IP Library Granted Patent US 11,065,608
Granted Patent B2
US 11,065,608 · App. 16/359,136 · Granted Jul 20, 2021

Multidentate ligands and use thereof

Inventors: Gerard Parkin (New York, NY); Michael Rauch (New York, NY); Serge Ruccolo (Somerville, MA)
Assignee: THE TRUSTEES OF COLUMBIA UNIVERSITY IN THE CITY OF NEW YORK
B01J31/183B01J31/1633B01J2231/12B01J2231/321B01J2231/323B01J2231/645B01J2231/648B01J2531/0247B01J2531/11B01J2531/22B01J2531/26B01J2531/847
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Quick Facts
Patent No.
US 11,065,608
App. No.
16/359,136
Granted
Jul 20, 2021
Kind
B2
Abstract

The present invention provides, inter alia, a multidentate ligand having the structure of: Also provided are methods of preparing metal complexes from the multidentate ligand, and the metal complexes prepared by such methods. Further provided are catalysts comprising such metal complexes, and various uses of such catalysts.

Claims (7)

1. A multidentate ligand having the structure of formula

wherein:

Z is a linker group that comprises a silicon-containing group;

R 1 is selected from the group consisting of H, halide, alkyl, aryl, aralkyl, heteroalkyl, heteroaryl, alkoxy, hydroxy, heteroalkoxy, amino, alkylamino, arylamino, cyano, nitro, sulfonyl, or a heterocyclic group;

R 2 and R 3 are independently selected from the group consisting of H, halide, alkyl, aryl, aralkyl, heteroalkyl, heteroaryl, alkoxy, hydroxy, heteroalkoxy, amino, alkylamino, arylamino, cyano, nitro, sulfonyl, or a heterocyclic group; or together form a saturated or unsaturated C 5-7 homocyclic or heterocyclic ring, wherein the ring is optionally substituted with groups selected from H, halide, alkyl, aryl, aralkyl, heteroalkyl, heteroaryl, alkoxy, hydroxy, heteroalkoxy, amino, alkylamino, arylamino, cyano, nitro, sulfonyl, or a heterocyclic group.

2. The multidentate ligand of claim 1 , wherein Z is Si(R 4 ) 2 ; and wherein R 4 is selected from the group consisting of H, halide, alkyl, aryl, aralkyl, heteroalkyl, heteroaryl, alkoxy, hydroxy, heteroalkoxy, amino, alkylamino, arylamino, cyano or a heterocyclic group.

3. The multidentate ligand according to claim 1 , having the following structure:

Assignments (1)
CONFIRMATORY LICENSE Recorded Oct 25, 2019
From: COLUMBIA UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 050832/0532 →
Continuity (2)
Provisional Application 62646062 · Mar 21, 2018
Related Publication 20190291088A1 · Sep 26, 2019