IP Library Granted Patent US 11,185,920
Granted Patent B2
US 11,185,920 · App. 16/230,093 · Granted Nov 30, 2021

Methods and systems for making metal-containing particles

Inventors: Terrence Hyde Murphy (Chicago, IL); William Peter Wilke, IV (Saint John, IN); Philip Michael Kowalski (Wanatah, IN)
Assignee: Hammond Group, Inc.
B22F9/082B22F9/26C01G21/06C22C1/053H01M4/364H01M4/56H01M4/57H01M10/06B22F2009/0824B22F2009/0848B22F2009/0876B22F2301/30B22F2302/25B22F2999/00C01P2002/30C01P2004/51C01P2004/61C01P2006/12C01P2006/60C22C1/1042
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Quick Facts
Patent No.
US 11,185,920
App. No.
16/230,093
Granted
Nov 30, 2021
Kind
B2
Abstract

According to one or more embodiments presently described, metal-containing particles may be made by a method that includes introducing a molten material into a reaction zone of a reactor system, passing a process gas into the reaction zone in a direction substantially tangential to a sidewall of the reaction zone, and contacting the process gas with the molten material in the reaction zone to form metal-containing particles. The molten material may be introduced into an upper portion of the reaction zone The reaction zone may include a substantially circular cross-section, and the molten metal may be introduced into the reaction zone in a laminar flow or as atomized particles.

Claims (16)

1. A method for making metal-containing particles, the method comprising:

introducing a molten material into a reaction zone of a reactor system, wherein the molten material is introduced into an upper portion of the reaction zone, wherein the reaction zone comprises a circular cross-section, and wherein the molten metal is introduced into the reaction zone in a laminar flow;

passing a process gas into the reaction zone in a direction substantially tangential to a sidewall of the reaction zone;

contacting the process gas with the molten material in the reaction zone to form metal-containing particles.

2. The method of claim 1 , wherein at least 99% of the particles are non-oxidized metals, metalloids or alloys.

3. The method of claim 2 , wherein at least 95% of the particles are pure lead metal particles.

4. The method of claim 1 , wherein the process gas is inert.

5. The method of claim 1 , wherein the reaction zone operates at a temperature of at least 621° F.

6. The method of claim 1 , further comprising separating the process gas from the formed metal-containing particles.

7. The method of claim 6 , wherein the separating occurs in a separation zone comprising a frustum.

8. The method of claim 7 , further comprising providing a cooling air supply to a separation section zone where separation of the metal-containing particles and process gas occurs.

9. The method of claim 7 , wherein the process gas flows upwardly to exit the separation zone.

10. The method of claim 7 , wherein the metal-containing particles flow downwardly to exit the separation zone.

11. The method of claim 1 , wherein the process gas is an oxidizing agent and metal oxide particles are formed.

12. The method of claim 1 , wherein a flow of gas impinges upon the laminar flow of molten material.

13. The method of claim 1 , wherein the molten metal is dispensed in a hollow conical pattern, which is contacted by a gas annulus.

Assignments (2)
SECURITY INTEREST Recorded Jul 26, 2019
From: HAMMOND GROUP, INC.
To: BMO HARRIS BANK N.A.
Reel/Frame 049871/0423 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 17, 2019
From: MURPHY, TERRENCE HYDE; WILKE, WILLIAM PETER, IV; KOWALSKI, PHILIP MICHAEL
To: HAMMOND GROUP, INC.
Reel/Frame 048914/0985 →
Continuity (3)
Provisional Application 62616593 · Jan 12, 2018
Provisional Application 62743698 · Oct 10, 2018
Related Publication 20190217392A1 · Jul 18, 2019