IP Library Granted Patent US 12,196,645
Granted Patent B1
US 12,196,645 · App. 16/227,785 · Granted Jan 14, 2025

Systems and methods for measuring material degradation

Inventors: Stephen J. Bauer (Albuquerque, NM); William Payton Gardner (Missoula, MT)
Assignee: National Technology & Engineering Solutions of Sandia, LLC
G01M5/0033E21B43/26E21B47/11E21B49/00C09K8/80C09K11/06
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Quick Facts
Patent No.
US 12,196,645
App. No.
16/227,785
Granted
Jan 14, 2025
Kind
B1
Abstract

Systems and methods that measure material deformation by measuring a tracer gas that has been added to or is present in an engineered material that is subsequently released from the material, measured, and correlated to a change in a property of the material upon a stress/strain being applied to the engineered material.

Claims (18)

1. A method for detecting a strained state of an engineered material, comprising:

homogeneously fixing within the engineered material an amount of a tracer gas when forming the engineered material;

applying a stress to the engineered material to release the tracer gas from the engineered material; and

sensing an amount of tracer gas released from within the engineered material and associating the amount of tracer gas sensed to the strained state within the engineered material;

wherein the engineered material is selected from the group consisting essentially of glass, ceramics and cermets.

2. The method of claim 1 , further comprising:

correlating the amount of the sensed tracer gas to a state of the engineered material.

3. The method of claim 2 , wherein the state of the engineered material is selected from a group consisting of fracture volume, fracture size, fracture number/density and fracture location.

4. The method of claim 1 , wherein the tracer gas is fixed in the engineered material by disposing the tracer material within glass or polymer microspheres or beads or by diffusing the tracer gas into a crystalline or amorphous material within the engineered material.

5. The method of claim 1 , wherein the tracer gas is fixed in the engineered material by diffusing the tracer gas into a crystalline or amorphous material within the engineered material.

6. The method of claim 1 , wherein the stress is directly applied to the engineered material.

7. The method of claim 1 , wherein the strained state in the engineered material results from a temperature change or material chemical modification or degradation to the engineered material.

8. The method of claim 1 , wherein the tracer gas is fixed in the engineered material by diffusing the tracer gas into crystalline material within the engineered material.

9. The method of claim 1 , wherein the tracer gas is selected from a group consisting of noble gases, gases with specific isotopic composition and engineered gases.

10. The method of claim 9 , wherein the engineered gases are selected from a group consisting of refrigerants and insulators.

11. The method of claim 1 , wherein the tracer gas is fixed to a carrier material disposed within the engineered material.

12. The method of claim 11 , wherein the carrier material comprises quartz particles or fragments.

13. The method of claim 11 , wherein the carrier material is ceramic particles.

Assignments (2)
CONFIRMATORY LICENSE Recorded Feb 20, 2019
From: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 048382/0626 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 14, 2019
From: BAUER, STEPHEN J.
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 048350/0469 →
Continuity (1)
Provisional Application 62609159 · Dec 21, 2017
References Cited (4)
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US 20100307745A1 · Lafitte · 2010 [cited by examiner]
US 20110277996A1 · Cullick · 2011 [cited by examiner]
US 20130126158A1 · Gupta · 2013 [cited by examiner]