IP Library › Granted Patent US 11,673,170
Granted Patent B2
US 11,673,170 · App. 16/318,052 · Granted Jun 13, 2023

Method for cleaning a vacuum system used in the manufacture of OLED devices, method for vacuum deposition on a substrate to manufacture OLED devices, and apparatus for vacuum deposition on a substrate to manufacture OLED devices

Inventors: Jose Manuel Dieguez-Campo (Hanau, DE); Stefan Keller (Mainaschaff, DE); Jae Won Lee (Aschaffenburg, DE); Takashi Anjiki (Kyoto, JP); Dieter Haas (San Jose, CA)
Assignee: Applied Materials, Inc.
B08B7/04B08B3/08B08B7/0035B08B9/08C23C14/12C23C14/24C23C14/566H01L51/001H01L51/0011H01L51/56B08B2209/08
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Quick Facts
Patent No.
US 11,673,170
App. No.
16/318,052
Granted
Jun 13, 2023
Kind
B2
Abstract

The present disclosure provides a method for cleaning a vacuum system used in the manufacture of OLED devices. The method includes performing pre-cleaning for cleaning at least a portion of the vacuum system, and performing plasma cleaning using a remote plasma source.

Claims (31)

1. A method for cleaning a vacuum system used in the manufacture of OLEO devices, comprising:

performing pre-cleaning for cleaning at least a portion of a vacuum system, wherein the pre-cleaning includes a wet chemical cleaning process; and

performing plasma cleaning using a remote plasma source, the plasma cleaning performed after the pre-cleaning.

2. The method of claim 1 , wherein the plasma cleaning is a final cleaning procedure before operating the vacuum system.

3. The method of claim 1 , wherein the plasma cleaning includes a cleaning of a vacuum chamber.

4. The method of claim 3 , wherein the plasma cleaning includes a cleaning of one or more inner wads of the vacuum chamber.

5. The method of claim 1 , wherein the plasma cleaning includes a cleaning of components inside a vacuum chamber of the vacuum system.

6. The method of claim 5 , wherein the components are selected from the group consisting of mechanical components, moveable components, drives, valves, and any combination thereof.

7. The method of claim 1 , wherein the plasma cleaning includes a cleaning of one or more mask devices used during a deposition process.

8. The method of claim 1 , wherein the method is performed after a maintenance procedure of the vacuum system or portions of the vacuum system.

9. The method of claim 1 , wherein the plasma cleaning is performed in one or more chambers of the vacuum system selected from the group consisting of a load lock chamber, a cleaning chamber, a vacuum deposition chamber, a vacuum processing chamber, a transfer chamber, a routing module; and any combination thereof.

10. The method of claim 1 , wherein the plasma cleaning uses a plasma of pure oxygen or oxygen mixtures with nitrogen or argon.

11. The method of claim 1 , wherein the pre-cleaning is performed under atmosphere and the plasma cleaning is performed under vacuum.

12. The method of claim 1 , wherein the pre-cleaning and the plasma cleaning are performed in the same chamber.

13. The method of claim 1 , wherein the vacuum chamber has a pressure in the vacuum chamber of about 0.1 mbar to about 5 mbar during the plasma cleaning.

14. A method for vacuum deposition on a substrate to manufacture OLED devices, comprising:

performing pre-cleaning for cleaning at least a portion of a vacuum system, wherein the pre-cleaning includes a wet chemical cleaning process;

performing plasma cleaning using a remote plasma source for cleaning at least the portion of the vacuum system, the plasma cleaning performed after the pre-cleaning, and

depositing one or more layers of an organic material on a substrate.

15. The method of claim 14 , wherein the plasma cleaning uses a plasma of pure oxygen or oxygen mixtures with nitrogen or argon.

16. The method of claim 14 , wherein the pre-cleaning is performed under atmosphere and the plasma cleaning is performed under vacuum.

17. The method of claim 16 , further comprising reducing pressure after pre-cleaning to wherein the plasma cleaning is performed at a pressure of about 10 −5 mbar to about 10 −8 mbar, wherein reducing the pressure is performed before the plasma cleaning.

18. The method of claim 14 , wherein the plasma cleaning uses pure oxygen.

19. The method of claim 14 , wherein the plasma cleaning uses a mixture of (1) oxygen and (2) nitrogen or argon.

20. An apparatus for vacuum deposition on a substrate to manufacture OLED devices, comprising:

a vacuum chamber;

a remote plasma source connected to the vacuum chamber; and

a controller connected to the remote plasma source for performing plasma cleaning as a final cleaning procedure,

wherein the controller is configured to implement a method for cleaning a vacuum system used in the manufacture of OLED devices, comprising:

performing pre-cleaning for cleaning at least a portion of the vacuum system, wherein the pre-cleaning includes a wet chemical cleaning process; and

performing plasma cleaning using a remote plasma source.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 5, 2019
From: DIEGUEZ-CAMPO, JOSE MANUEL; KELLER, STEFAN; LEE, JAE WON
To: APPLIED MATERIALS GMBH & CO. KG
Reel/Frame 048237/0867 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 5, 2019
From: APPLIED MATERIALS GMBH & CO. KG
To: APPLIED MATERIALS, INC.
Reel/Frame 048238/0015 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 5, 2019
From: ANJIKI, TAKASHI; HAAS, DIETER
To: APPLIED MATERIALS, INC.
Reel/Frame 048238/0121 →
Continuity (1)
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