IP Library Granted Patent US 10,844,517
Granted Patent B2
US 10,844,517 · App. 16/225,848 · Granted Nov 24, 2020

Method of processing SiC single crystal and method of manufacturing SiC ingot

Inventor: Yohei Fujikawa (Hikone, JP)
Assignee: SHOWA DENKO K.K.
C30B29/36C30B23/002C30B23/02C30B29/605C30B29/66H01L21/02378H01L21/02433
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Quick Facts
Patent No.
US 10,844,517
App. No.
16/225,848
Granted
Nov 24, 2020
Kind
B2
Abstract

A method of processing a SiC single crystal includes a measuring step of measuring a shape of an atomic arrangement plane of the SiC single crystal along at least a first direction passing through a center in plan view and a second direction orthogonal to the first direction; and a surface processing step of processing a first plane serving as an attachment plane of the SiC single crystal, in which the surface processing step includes a grinding step of grinding the first plane, and in the grinding step, a difference is given to a surface state between the first plane and a second plane facing the first plane, and the atomic arrangement plane is flattened by Twyman's effect.

Claims (54)

1. A method of processing a SiC single crystal, comprising:

a measuring step of measuring a shape of an atomic arrangement plane of a SiC single crystal having a first plane and a second plane along at least a first direction passing through a center in plan view and a second direction orthogonal to the first direction; and

a surface processing step of processing the first plane serving as an attachment plane of the SiC single crystal,

wherein the surface processing step includes a grinding step of grinding the first plane, and

wherein in the grinding step, a difference is given to a surface state between the first plane and the second plane facing the first plane, and the atomic arrangement plane is flattened by Twyman's effect.

2. The method of processing a SiC single crystal according to claim 1 ,

wherein in the grinding step, in a case where the shape of the atomic arrangement plane is a saddle type, the first plane is ground along a direction in which an amount of curvature of the atomic arrangement plane is small, and

wherein in a case where the shape of the atomic arrangement plane is a bowl type, the first plane is concentrically ground.

3. The method of processing a SiC single crystal according to claim 1 ,

wherein the surface processing step includes a warp amount adjusting step of adjusting a warp amount of the SiC single crystal, and

wherein in the warp amount adjusting step, a thickness of the SiC single crystal is set, to adjust the warp amount of the SiC single crystal.

4. The method of processing a SiC single crystal according to claim 2 ,

wherein the surface processing step includes a warp amount adjusting step of adjusting a warp amount of the SiC single crystal, and

wherein in the warp amount adjusting step, a thickness of the SiC single crystal is set, to adjust the warp amount of the SiC single crystal.

5. The method of processing a SiC single crystal according to claim 1 ,

wherein the surface processing step includes a warp amount adjusting step of adjusting a warp amount of the SiC single crystal, and

wherein in the warp amount adjusting step, a grit number used for grinding of SiC single crystal is selected, to adjust the warp amount of the SiC single crystal.

6. The method of processing a SiC single crystal according to claim 2 ,

wherein the surface processing step includes a warp amount adjusting step of adjusting a warp amount of the SiC single crystal, and

wherein in the warp amount adjusting step, a grit number used for grinding of SiC single crystal is selected, to adjust the warp amount of the SiC single crystal.

7. The method of processing a SiC single crystal according to claim 3 ,

wherein the surface processing step includes a warp amount adjusting step of adjusting a warp amount of the SiC single crystal, and

wherein in the warp amount adjusting step, a grit number used for grinding of SiC single crystal is selected, to adjust the warp amount of the SiC single crystal.

8. The method of processing a SiC single crystal according to claim 1 ,

wherein a radius of curvature of the atomic arrangement plane of the SiC single crystal processed in the surface processing step is 28 m or more, or a maximum value of an amount of curvature is 100 μm or less.

9. The method of processing a SiC single crystal according to claim 2 ,

wherein a radius of curvature of the atomic arrangement plane of the SiC single crystal processed in the surface processing step is 28 m or more, or a maximum value of the amount of the curvature is 100 μm or less.

10. The method of processing a SiC single crystal according to claim 3 ,

wherein a radius of curvature of the atomic arrangement plane of the SiC single crystal processed in the surface processing step is 28 m or more, or a maximum value of an amount of curvature is 100 μm or less.

11. The method of processing a SiC single crystal according to claim 4 ,

wherein a radius of curvature of the atomic arrangement plane of the SiC single crystal processed in the surface processing step is 28 m or more, or a maximum value of an amount of curvature is 100 μm or less.

12. A method of manufacturing a SiC ingot using a SiC single crystal processed by the method of processing a SiC single crystal according to claim 1 as a seed crystal, the method comprising:

a step of attaching the first plane of the SiC single crystal as an attachment plane to a pedestal; and

a crystal growth step of performing crystal growth on the SiC single crystal attached to the pedestal as the seed crystal.

13. A method of manufacturing a SiC ingot using a SiC single crystal processed by the method of processing a SiC single crystal according to claim 2 as a seed crystal, the method comprising:

a step of attaching the first plane of the SiC single crystal as an attachment plane to a pedestal; and

a crystal growth step of performing crystal growth on the SiC single crystal attached to the pedestal as the seed crystal.

14. A method of manufacturing a SiC ingot using a SiC single crystal processed by the method of processing a SiC single crystal according to claim 3 as a seed crystal, the method comprising:

a step of attaching the first plane as an attachment plane of the SiC single crystal to a pedestal; and

a crystal growth step of performing crystal growth on the SiC single crystal attached to the pedestal as the seed crystal.

15. A method of manufacturing a SiC ingot using a SiC single crystal processed by the method of processing a SiC single crystal according to claim 4 as a seed crystal, the method comprising:

a step of attaching the first plane as an attachment plane of the SiC single crystal to a pedestal; and

a crystal growth step of performing crystal growth on the SiC single crystal attached to the pedestal as the seed crystal.

16. A method of manufacturing a SiC ingot using a SiC single crystal processed by the method of processing a SiC single crystal according to claim 5 as a seed crystal, the method comprising:

a step of attaching the first plane of the SiC single crystal to a pedestal as an attachment plane; and

a crystal growth step of performing crystal growth on the SiC single crystal attached to the pedestal as the seed crystal.

17. The method of manufacturing a SiC ingot according to claim 12 ,

wherein a difference in a coefficient of thermal expansion between the pedestal and the SiC single crystal at a crystal growth temperature is 0.3×10 −6 /° C. or less.

18. The method of manufacturing a SiC ingot according to claim 13 ,

wherein a difference in a coefficient of thermal expansion between the pedestal and the SiC single crystal at a crystal growth temperature is 0.3×10 −6 /° C. or less.

19. The method of manufacturing a SiC ingot according to claim 14 ,

wherein a difference in a coefficient of thermal expansion between the pedestal and the SiC single crystal at a crystal growth temperature is 0.3×10 −6 /° C. or less.

20. The method of manufacturing a SiC ingot according to claim 15 ,

wherein a difference in a coefficient of thermal expansion between the pedestal and the SiC single crystal at a crystal growth temperature is 0.3×10 −6 /° C. or less.

Assignments (3)
CHANGE OF ADDRESS Recorded Feb 14, 2024
From: RESONAC CORPORATION
To: RESONAC CORPORATION
Reel/Frame 066599/0037 →
CHANGE OF NAME Recorded Jun 23, 2023
From: SHOWA DENKO K.K.
To: RESONAC CORPORATION
Reel/Frame 064082/0513 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 19, 2018
From: FUJIKAWA, YOHEI
To: SHOWA DENKO K.K.
Reel/Frame 047819/0865 →