IP Library Granted Patent US 11,168,349
Granted Patent B2
US 11,168,349 · App. 16/319,853 · Granted Nov 9, 2021

Method for measuring glycated hemoglobin

Inventors: Haruyo Soya (Sunto-gun, JP); Yuki Katayama (Sunto-gun, JP); Noriyuki Ogawa (Sunto-gun, JP)
Assignee: Hitachi Chemical Diagnostics Systems Co., Ltd.
C12Q1/28C12Q1/26G01N33/72
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Quick Facts
Patent No.
US 11,168,349
App. No.
16/319,853
Granted
Nov 9, 2021
Kind
B2
Abstract

A method is provided for measuring glycated hemoglobin in a hemoglobin-containing sample which comprises reacting glycated hemoglobin in the hemoglobin-containing sample with an enzyme that catalyzes a reaction of oxidizing the glycated hemoglobin to generate hydrogen peroxide, in the presence of at least one anionic surfactant selected from the group consisting of N-acyl taurine in which a hydrogen atom of the amino group may be substituted with a substituent, alkyl sulfoacetic acid, polyoxyethylene alkyl ether acetic acid, N-acyl amino acid in which a hydrogen atom of the amino group may be substituted with a substituent, polyoxyethylene alkyl ether phosphoric acid, polyoxyethylene polycyclic phenyl ether phosphoric acid, alkyl phosphoric acid, and salts thereof, to generate hydrogen peroxide, and measuring the generated hydrogen peroxide.

Claims (12)

1. A method for measuring glycated hemoglobin in a hemoglobin-containing sample, comprising:

reacting glycated hemoglobin in the hemoglobin-containing sample with an enzyme that catalyzes a reaction of oxidizing the glycated hemoglobin to generate hydrogen peroxide, in the presence of at least one anionic surfactant selected from the group consisting of N-acyl taurine in which a hydrogen atom of the amino group is optionally substituted with a substituent, alkyl sulfoacetic acid, polyoxyethylene alkyl ether acetic acid, N-acyl amino acid in which a hydrogen atom of the amino group is optionally substituted with a substituent, polyoxyethylene alkyl ether phosphoric acid, polyoxyethylene polycyclic phenyl ether phosphoric acid, alkyl phosphoric acid, and salts thereof; and

measuring the generated hydrogen peroxide.

2. The method according to claim 1 , wherein the measurement of the hydrogen peroxide is carried out with a reagent for measuring hydrogen peroxide.

3. The method according to claim 2 , wherein the reagent for measuring hydrogen peroxide is a reagent containing a peroxidase and a leuco-type chromogen.

4. The method according to claim 3 , wherein the leuco-type chromogen is a phenothiazine-based chromogen.

5. The method according to claim 4 , wherein the phenothiazine-based chromogen is 10-(carboxymethylaminocarbonyl)-3,7-bis(dimethylamino)phenothiazine or a salt thereof.

6. The method according to claim 1 , wherein the method comprises

reacting the glycated hemoglobin in the hemoglobin-containing sample with at least one anionic surfactant selected from the group consisting of N-acyl taurine in which a hydrogen atom of the amino group may be substituted with a substituent, alkyl sulfoacetic acid, polyoxyethylene alkyl ether acetic acid, N-acyl amino acid in which a hydrogen atom of the amino group may be substituted with a substituent, polyoxyethylene alkyl ether phosphoric acid, polyoxyethylene polycyclic phenyl ether phosphoric acid, alkyl phosphoric acid, and salts thereof,

then adding the enzyme that catalyzes a reaction of oxidizing the glycated hemoglobin, and

reacting the glycated hemoglobin in the hemoglobin-containing sample with the enzyme that catalyzes a reaction of oxidizing the glycated hemoglobin to generate hydrogen peroxide, in the presence of the at least one anionic surfactant selected from the group consisting of N-acyl taurine in which a hydrogen atom of the amino group may be substituted with a substituent, alkyl sulfoacetic acid, polyoxyethylene alkyl ether acetic acid, N-acyl amino acid in which a hydrogen atom of the amino group may be substituted with a substituent, polyoxyethylene alkyl ether phosphoric acid, polyoxyethylene polycyclic phenyl ether phosphoric acid, alkyl phosphoric acid, and salts thereof.

7. The method according to claim 1 , wherein the at least one anionic surfactant comprises at least one surfactant selected from the group consisting of N-acyl taurine in which a hydrogen atom of the amino group is optionally substituted with a substituent, alkyl sulfoacetic acid, polyoxyethylene alkyl ether acetic acid, polyoxyethylene alkyl ether phosphoric acid, polyoxyethylene polycyclic phenyl ether phosphoric acid, alkyl phosphoric acid, and salts thereof.

Assignments (5)
CHANGE OF NAME Recorded Sep 23, 2025
From: KYOWA MEDEX CO., LTD.
To: HITACHI CHEMICAL DIAGNOSTICS SYSTEMS CO., LTD.
Reel/Frame 072925/0508 →
CHANGE OF NAME Recorded Sep 23, 2025
From: HITACHI CHEMICAL DIAGNOSTICS SYSTEMS CO., LTD.
To: MINARIS MEDICAL CO., LTD.
Reel/Frame 072925/0657 →
CHANGE OF NAME Recorded Sep 23, 2025
From: MINARIS MEDICAL CO., LTD.
To: CANON MEDICAL DIAGNOSTICS CORPORATION
Reel/Frame 072925/0690 →
CHANGE OF NAME Recorded Aug 27, 2019
From: KYOWA MEDEX CO., LTD.
To: HITACHI CHEMICAL DIAGNOSTICS SYSTEMS CO., LTD.
Reel/Frame 050180/0181 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 7, 2019
From: SOYA, HARUYO; KATAYAMA, YUKI; OGAWA, NORIYUKI
To: KYOWA MEDEX CO., LTD.
Reel/Frame 048526/0684 →
Priority Claims (1)
JP JP2016-150498 · Jul 29, 2016 · national
Continuity (1)
Related Publication 20190249222A1 · Aug 15, 2019