IP Library › Granted Patent US 10,561,655
Granted Patent B2
US 10,561,655 · App. 16/356,360 · Granted Feb 18, 2020

SHP2 inhibitors and uses thereof

Inventors: Yinong Xie (Dover, DE); Lee E. Babiss (Dover, DE)
Assignee: SYNBLia Therapeutics, Inc.
A61K31/513A61K31/4402A61K31/519A61P35/00A61P37/00C07D213/64C07D401/04C07D487/04
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,561,655
App. No.
16/356,360
Granted
Feb 18, 2020
Kind
B2
Abstract

Compounds of Formula 1 as inhibitors of protein tyrosine phosphatase SHP2 are disclosed. The pharmaceutical compositions comprising compounds of Formula 1, methods of synthesis of these compounds, methods of treatment for diseases associated with the aberrant activity of SHP2 such as cancer using these compounds or compositions containing these compounds are also disclosed.

Claims (27)

1. A compound represented by a formula:

or a pharmaceutically acceptable salt thereof;

wherein X is S;

Ring A is an optionally substituted aryl having 6-10 ring carbon atoms; an optionally substituted 5-membered mono-cyclic heteroaryl comprising 0-4 ring nitrogen atoms, 0-1 ring oxygen atom, 0-1 ring sulfur atom, and at least one N, O, or S ring atom; an optionally substituted 6-membered mono-cyclic heteroaryl comprising 1-3 ring nitrogen atoms; or an optionally substituted bicyclic ring system having 5-10 ring carbon atoms, 0-4 ring nitrogen atoms, 0-1 ring oxygen atom, or 0-1 ring sulfur atom, wherein the bicyclic ring system is unsaturated or partially saturated;

Ring B is:

wherein R A and R B are independently H or C 1-12 hydrocarbyl, or —N(R A )(R B ) is an optionally substituted heterocyclic ring system, wherein the heterocyclic ring system is a mono-cyclic ring having 2-8 ring carbon atoms, 1-2 ring nitrogen atoms, 0-1 ring oxygen atom, and 0-1 ring sulfur atom; a bicyclic ring system having 5-12 ring carbon atoms, 1-2 ring nitrogen atoms, 0-1 ring oxygen atom, and 0-1 ring sulfur atom; or a tricyclic ring system having 8-16 ring carbon atoms, 1-2 ring nitrogen atoms, 0-1 ring oxygen atom, and 0-1 ring sulfur atom; wherein the bicyclic ring system is a spiro, fused, or bridged ring system, wherein the heterocyclic ring system is saturated or partially saturated; and

wherein substituted Ring A and substituted Ring B are independently having one or more substituents; wherein each substituent of Ring A or Ring B is independently alkyl, alkenyl, alkynyl, —NR A R B , —OR A , —S—R A , aryl, heteroaryl, heterocyclyl, hydroxy, alkoxy, aryloxy, —C(O)—R A , R A —C(O)O— alkylcarboxylate, —SH, cyano, halogen, —C(═S)—R A , —OC(O)—NR A R B , R A —OC(O)—N(R A )—, —OC(═S)—NR A R B , R A —OC(═S)—N(R A )—, —C(O)NR A R B , R A —C(O)N(R A )—, (R A R B )N—S(O) 2 —, —N(R A )—S(O) 2 —R A , nitro, R A —S(═O)—, —S(O) 2 —R A , haloalkyl, haloalkoxyl, —S(O) 2 C(X′) 3 wherein X′ is halogen, —N(R A )S(O) 2 C(X′) 3 wherein X′ is halogen, amino, —N(R A )C(O)-heteroaryl, —N(R A )C(O)-heterocyclyl, —C(O)N(R A )-heteroaryl, —C(O)N(R A )-heterocyclyl, or a combination thereof.

2. The compound of claim 1 , wherein Ring A is optionally substituted phenyl.

3. The compound of claim 1 , wherein Ring A is optionally substituted pyridinyl.

4. The compound of claim 1 , wherein Ring A is optionally substituted pyridin-4-yl.

5. The compound of claim 1 , wherein Ring A is optionally substituted 2,3-dichlorophenyl.

6. The compound of claim 1 , wherein Ring A is optionally substituted 2,3-dichloro-pyridin-4-yl.

7. The compound of claim 1 , wherein Ring A is optionally substituted 2-amino-3-chloropyridin-4-yl.

8. The compound of claim 1 , wherein Ring A is any one of the following:

9. The compound of claim 1 , wherein Ring B is 5-((3S,4S)-4-amino-3-methyl-2-oxa-8-azaspiro[4.5]decan-8-yl)-6-oxo-1,6-dihydropyrazin-2-yl.

10. The compound of claim 1 , wherein Ring B is any one of the following:

11. The compound of claim 1 , wherein the compound is an R-enantiomer.

12. The compound of claim 1 , wherein the compound is an S-enantiomer.

13. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the compound is any one of the following compounds that is:

14. The compound of claim 1 , wherein any substituent of the compound has a molecular weight of about 15 g/mol to about 500 g/mol.

15. A pharmaceutical composition comprising a compound of claim 1 or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable vehicle, diluent, or carrier.

