IP Library Granted Patent US 11,404,290
Granted Patent B2
US 11,404,290 · App. 16/376,861 · Granted Aug 2, 2022

Method and apparatus for pulse gas delivery

Inventors: Junhua Ding (Boxborough, MA); Michael L'Bassi (Sterling, MA)
Assignee: MKS Instruments, Inc.
H01L21/67017G05B15/02G05D7/0647
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Quick Facts
Patent No.
US 11,404,290
App. No.
16/376,861
Granted
Aug 2, 2022
Kind
B2
Abstract

In a pulse gas delivery system, a chamber is pre-charged to a prescribed pressure through an upstream valve. Thereafter, a downstream control valve is opened to control flow of the gas during a gas pulse. A dedicated controller may control the downstream control valve in a feedback loop during the pulse based on pressure and temperature detected during the pulse.

Claims (93)

1. A pulse gas delivery system comprising:

a chamber having a volume;

a pressure sensor configured to detect pressure of gas within the chamber;

a temperature sensor configured to detect a temperature indicative of temperature of the gas within the chamber;

an upstream valve configured to control flow of a gas into the chamber;

a downstream adjustable control valve, the openness of which can be controlled, configured to control flow rate of the gas out of the chamber; and

a controller configured to control the upstream valve and the downstream control valve to charge the chamber to an initial pressure and to thereafter control measured flow rate through the downstream control valve during a gas pulse of the gas flowing out of the chamber to control delivered dose and period of the gas pulse, measured flow rate being calculated from a rate of pressure decay calculation based on the detected pressure and temperature, and

wherein the controller is further configured to control the downstream control valve to regulate the measured flow rate of the gas out of the chamber calculated from the rate of pressure decay calculation during the gas pulse to a targeted flow rate set point.

2. The pulse gas delivery system of claim 1 , wherein the controller is configured to control opening of the downstream control valve in a feedback loop to regulate the flow rate out of the system during the pulse based on pressure and temperature detected during the pulse.

3. The pressure based pulse gas delivery system of claim 1 , wherein the controller is configured to calculate the flow rate Q based on the following function:

Q

=

-

V

×

T

stp

P

stp

d

(

P

T

)

dt

where V represents the volume of the chamber, T stp represents standard temperature, P stp represents standard pressure, P represents the pressure of the gas within the chamber, and T represents the temperature of the gas within the chamber.

4. The pulse gas delivery system of claim 1 , wherein the controller is further configured to calculate a dose of the gas delivered out of the chamber and to control the downstream control valve to deliver a prescribed dose of gas during a prescribed period of the gas pulse.

5. The pulse gas delivery system of claim 4 , wherein the controller is configured to calculate the dose of the gas delivered out of the chamber based on volume of the chamber, the initial pressure of the gas within the chamber as detected by the pressure sensor when the pulse is started, the pressure of the gas within the chamber as detected by the pressure sensor during the pulse, and the temperature of the gas as detected by the temperature sensor during the pulse.

6. The pulse gas delivery system of claim 5 , wherein the controller is configured to calculate the dose Dn(t) of the gas delivered out of the chamber at a time t during the pulse according to the following function:

Dn ( t )= V× ( P t0 −P t )/( R×T t ),

where V represents the volume of the chamber, P t0 represents the pressure of the gas within the chamber when the pulse is started, P t represents the pressure of the gas within the chamber at the time t during the pulse, and T t represents the temperature of the gas at the time t during the pulse.

7. The pulse gas delivery system of claim 1 , wherein the controller is further configured to calculate a dose of the gas delivered out of the chamber and to control the downstream control valve to deliver a prescribed dose of gas during a prescribed period of the gas pulse.

8. The pulse gas delivery system of claim 7 , wherein the controller is configured to calculate the dose of the gas delivered out of the chamber based on the volume of the chamber, the initial pressure of the gas within the chamber as detected by the pressure sensor when the pulse is started, the pressure of the gas within the chamber as detected by the pressure sensor during the pulse, and the temperature of the gas as detected by the temperature sensor during the pulse.

9. The pulse gas delivery system of claim 8 , wherein the controller is configured to calculate the dose Dn(t) of the gas delivered out of the chamber at a time t during the pulse according to the following function:

Dn ( t )= V× ( P t0 −P t )/( R×T t ),

where V represents the volume of the chamber, P t0 represents the pressure of the gas within the chamber when the pulse is started, P t represents the pressure of the gas within the chamber at the time t during the pulse, and T t represents the temperature of the gas at the time t during the pulse.

10. The pulse gas delivery system of claim 1 , wherein the controller is configured to adjust the flow rate during the pulse to achieve a prescribed pulse shape.

11. The pulse gas delivery system of claim 1 , wherein the controller is configured to adjust the downstream control valve to achieve a constant flow rate during the pulse.

