IP Library Granted Patent US 10,345,626
Granted Patent B2
US 10,345,626 · App. 16/190,728 · Granted Jul 9, 2019

Graded index single crystal active waveguide in glass

Inventors: Himanshu Jain (Bethlehem, PA); Volkmar Dierolf (Allentown, PA); Keith J. Veenhuizen (Lebanon, PA)
Assignee: Lehigh University
G02F1/0018G02B6/122G02B6/13G02F1/035G02B2006/12095G02F2202/20G02F2203/07
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Quick Facts
Patent No.
US 10,345,626
App. No.
16/190,728
Granted
Jul 9, 2019
Kind
B2
Abstract

In one aspect the invention provides a graded refractive index single crystal waveguide having a glass block containing at least one crystal core, the crystal core having a central portion extending along an axis from a first end to a second end; an interface defining a peripheral boundary of the crystal core at a junction of the crystal core and an adjacent portion of the glass block, and a continuous, radially symmetric misorientation transverse to the central portion; wherein the misorientation has a misorientation angle that increases with increasing distance from the central portion towards the interface.

Claims (13)

1. A method of making a graded refractive index single crystal waveguide, the method comprising:

a) providing a block of glass;

b) focusing a plurality of femtosecond (fs) laser pulses having a power density on a focal point within the block of glass, thereby heating the glass and inducing crystallization;

c) translating the focal point through the glass along an axis at a scanning speed, thereby generating a single crystal within the glass, the crystal comprising a lattice oriented along the axis,

wherein the single crystal comprises a central portion extending along the axis, an interface defining a peripheral boundary of the crystal core at a junction of the crystal core and an adjacent portion of the glass block and a continuous, radially symmetric misorientation transverse to the central portion;

wherein the misorientation has a misorientation angle that increases with increasing distance from the central portion towards the interface.

2. The method according to claim 1 , wherein the misorientation angle reaches a maximum of about 15° at the interface of the crystal core.

3. The method according to claim 1 , wherein the glass comprises 35Li 2 O-35Nb 2 O 5 -30SiO 2 glass.

4. The method according to claim 1 , wherein the crystal core comprises LiNbO 3 .

5. The method according to claim 1 , wherein the power density is between about 151 GW/m 2 and about 243 GW/m 2 .

6. The method according to claim 1 , wherein the laser scanning speed is between about 15 and about 75 μm/s.

7. The method according to claim 1 , wherein the power density and scanning speed are 243 GW/m 2 and 15 μm/s; 243 GW/m 2 and 25 μm/s; or 209 GW/m 2 and 15 μm/s, respectively.

8. The method according to claim 1 , wherein the plurality of pulses has a frequency of about 200 kHz.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 16, 2023
From: LEHIGH UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 063650/0704 →
CONFIRMATORY LICENSE Recorded Jan 5, 2021
From: LEHIGH UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 054898/0961 →
Continuity (3)
Division 15816794 · Nov 17, 2017
Provisional Application 62423465 · Nov 17, 2016
Related Publication 20190079320A1 · Mar 14, 2019