IP Library Granted Patent US 11,421,345
Granted Patent B2
US 11,421,345 · App. 16/329,084 · Granted Aug 23, 2022

Ultrafine nanowires as highly efficient electrocatalysts

Inventors: Xiangfeng Duan (Los Angeles, CA); Yu Huang (Los Angeles, CA); Mufan Li (Los Angeles, CA)
Assignee: THE REGENTS OF UNIVERSITY OF CALIFORNIA
C30B33/10B22F1/054B22F1/16B22F1/17B22F9/24C25B11/02C25F1/00C25F7/00C30B7/14C30B29/52C30B29/60H01M4/926B22F2998/10B82Y30/00B82Y40/00
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Quick Facts
Patent No.
US 11,421,345
App. No.
16/329,084
Granted
Aug 23, 2022
Kind
B2
Abstract

A manufacturing method includes: (1) providing M-M′ nanowires, wherein M′ is at least one sacrificial metal different from M; and (2) subjecting the M-M′ nanowires to electrochemical de-alloying to form jagged M nanowires.

Claims (13)

1. A catalyst material comprising:

a catalyst support; and

jagged Pt nanowires affixed to the catalyst support.

2. The catalyst material of claim 1 , wherein the jagged Pt nanowires have an average diameter in a range of up to 5 nm.

3. The catalyst material of claim 1 , wherein the jagged Pt nanowires have an electrochemical active surface area of at least 80 m 2 /g Pt .

4. The catalyst material of claim 1 , wherein the jagged Pt nanowires have a mass activity for oxygen reduction reaction at 0.9 V vs. RHE of at least 8 A/mg Pt .

5. The catalyst material of claim 1 , wherein the jagged Pt nanowires are produced by a process comprising:

providing Pt-M′ nanowires, wherein M′ is at least one sacrificial metal different from Pt; and

subjecting the Pt-M′ nanowires to electrochemical de-alloying to form jagged Pt nanowires.

6. The catalyst material of claim 1 , wherein the jagged Pt nanowires comprise a jagged surface containing defective sites.

7. The catalyst material of claim 1 , wherein the jagged Pt nanowires comprise a jagged surface containing a plurality of atomic steps.

8. The catalyst material of claim 1 , wherein the jagged Pt nanowires have an average diameter in a range of up to 10 nm.

9. The catalyst material of claim 1 , wherein the jagged Pt nanowires have an electrochemical active surface area of at least 110 m 2 /g Pt .

Assignments (1)
CONFIRMATORY LICENSE Recorded Apr 26, 2023
From: UNIVERSITY OF CALIFORNIA LOS ANGELES
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 063472/0956 →
Continuity (2)
Provisional Application 62381176 · Aug 30, 2016
Related Publication 20190226120A1 · Jul 25, 2019