IP Library Granted Patent US 10,968,191
Granted Patent B2
US 10,968,191 · App. 16/273,619 · Granted Apr 6, 2021

Energy-efficient and environmentally friendly process for the production of target chemical compounds from cellulosic material

Inventors: Henning Marckmann (Buchloe, DE); Ralf Hortsch (Munich, DE); Marco Schuth (Altdorf, DE); Bernhard Arzt (Kandel, DE)
Assignee: Clariant International Ltd.
C07D307/50B01D11/0223B01D11/0292B01J20/18C07C45/55C07C51/31C08H8/00
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Quick Facts
Patent No.
US 10,968,191
App. No.
16/273,619
Granted
Apr 6, 2021
Kind
B2
Abstract

The present invention is directed to an energy-efficient and environmentally friendly process for the production of chemical target compounds from cellulosic material. In a further aspect, the present invention is directed to a system for conducting the process according to the inventive process.

Claims (16)

1. A process for the production of chemical target compounds from cellulosic material comprising the steps

a) treating cellulosic material by applying steam;

b) separating the steam containing at least one chemical target compound from the treated cellulosic material;

c) transferring the separated steam to a segregation device;

d) segregating the phase containing the least one chemical target compound from the steam by rectification;

e) subjecting the steam to a utilization step.

2. The process according to claim 1 , wherein the segregation comprises steam transformation of the steam containing the at least one chemical target compound.

3. The process according to claim 2 , wherein the segregation comprises decanting the phase containing the at least one chemical target compound from the transformed steam, resulting in said phase containing the at least one chemical target compound and a residual watery phase.

4. The process according to claim 3 , wherein the residual watery phase is recycled to step d) after decanting the phase containing the at least one chemical target compound.

5. The process according to claim 1 , wherein the utilization step e) is selected from evaporation, drying, heating, sterilizing, energy generating and distillation.

6. The process according to claim 1 , further comprising the step

f) condensing the utilized steam of step e).

7. The process according to claim 6 , further comprising the step

g) recycling of the utilized steam.

8. The process according to claim 7 , wherein the utilized steam is recycled to step a) of the process.

9. The process according to claim 1 , wherein the segregated chemical target compound according to step d) is one or more compounds selected from phenolic compounds, furans4-OH benzyl alcohol, 4-OH benzaldehyde, 4-OH benzoic acid, trimethyl benzaldehyde, 2-furoic acid, coumaric acid, ferulic acid, phenol, guaiacol, veratrole, pyrogallol, pyrogallol mono methyl ether, vanillyl alcohol, vanillin, isovanillin, vanillic acid, isovanillic acid, homovanillic acid, veratryl alcohol, veratraldehyde, veratric acid, 2-O-methyl gallic acid, syringyl alcohol, syringaldehyde, syringic acid, trimethyl gallic acid, homocatechol, ethyl vanillin, creosol, p-methyl anisol, anisaldehyde, anisic acid, furfural, hydroxymethylfurfural, 5-hydroxymethylfurfural, formic acid, acetic acid, levulinic acid, cinnamic acid, coniferyl aldehyde, isoeugenol, hydroquinone and eugenol.

Assignments (2)
CONFIRMATORY DEED OF ASSIGNMENT EFFECTIVE MAY 1, 2018 Recorded Nov 2, 2022
From: CLARIANT INTERNATIONAL LTD
To: CLARIANT PRODUKTE (DEUTSCHLAND) GMBH
Reel/Frame 061875/0121 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 13, 2019
From: MARCKMANN, HENNING; HORTSCH, RALF; SCHUTH, MARCO; ARZT, BERNHARD
To: CLARIANT INTERNATIONAL LTD.
Reel/Frame 048319/0747 →
Priority Claims (1)
EP 14002758 · Aug 6, 2014 · regional
Continuity (2)
Continuation 15501482
Related Publication 20190177292A1 · Jun 13, 2019
Cited By (1)
US 12,453,931