into a powder feed supply of the binder jet printer;

positioning a build platform of the binder jet printer;

spreading, with a powder transport device, the neutron absorbing powder from the powder feed supply into a layer of a powder bed on the build platform;

selectively depositing binder with a movable binder jet print head on the layer of neutron absorbing powder on the build platform by moving the binder jet printer head along binder jet printer head rails to form a pattern of binder on the layer that together with additional layers of neutron absorbing powder and binder forms a neutron collimator component in the powder bed;

repeating said positioning the build platform of the binder jet printer, said spreading the neutron absorbing powder from the powder feed supply into additional layers on the build platform, and said selectively depositing binder with the movable binder jet print head on the layer of neutron absorbing powder on the build platform to binder jet print the neutron collimator component in the powder bed on the build platform;

transporting the powder bed including the neutron collimator component from the build platform to a curing oven;

heating the powder bed including the neutron collimator component in the curing oven to cure the neutron collimator component by evaporating solvent from the binder;

de-powdering the neutron collimator component from the powder bed; and

infiltrating the de-powdered neutron collimator component with ethyl cyanoacrylate to strengthen mechanical properties of the neutron collimator component without densification via sintering.

2. The method of claim 1 wherein the neutron absorbing component has less than 5% hydrogen by weight.

3. The method of claim 1 wherein the neutron absorbing component has less than 2% hydrogen by weight.

4. The method of claim 1 , including physically isolating the neutron absorbing powder from moving parts of the binder jet with a bellows system installed on the binder jet printer, the bellows system including a shield for shielding moving binder jet printer components from the neutron absorbing powder.

5. The method of claim 1 , wherein the neutron collimator component includes one or more pinholes.

6. The method of claim 1 , wherein the neutron collimator component includes one or more apertures.

7. A method of additively manufacturing a neutron optic component with a binder jet printer, the method comprising:

loading neutron absorbing powder into a powder feed supply of the binder jet printer;

positioning a build platform of the binder jet printer;

spreading, with a powder transport device, the neutron absorbing powder from the powder feed supply into a layer of a powder bed on the build platform;

selectively depositing binder with a movable binder jet print head on the layer of neutron absorbing powder on the build platform by moving the binder jet printer head along binder jet printer head rails to form a pattern of binder on the layer that together with additional layers of neutron absorbing powder and binder forms a neutron optic component in the powder bed;

repeating said positioning the build platform of the binder jet printer, said spreading the neutron absorbing powder from the powder feed supply into additional layers on the build platform, and said selectively depositing binder with the movable binder jet print head on the layer of neutron absorbing powder on the build platform to binder jet print the neutron optic component in the powder bed on the build platform;

transporting the powder bed including the neutron optic component from the build platform to a curing oven;

heating the powder bed including the neutron optic component in the curing oven to cure the neutron optic component by evaporating solvent from the binder;

de-powdering the neutron optic component from the powder bed; and

infiltrating the de-powdered neutron optic component with ethyl cyanoacrylate to strengthen mechanical properties of the neutron optic component without densification via sintering.

8. The method of claim 7 wherein the neutron absorbing component has less than 5% hydrogen by weight.

9. The method of claim 7 wherein the neutron absorbing component has less than 2% hydrogen by weight.

10. The method of claim 7 , including physically isolating the neutron absorbing powder from moving parts of the binder jet with a bellows system installed on the binder jet printer, the bellows system including a shield for shielding moving binder jet printer components from the neutron absorbing powder.

11. The method of claim 7 , wherein the neutron optic component is a neutron collimator.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 7, 2021
From: ANDERSON, DAVID C.; RAMIREZ-CUESTA, ANIBAL J.; STONE, MATTHEW B.; ELLIOTT, AMELIA M.; SIDDEL, DEREK H.
To: UT-BATTELLE, LLC
Reel/Frame 056169/0554 →
CONFIRMATORY LICENSE Recorded Nov 29, 2018
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 047616/0538 →
Continuity (2)
Provisional Application 62569771 · Oct 9, 2017
Related Publication 20190108923A1 · Apr 11, 2019
Cited By (1)
US 12,688,945