IP Library › Granted Patent US 10,683,399
Granted Patent B2
US 10,683,399 · App. 16/354,728 · Granted Jun 16, 2020

Biodegradable textiles, masterbatches, and method of making biodegradable fibers

Inventors: Andrea Ferris (Hayward, CA); Alan McIntosh (Hayward, CA); Sudeep Motupalli Rao (Santa Rosa, CA); Robert A. Usher (Charlotte, NC)
Assignee: Intrinsic Advanced Materials, LLC
C08J3/226C08K3/26D01F1/10D04H1/4291D04H1/435D04H1/4334D04H1/4382D04H1/56D04H3/16C08J2367/04C08J2467/00C08J2477/00C08K2003/265
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Quick Facts
Patent No.
US 10,683,399
App. No.
16/354,728
Granted
Jun 16, 2020
Kind
B2
Abstract

A masterbatch is disclosed, along with associated methods, and biodegradable filaments, fibers, yarns and fabrics. The masterbatch includes 0.2 to 5 mass % CaCO 3 , an aliphatic polyester with a repeat unit having from two to six carbons in the chain between ester groups, with the proviso that the 2 to 6 carbons in the chain do not include side chain carbons, and a carrier polymer selected from the group consisting of PET, nylon, other thermoplastic polymers, and combinations thereof.

Claims (18)

1. A masterbatch comprising:

39-48 weight % polyethylene terephthalate (PET);

39-49 weight % polycaprolactone (PCL); and

1 weight % calcium carbonate.

2. The masterbatch according to claim 1 and further comprising a composition selected from the group consisting of 5-10 weight % polylactic acid (PLA), 5-10 weight % polyhydroxybutyrate (PHB), 5-10 weight % polybutylene adipate terephthalate (PBAT), 10-20 weight % polybutylene succinate (PBS), 1 weight % silicon dioxide, and combinations of these compositions.

3. A molten intermediate, comprising:

the masterbatch of claim 1 ; and

at least 90 mass % of a polymer selected from the group consisting of polyethylene terephthalate (PET), nylon, other thermoplastic polymers, and combinations thereof.

4. A quenched, size-characterized plurality of polymer pellets formed from the molten intermediate of claim 3 .

5. A quenched polymer filament formed from the molten intermediate of claim 3 .

6. The molten intermediate of claim 3

further comprising polybutylene succinate (PBS) in an amount of 9-11 mass %; and

at least 90 mass % of a polymer selected from the group consisting of polyethylene terephthalate (PET), nylon, other thermoplastic polymers, and combinations thereof.

7. The molten intermediate of claim 3 consisting essentially of:

0.39-0.49 weight % polycaprolactone (PCL); and

0.01 weight % calcium carbonate; and

at least 90 mass % polyethylene terephthalate (PET).

8. The molten intermediate of claim 3 and further comprising a composition selected from the group consisting of 0.05-0.1 weight % polylactic acid (PLA), 0.05-0.1 weight % polyhydroxybutyrate (PHB), 0.05-0.1 weight % polybutylene adipate terephthalate (PBAT), 0.10-0.20 weight % polybutylene succinate (PBS), 0.01 weight % silicon dioxide, and combinations of these compositions.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 18, 2021
From: USHER, ROBERT A
To: INTRINSIC ADVANCED MATERIALS, LLC
Reel/Frame 055639/0951 →
Continuity (3)
Provisional Application 62690227 · Jun 26, 2018
Provisional Application 62690243 · Jun 26, 2018
Related Publication 20190390020A1 · Dec 26, 2019