IP Library Granted Patent US 11,066,396
Granted Patent B2
US 11,066,396 · App. 16/309,390 · Granted Jul 20, 2021

3-aryl- heteroaryl substituted 5-trifluoromethyl oxadiazoles as histonedeacetylase 6 (HDAC6) inhibitors

Inventors: Abbas Walji (Lansdale, PA); Richard Berger (Harleysville, PA); Craig A. Stump (Pottstown, PA); Kelly-Ann S. Schlegel (Fleetwood, PA); James J. Mulhearn (Elkins, PA); Thomas J. Greshock (Collegeville, PA); Deping Wang (Furlong, PA); Mark E. Fraley (North Wales, PA); Kristen G. Jones (Oreland, PA)
Assignee: MERCK SHARP & DOHME CORP.
C07D413/10A61K45/06A61P3/10A61P9/00A61P11/06A61P25/18A61P25/28A61P29/00A61P35/00A61P37/00A61P37/02C07D271/06C07D271/113C07D413/04C07D413/12C07D413/14C07D417/12C07D417/14C07D471/04C07D471/14C07D487/04C07D491/048C07D491/052C07D498/04C07D513/04C07F7/0807
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Quick Facts
Patent No.
US 11,066,396
App. No.
16/309,390
Granted
Jul 20, 2021
Kind
B2
Abstract

The present invention is directed to substituted 5-trifluoromethyl oxadiazole compounds of generic formula (I) or a pharmaceutically acceptable salt thereof. In particular, the invention is directed to a class of aryl and heteroaryl substituted 5-trifluoromethyl oxadiazole compounds of formula I which may be useful as HDAC6 inhibitors for treating cellular proliferative diseases, including cancer, neurodegenerative diseases, such as schizophrenia and stroke, as well as other diseases.

Claims (25)

1. A compound of formula (I):

or a pharmaceutically acceptable salt thereof wherein;

X represents phenyl, wherein said phenyl is optionally substituted with one or two fluoro;

Z is —N;

R 1 and R 2 can combine together with the nitrogen atom to which they are attached to form a six membered monocyclic, heterocyclic non-aromatic ring optionally interrupted by 1 heteroatoms O, wherein said heterocyclic ring is optionally substituted with 1 to 2 groups of R a ;

R a is selected from the group consisting of H, phenyl and ═O, wherein said phenyl is optionally substituted with 1 group R b ;

R b is halo,

n represents 0.

2. The compound according to claim 1 wherein R 1 and R 2 combine together with the nitrogen atom to which they are attached to form optionally substituted morpholinyl, morpholinonyl, piperidinonyl, or piperidinyl, wherein said groups are optionally substituted with 1 to 2 R a selected from the group consisting of phenyl, or a pharmaceutically acceptable salt thereof.

3. The compound according to claim 2 wherein R 1 and R 2 combine together with the nitrogen atom to which they are attached to form morpholinyl, morpholinonyl, piperidinonyl, or piperidinyl, and at least one R a is present which is positioned adjacent to the nitrogen atom to which R 1 and R 2 originally are attached, or a pharmaceutically acceptable salt thereof.

4. The compound according to claim 3 wherein the R a substituent attached adjacent to the nitrogen atom to which R 1 and R 2 are originally attached is phenyl, or a pharmaceutically acceptable salt thereof.

5. The compound according to claim 1 as represented by structural formula II:

or a pharmaceutically acceptable salt thereof, wherein

is defined as Q and Q is represented by structural formulas (c), (d), (e), or (f);

represents the bond that links the nitrogen to which it is attached to the rest of the molecule;

and R a′ is R a and R a is as defined in claim 1 .

6. The compound according to claim 5 wherein Q is (c), (d), (e), or (f), at least one R a is attached and is phenyl, or a pharmaceutically acceptable salt thereof.

7. The compound according to claim 6 wherein at least one R a present, is phenyl, and is located on the carbon atom directly adjacent to the linking nitrogen atom, or a pharmaceutically acceptable salt thereof.

8. A compound which is selected from the group consisting of:

(R)-5-phenyl-4-(4-(5-(trifluoromethyl)-1,2,4-oxadiazol-3-yl)phenyl)morpholin-3-one,

(R)-4-(3-fluoro-4-(5-(trifluoromethyl)-1,2,4-oxadiazol-3-yl)phenyl)-5-phenylmorpholin-3-one,

(R)-4-(2,5-difluoro-4-(5-(trifluoromethyl)-1,2,4-oxadiazol-3-yl)phenyl)-5-phenylmorpholin-3-one,

(R)-4-(2-fluoro-4-(5-(trifluoromethyl)-1,2,4-oxadiazol-3-yl)phenyl)-5-phenylmorpholin-3-one,

or a pharmaceutically acceptable salt thereof.

9. A pharmaceutical composition comprising a compound of claim 1 , or a pharmaceutically acceptable salt thereof and a pharmaceutically acceptable carrier.

Assignments (2)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 12, 2018
From: BERGER, RICHARD; STUMP, CRAIG A.; MULHERN, JAMES J.; WANG, DEPING; FRALEY, MARK E.; GRESHOCK, THOMAS J.; SCHLEGEL, KELLY ANN S.; WALJI, ABBAS; JONES, KRISTEN G.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 047758/0930 →
Continuity (2)
Provisional Application 62353854 · Jun 23, 2016
Related Publication 20190185462A1 · Jun 20, 2019
Cited By (1)
US 12,590,084