IP Library Granted Patent US 11,077,327
Granted Patent B1
US 11,077,327 · App. 16/201,224 · Granted Aug 3, 2021

Degradation of chemical agents using metal-organic framework compositions

Inventors: Dorina F. Sava Gallis (Albuquerque, NM); Mark D. Tucker (Albuquerque, NM); Mark K. Kinnan (Albuquerque, NM); Jeffery A. Greathouse (Albuquerque, NM)
Assignee: National Technology & Engineering Solutions of Sandia, LLC
A62D3/30B01J31/1691A62D2101/02A62D2101/26
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Quick Facts
Patent No.
US 11,077,327
App. No.
16/201,224
Granted
Aug 3, 2021
Kind
B1
Abstract

The present invention relates to a metal-organic framework composition, as well as constructs and methods thereof. In one particular example, the composition is employed to degrade a chemical agent in a non-aqueous environment.

Claims (15)

1. A method of catalytically degrading a chemical agent, the method comprising:

providing a metal-organic framework composition comprising a plurality of metal clusters and a plurality of ligands coordinating with the plurality of metal clusters, wherein the metal of each metal cluster comprises one or more rare earth metal ions and each of the plurality of ligands comprises a 2,5-dihydroxyterephthalic acid (DOBDC) linker;

combining the metal-organic framework composition with the chemical agent and a non-aqueous solvent; and

determining a rate of decomposition of the chemical agent.

2. A method of treating a contaminated article, the method comprising:

applying a decontamination formulation to a surface of the contaminated article, wherein the decontamination formulation comprises a metal-organic framework composition and a non-aqueous solvent, and wherein the metal-organic framework composition comprises a plurality of metal clusters and a plurality of ligands coordinating with the plurality of metal clusters and wherein the metal of each metal cluster comprises one or more rare earth metal ions and each of the plurality of ligands comprises a 2,5-dihydroxyterephthalic acid (DOBDC) linker.

3. The method of claim 2 , further comprising:

reapplying the decontamination formulation to the surface after about 15 minutes or longer.

4. The method of claim 2 , wherein the contaminated article comprises electronics or circuitry.

5. The method of claim 1 , wherein the at least one metal cluster comprises a hexanuclear cluster.

6. The method of claim 5 , wherein the hexanuclear cluster comprises Eu, Nd, Yb, Y, Tb, La, Ce, Pr, Sm, Gd, Dy, Ho, Er, Tm, or Lu.

7. The method of claim 1 , wherein the plurality of metal clusters comprises a first metal ion and a second metal ion that is different than the first metal ion.

8. The method of claim 1 , further comprising a particle that comprises the plurality of metal clusters and the plurality of ligands.

9. The method of claim 1 , wherein the metal-organic framework composition comprises EuDOBDC, YDOBDC, NdDOBDC, YbDOBDC, TbDOBDC, Nd 0.67 Yb 0.33 DOBDC, or Nd 0.46 Yb 0.54 DOBDC.

10. The method of claim 1 , wherein the non-aqueous solvent comprises an alcohol or a hydrofluoroether.

Assignments (2)
CONFIRMATORY LICENSE Recorded Feb 20, 2019
From: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 048382/0871 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 14, 2019
From: SAVA GALLIS, DORINA F.; TUCKER, MARK D.; KINNAN, MARK K.; GREATHOUSE, JEFFREY A.
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 048350/0434 →
Continuity (1)
Provisional Application 62591125 · Nov 27, 2017
Cited By (1)
US 12,708,118