IP Library Granted Patent US 10,927,045
Granted Patent B2
US 10,927,045 · App. 16/244,660 · Granted Feb 23, 2021

Ceramic composite materials and methods

Inventor: Chengying Xu (Tallahassee, FL)
Assignee: Florida State University Research Foundation, Inc.
C04B35/806B82Y30/00C04B35/58C04B35/62844C04B35/62886C04B35/62894C04B35/64H01B1/02H01B1/04C04B2235/3873C04B2235/483C04B2235/526C04B2235/5248C04B2235/5264C04B2235/5268C04B2235/5288C04B2235/616C04B2235/77C04B2235/96H05K9/009
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Quick Facts
Patent No.
US 10,927,045
App. No.
16/244,660
Granted
Feb 23, 2021
Kind
B2
Abstract

Provided herein are methods of making composite materials. The methods may include infiltrating a carbon nanoscale fiber network with a ceramic precursor, curing the ceramic precursor, and/or pyrolyzing the ceramic precursor. The infiltrating, curing, and pyrolyzing steps may be repeated one or more times. Composite materials also are provided that include a ceramic material and carbon nanoscale fibers.

Claims (13)

1. A composite material comprising:

a ceramic material dispersed in a carbon nanoscale fiber network which (a) comprises a plurality of substantially aligned mechanically stretched carbon nanoscale fibers having an aspect ratio greater than 100,000:1, and (b) is in the form of a sheet or a strip,

wherein the composite material (i) includes a volume fraction of the plurality of substantially aligned carbon nanoscale fibers of at least 35%, and (ii) has an electrical conductivity of at least 1.75×10 4 S/m.

2. The composite material of claim 1 , wherein the composite material is flexible.

3. The composite material of claim 1 , wherein the volume fraction of the plurality of substantially aligned carbon nanoscale fibers in the composite material is about 40% to about 80%.

4. The composite material of claim 1 , wherein the electrical conductivity of the composite material is about 2.0×10 4 S/m to about 3.0×10 4 S/m.

5. The composite material of claim 1 , wherein the composite material has a tensile strength of at least 400 MPa.

6. The composite material of claim 1 , wherein the composite material has a tensile strength of about 450 MPa to about 650 MPa.

7. The composite material of claim 1 , wherein the ceramic material comprises silicon carbonitride.

8. The composite material of claim 1 , wherein the ceramic material is evenly dispersed in the carbon nanoscale fiber network.

9. The composite material of claim 1 , wherein the plurality of substantially aligned carbon nanoscale fibers comprises single-wall carbon nanotubes, multi-wall carbon nanotubes, or a combination thereof.

10. The composite material of claim 1 , wherein the mechanically stretched carbon nanoscale fiber network is a buckypaper.

11. The composite material of claim 1 , wherein the plurality of substantially aligned carbon nanoscale fibers comprises pristine carbon nanotubes.

Assignments (2)
CONFIRMATORY LICENSE Recorded Dec 6, 2019
From: FLORIDA STATE UNIVERSITY
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA
Reel/Frame 051262/0165 →
CONFIRMATORY LICENSE Recorded Oct 15, 2019
From: FLORIDA STATE UNIVERSITY
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA
Reel/Frame 050730/0959 →
Continuity (3)
Division 15492628 · Apr 20, 2017
Provisional Application 62325748 · Apr 21, 2016
Related Publication 20200024200A1 · Jan 23, 2020