IP Library Granted Patent US 10,525,457
Granted Patent B2
US 10,525,457 · App. 16/351,989 · Granted Jan 7, 2020

Anion exchange membranes and polymers for use in same

Inventors: Chulsung Bae (Cohoes, NY); Angela Dee Mohanty (Clifton Park, NY)
Assignee: Rensselaer Polytechnic Institute
B01J41/14C08F8/04C08F8/24C08F8/42C08F8/44C25B13/08H01M8/083H01M8/103H01M8/1023H01M2008/1095Y02P70/56
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Quick Facts
Patent No.
US 10,525,457
App. No.
16/351,989
Granted
Jan 7, 2020
Kind
B2
Abstract

Embodiments of the invention relate generally to anion exchange membranes and, more particularly, to anion exchange membranes comprising a styrene block copolymer and methods for their manufacture. In one embodiment, the invention provides a polymer according to formula IV, wherein x and y are mol %, QA is or each of R 1 and R 2 is, independently, a linear alkyl chain or a cyclic alkyl chain, and Z is selected from a group consisting of: a linear alkyl chain, a cyclic alkyl chain, and an alkylene ether chain.

Claims (16)

1. A polymer according to formula IV

wherein x and y are mol %, QA is

each of R1 and R2 is, independently, a linear alkyl chain or a cyclic alkyl chain, and Z is selected from a group consisting of: a linear alkyl chain, a cyclic alkyl chain, and an alkylene ether chain.

2. A method of preparing the polymer of claim 1 , the method comprising:

methylizing a polymer of formula III; and

carrying our an ion exchange reaction on the resulting polymer

wherein x and y are mol %, QA is

each of R1 and R2 is, independently, a linear alkyl chain or a cyclic alkyl chain, and Z is selected from a group consisting of: a linear alkyl chain, a cyclic alkyl chain, and an alkylene ether chain.

3. The method according to claim 2 , further comprising:

preparing the polymer of formula III by:

carrying out a palladium-catalyzed Suzuki coupling reaction using a polymer of formula II and an aryl bromide-containing amine

wherein x and y are mol %.

4. The method of claim 3 , further comprising:

preparing the polymer of formula II by:

carrying our an iridium-catalyzed borylation using a polymer of formula I and bis(pinacolato)diboron

wherein x and y are mol %.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 26, 2019
From: BAE, CHULSUNG; MOHANTY, ANGELA
To: RENSSELAER POLYTECHNIC INSTITUTE
Reel/Frame 051121/0018 →
Continuity (3)
Continuation 15326538
Provisional Application 62027497 · Jul 22, 2014
Related Publication 20190308185A1 · Oct 10, 2019