IP Library Granted Patent US 10,781,211
Granted Patent B2
US 10,781,211 · App. 16/300,501 · Granted Sep 22, 2020

Spirocycle compounds and methods of making and using same

Inventors: Daniel J. Buzard (San Diego, CA); Michael B. Shaghafi (San Diego, CA); Justin S. Cisar (San Diego, CA); Cheryl A. Grice (Encinitas, CA); Todd K. Jones (Solana Beach, CA); Olivia D. Weber (San Diego, CA)
Assignee: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
C07D471/10A61K31/499A61K31/538A61K31/5377A61K31/541A61K31/55C07D519/00
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Quick Facts
Patent No.
US 10,781,211
App. No.
16/300,501
Granted
Sep 22, 2020
Kind
B2
Abstract

Provided herein are spirocycle compounds and pharmaceutical compositions comprising said compounds. The subject compounds and compositions are useful as modulators of MAGL and/or ABHD6. Furthermore, the subject compounds and compositions are useful for the treatment of pain.

Claims (29)

1. A method of treating acute pain, inflammatory pain, cancer pain, pain caused by peripheral neuropathy, central pain, fibromyalgia, migraine, vasoocclussive painful crises in sickle cell disease, spasticity or pain associated with multiple sclerosis, functional chest pain, rheumatoid arthritis, osteoarthritis, functional dyspepsia, Persistent Motor Tic Disorder, Persistent Vocal Tic Disorder, attention deficit hyperactivity disorder (ADHD), obsessive-compulsive disorder (OCD), glaucoma, atopic dermatitis, pruritis, or Down's Syndrome in a patient, comprising administering to the patient a therapeutically effective amount of a compound of Formula (Ia):

wherein:

R 1 is H or C 1-6 alkyl;

R 2 is H or C 1-6 alkyl;

each R 3 is independently selected from C 1-6 alkyl, C 2-6 alkenyl, C 2-6 alkynyl, halogen, —CN, C 1-6 haloalkyl, C 1-6 aminoalkyl, heterocycloalkyl, —C 1-6 alkyl(heterocycloalkyl), heteroaryl, —SF 5 , —NR 5 R 6 , —CO 2 R 8 , —C(O)R 8 , and —C(O)NR 8 R 9 , wherein heterocycloalkyl and —C 1-6 alkyl(heterocycloalkyl) are optionally substituted with one or two R 4 ; or two adjacent R 3 form a heterocycloalkyl ring optionally substituted with one, two, or three R 4 ;

each R 4 is independently selected from C 1-6 alkyl, C 1-6 haloalkyl, C 3-8 cycloalkyl, halogen, oxo, —CN, —CO 2 R 8 , —C(O)R 8 , —C(O)NR 8 R 9 , —SO 2 R 8 , —NR 9 C(O)R 8 , and —NR 9 SO 2 R 8 ;

each R 5 and R 6 is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 1-6 aminoalkyl, C 3-8 cycloalkyl, —C 1-6 alkyl(heterocycloalkyl), —C 1-6 alkyl-C(O)(heterocycloalkyl), heterocycloalkyl, aryl, and heteroaryl; or R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring optionally substituted with one, two, or three R 10 ;

each R 7 is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 1-6 aminoalkyl, C 3-8 cycloalkyl, —C 1-6 alkyl(heterocycloalkyl), —C 1-6 alkyl-C(O)(heterocycloalkyl), heterocycloalkyl, aryl, and heteroaryl, wherein heterocycloalkyl, aryl, and heteroaryl are optionally substituted with one or two groups selected from oxo, C 1-6 alkyl, C 1-6 haloalkyl, CO 2 H, and C(O)NH 2 ;

each R 8 and R 9 is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 3-8 cycloalkyl, aryl, and heteroaryl; or R 8 and R 9 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring optionally substituted with one or two groups selected from C 1-6 alkyl, C 1-6 haloalkyl, CO 2 H, and C(O)NH 2 ;

each R 10 is independently selected from C 1-6 alkyl, C 3-8 cycloalkyl, C 1-6 haloalkyl, halogen, oxo, —CN, —CO 2 R 8 , —C(O)R 8 , —C(O)NR 8 R 9 , —SO 2 R 8 , —NR 9 C(O)R 8 , and —NR 9 SO 2 R 8 ;

p is 0, 1, 2, 3, 4, or 5;

n is 0 or 1; and

m is 1 or 2; provided that when n is 0, then m is 2; and when n is 1, then m is 1;

or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof.

2. The method of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein each R 3 is independently selected from C 1-6 alkyl, C 2-6 alkynyl, halogen, —CN, C 1-6 haloalkyl, heterocycloalkyl, —C 1-6 alkyl(heterocycloalkyl), heteroaryl, —SF 5 , —NR 5 R 6 , —OR 7 , —CO 2 R 8 , and —C(O)NR 8 R 9 .

3. The method of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 1 and R 2 are both H.

4. The method of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 1 and R 2 are both —CH 3 .

5. The method of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein each R 3 is independently selected from C 1-6 alkyl, halogen, C 1-6 haloalkyl, —C 1-6 alkyl(heterocycloalkyl), —NR 5 R 6 , —CO 2 R 8 , and —C(O)NR 8 R 9 .

6. The method of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein each R 3 is independently selected from halogen, C 1-6 haloalkyl, —NR 5 R 6 , and —OR 7 .

7. The method of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring substituted with one or two R 10 independently selected from C 1-6 alkyl, C 3-8 cycloalkyl, C 1-6 haloalkyl, halogen, —CO 2 R 8 , —C(O)R 8 , —C(O)NR 8 R 9 , —SO 2 R 8 , —NR 9 C(O)R 8 , and —NR 9 SO 2 R 8 .

8. The method of claim 7 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring substituted with one or two R 10 independently selected from C 1-6 alkyl and —CO 2 H.

9. The method of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form an unsubstituted heterocycloalkyl ring.

10. The method of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring, optionally substituted with one, two, or three R 10 selected from:

11. The method of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein each R 7 is independently selected from C 1-6 alkyl, C 1-6 haloalkyl, C 1-6 aminoalkyl, —C 1-6 alkyl(heterocycloalkyl), —C 1-6 alkyl-C(O)(heterocycloalkyl), heterocycloalkyl, and heteroaryl.

12. The method of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein two adjacent R 3 form a heterocycloalkyl ring optionally substituted with one or two R 4 .

13. The method of claim 1 , wherein p is 2.

14. The method of claim 1 , wherein p is 1.

15. The method of claim 1 , wherein n is 0 and m is 2.

16. The method of claim 1 , wherein n is 1 and m is 1.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE THE RECEIVING PARTY NAME PREVIOUSLY RECORDED AT REEL: 055679 FRAME: 0885. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 11, 2021
From: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
To: H. LUNDBECK A/S
Reel/Frame 056544/0697 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2021
From: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
To: H. LUNDBECK A/S.
Reel/Frame 055679/0885 →
CHANGE OF NAME Recorded Sep 10, 2019
From: ABIDE THERAPEUTICS, INC.
To: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
Reel/Frame 050330/0554 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 25, 2019
From: BUZARD, DANIEL J.; SHAGHAFI, MICHAEL B.; CISAR, JUSTIN S.; GRICE, CHERYL A.; JONES, TODD K.; WEBER, OLIVIA D.
To: ABIDE THERAPEUTICS, INC.
Reel/Frame 048686/0678 →
Continuity (2)
Provisional Application 62335597 · May 12, 2016
Related Publication 20200022977A1 · Jan 23, 2020
Cited By (2)
US 12,286,421 US 12,378,219