16. A compound represented by a formula:

or a pharmaceutically acceptable salt thereof;

wherein X is S;

wherein Ring A is optionally substituted phenyl, optionally substituted naphthalen-1-yl, optionally substituted pyridin-3-yl, optionally substituted pyridin-4-yl, optionally substituted 2-oxo-1,2-dihydropyridin-4-yl, optionally substituted 1H-indol-4-yl, optionally substituted 2-oxoindolin-4-yl, optionally substituted indolin-4-yl, optionally substituted 3-(2-oxo-2,5-dihydro-1H-pyrrole-3-carboxamido)phenyl, optionally substituted 3-(4-oxo-4H-pyrido[1,2-a]pyrimidine-3-carboxamido)phenyl, optionally substituted 3-(4-oxo-4H-pyrazino[1,2-a]pyrimidine-3-carboxamido)phenyl, optionally substituted 3-(5-oxo-5H-thiazolo[3,2-a]pyrimidine-6-carboxamido)phenyl, optionally substituted 3-(5-oxo-1,5-dihydroimidazo[1,2-a]pyrimidine-6-carboxamido)phenyl, or optionally substituted 3-(4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidine-3-carboxamido)phenyl;

wherein Ring B is 6-oxo-5-(piperidin-1-yl)-1,6-dihydropyrazin-2-yl, 6-oxo-5-(pyrrolidin-1-yl)-1,6-dihydropyrazin-2-yl, 5-(hexahydropyrrolo[3,4-c]pyrrol-2(1H)-yl)-6-oxo-1,6-dihydropyrazin-2-yl, 5-(3,6-diazabicyclo[3.2.0]heptan-6-yl)-6-oxo-1,6-dihydropyrazin-2-yl, 6-oxo-5-(2-oxa-8-azaspiro[4.5]decan-8-yl)-1,6-dihydropyrazin-2-yl, 6-oxo-5-(piperidin-4-ylamino)-1,6-dihydropyrazin-2-yl, optionally substituted 6-oxo-5-(spiro[bicyclo[3.1.0]hexane-3,4′-piperidin]-1′-yl)-1,6-dihydropyrazin-2-yl, 6-oxo-5-(8-azaspiro[4.5]decan-8-yl)-1,6-dihydropyrazin-2-yl, 6-oxo-5-(2-azaspiro[3.4]octan-2-yl)-1,6-dihydropyrazin-2-yl, 5-(3-azabicyclo[3.1.0]hexan-3-yl)-6-oxo-1,6-dihydropyrazin-2-yl, 6-oxo-5-(3H-spiro[benzofuran-2,4′-piperidin]-1′-yl)-1,6-dihydropyrazin-2-yl, 5-(5,7-dihydrospiro[cyclopenta[b]pyridine-6,4′-piperidin]-1′-yl)-6-oxo-1,6-dihydropyrazin-2-yl, 5-(1,3-dihydrospiro[indene-2,4′-piperidin]-1′-yl)-6-oxo-1,6-dihydropyrazin-2-yl, 5-(4,6-dihydrospiro[cyclopenta[d]thiazole-5,4′-piperidin]-1′-yl)-6-oxo-1,6-dihydropyrazin-2-yl, or 6-oxo-5-(spiro[indoline-2,4′-piperidin]-1′-yl)-1,6-dihydropyrazin-2-yl; and

wherein substituted Ring A and substituted Ring B are independently having one or more substituents; wherein each substituent of Ring A or Ring B is independently alkyl, alkenyl, alkynyl, —NR A R B , —OR A , —S—R A , aryl, heteroaryl, heterocyclyl, hydroxy, alkoxy, aryloxy, —C(O)—R A , R A —C(O)O— alkylcarboxylate, —SH, cyano, halogen, —C(═S)—R A , —OC(O)—NR A R B , R A —OC(O)—N(R A )—, —OC(═S)—NR A R B , R A —OC(═S)—N(R A )—, —C(O)NR A R B , R A —C(O)N(R A )—, (R A R B )N—S(O) 2 —, —N(R A )—S(O) 2 —R A , nitro, R A —S(═O)—, —S(O) 2 —R A , haloalkyl, haloalkoxyl, —S(O) 2 C(X′) 3 wherein X′ is halogen, —N(R A )S(O) 2 C(X′) 3 wherein X′ is halogen, amino, —N(R A )C(O)-heteroaryl, —N(R A )C(O)-heterocyclyl, —C(O)N(R A )-heteroaryl, —C(O)N(R A )-heterocyclyl, or a combination thereof.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 29, 2021
From: CHENGDU SYNBLIC THERAPEUTICS INC., LTD.
To: SUZHOU PUHE BIOPHARMA CO., LTD.
Reel/Frame 057648/0120 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 15, 2021
From: SYNBLIA THERAPEUTICS, INC.
To: CHENGDU SYNBLIC THERAPEUTICS INC., LTD.
Reel/Frame 057597/0774 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 18, 2019
From: XIE, YINONG; BABISS, LEE E.
To: SYNBLIA THERAPEUTICS, INC.
Reel/Frame 048932/0755 →
Continuity (2)
Provisional Application 62646107 · Mar 21, 2018
Related Publication 20190290649A1 · Sep 26, 2019
Cited By (1)
US 12,390,469