IP Library Granted Patent US 11,046,857
Granted Patent B2
US 11,046,857 · App. 16/342,433 · Granted Jun 29, 2021

Precipitation of polyether block amide and thermoplastic polyethylene to enhance operational window for three dimensional printing

Inventors: Luke Rodgers (St. Petersburg, FL); Erik Gjovik (St. Petersburg, FL)
Assignee: JABIL INC.
C09D11/102B33Y70/00C08G69/40C08J3/14C08K7/22C08K9/04C08L101/00C09D11/108C08J2323/00C08J2375/04C08J2377/00C08J2387/00
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Quick Facts
Patent No.
US 11,046,857
App. No.
16/342,433
Granted
Jun 29, 2021
Kind
B2
Abstract

A polymer material suitable for three-dimensional printing that may include at least one of polyether block amide, thermoplastic polyeurothane, and thermoplastic olefin. The polymer is formed through chemical precipitation forming a precipitated pulverulent polymer which possesses increased operating window characteristics selected from the group consisting at least one of a wider than typical range between and among the melting and recrystallization temperatures, a larger enthalpy upon melting, and a low volumetric change during recrystallization.

Claims (21)

1. A polymer material suitable for three-dimensional printing, comprising:

a precipitated thermoplastic polyurethane;

wherein the precipitated thermoplastic polyurethane is formed through chemical precipitation of a baseline thermoplastic polyurethane;

wherein the precipitated thermoplastic polyurethane has a larger enthalpy upon melting, compared to the baseline thermoplastic polyurethane.

2. The polymer material of claim 1 , wherein the precipitated thermoplastic polyurethane has a particle geometry not formed from milling.

3. The polymer material of claim 1 , wherein the precipitated thermoplastic polyurethane has an increased range between its melting temperature and recrystallization temperature, compared to the baseline thermoplastic polyurethane.

4. The polymer material of claim 1 , wherein the precipitated thermoplastic polyurethane includes a melting temperature that is higher than its recrystallization temperature, and wherein the precipitated thermoplastic polyurethane comprises a first crystallite having a first melting enthalpy and a second crystallite having a second melting enthalpy.

5. The polymer material of claim 1 , wherein the precipitated thermoplastic polyurethane may be sinterable from about room temperature to less than about 150 degrees Celsius.

6. The polymer material of claim 1 , wherein the precipitated thermoplastic polyurethane produced through chemical precipitation has a particle size range from about 25 microns to about 75 microns.

7. The polymer material of claim 1 , wherein the precipitated thermoplastic polyurethane is formed through precipitating the polymer in a solvent and allowing the polymer to form crystallites.

8. A polymer material, the polymer material comprising:

a precipitated thermoplastic polyurethane;

wherein the precipitated thermoplastic polyurethane is formed through chemical precipitation of a baseline thermoplastic polyurethane;

wherein the baseline thermoplastic polyurethane has a first recrystallization temperature and the precipitated thermoplastic polyurethane has a second recrystallization temperature; and

wherein the second recrystallization temperature is less than the first recrystallization temperature.

9. A polymer material, the polymer material comprising:

a precipitated thermoplastic polyurethane;

wherein the precipitated thermoplastic polyurethane is formed through chemical precipitation of a baseline thermoplastic polyurethane;

wherein the baseline thermoplastic polyurethane has a first average particle size range and the precipitated thermoplastic polyurethane has a second average particle size range;

wherein the second average particle size range is smaller than the first particle size range; and

wherein the second average particle size range is from about 25 microns to about 75 microns.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 28, 2021
From: RODGERS, LUKE
To: JABIL INC.
Reel/Frame 056380/0401 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 28, 2021
From: RODGERS, LUKE
To: JABIL INC.
Reel/Frame 056389/0319 →
Continuity (2)
Provisional Application 62409036 · Oct 17, 2016
Related Publication 20190264047A1 · Aug 29, 2019