12. A method of pulse gas delivery comprising:

(i) opening an upstream valve while closing a downstream adjustable control valve to charge a chamber with a gas to an initial pressure;

(ii) closing the upstream valve when the initial pressure is reached;

(iii) once the initial pressure is reached and after the upstream valve is closed, opening the downstream adjustable control valve to start a pulse of the gas flowing out of the chamber;

(iv) measuring flow rate from a rate of pressure decay calculation during the pulse of the gas based on pressure and temperature of the gas in the chamber; and

(v) controlling openness of the downstream adjustable control valve during the pulse of the gas flowing out of the chamber to regulate the measured flow rate from the rate of pressure decay calculation to a targeted flow rate set point during the pulse of the gas and to deliver a prescribed dose over a prescribed period of the pulse.

13. The method of pulse gas delivery as claimed in claim 12 , further comprising detecting, during the pulse, pressure and temperature of the gas within the chamber and controlling the downstream control valve based on the detected pressure and temperature.

14. The method of pulse gas delivery as claimed in claim 12 , further comprising controlling the downstream control valve to be closed when the prescribed dose of gas is reached.

15. The method of pulse gas delivery as claimed in claim 12 , further comprising controlling the downstream control valve to be closed when a desired pulse on time is reached.

16. The method of pulse gas delivery as claimed in claim 12 , further comprising repeating (i) to (iv) under control of a dedicated controller for a number of pulses.

17. The method of pulse gas delivery as claimed in claim 12 further comprising, during the pulse, computing a dose of gas delivered out of the chamber and controlling the downstream control valve to deliver a prescribed dose of gas during a prescribed pulse time.

18. The method of pulse gas delivery as claimed in claim 12 further comprising adjusting flow rate during the pulse to achieve a prescribed pulse shape.

19. The method of pulse gas delivery as claimed in claim 12 further comprising adjusting the downstream control valve during the pulse to achieve a constant flow rate during the pulse.

20. A method of delivering a pulse of gas, the method comprising:

opening an upstream valve while closing a downstream adjustable control valve to charge a chamber with a gas to an initial pressure;

closing the upstream valve when the initial pressure is reached;

once the initial pressure is reached and after the upstream valve is closed, opening the downstream adjustable control valve to start a pulse of the gas flowing out of the chamber;

detecting a pressure of the gas within the chamber with a pressure sensor;

detecting a temperature indicative of temperature of the gas within the chamber with a temperature sensor; and

regulating measured flow rate of the gas during the pulse of the gas flowing out of the chamber to a targeted flow rate set point by controlling the downstream adjustable control valve during the pulse of the gas, the measured flow rate being calculated from a rate of pressure decay calculation based on the detected pressure and temperature.

21. The method of claim 20 , wherein controlling the flow rate of the gas through the downstream control valve is based on feedback from the pressure and the temperature detected during the pulse.

22. The method of claim 20 , further comprising:

calculating the flow rate Q based on the following function:

Q

=

-

V

×

T

stp

P

stp

d

(

P

T

)

dt

,

where V represents volume of the chamber, T stp represents standard temperature, P stp represents standard pressure, P represents the pressure of the gas within the chamber, and T represents the temperature of the gas within the chamber.

23. The method of claim 20 , further comprising:

calculating a dose of the gas delivered out of the chamber and controlling the downstream control valve to deliver a prescribed dose of gas during a prescribed period of the gas pulse.

24. The method of claim 20 , further comprising:

calculating the dose of the gas delivered out of the chamber based on volume of the chamber, initial pressure of the gas within the chamber as detected by the pressure sensor when the pulse is started, the pressure of the gas within the chamber as detected by the pressure sensor during the pulse, and the temperature of the gas as detected by the temperature sensor during the pulse.

25. The method of claim 24 , further comprising:

calculating the dose Dn(t) of the gas delivered out of the chamber at a time t during the pulse according to the following function:

Dn ( t )= V× ( P t0 −P t )/( R×T t ),

where V represents the volume of the chamber, P t0 represents the pressure of the gas within the chamber when the pulse is started, P t represents the pressure of the gas within the chamber at the time t during the pulse, and T t represents the temperature of the gas at the time t during the pulse.

26. The method of claim 20 , further comprising:

adjusting flow rate during the pulse to achieve a prescribed pulse shape.

27. The method of claim 20 , further comprising: adjusting the downstream control valve to achieve a constant flow rate during the pulse.

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded Aug 24, 2022
From: BARCLAYS BANK PLC
To: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
Reel/Frame 062739/0001 →
RELEASE OF SECURITY INTEREST Recorded Aug 24, 2022
From: BARCLAYS BANK PLC
To: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
Reel/Frame 063009/0001 →
SECURITY INTEREST Recorded Aug 19, 2022
From: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 061572/0069 →
PATENT SECURITY AGREEMENT - ABL Recorded Aug 7, 2019
From: ELECTRO SCIENTIFIC INDUSTRIES, INC.; MKS INSTRUMENTS, INC.; NEWPORT CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049987/0762 →
PATENT SECURITY AGREEMENT - TERM LOAN Recorded Aug 7, 2019
From: ELECTRO SCIENTIFIC INDUSTRIES, INC.; MKS INSTRUMENTS, INC.; NEWPORT CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049987/0820 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 5, 2019
From: DING, JUNHUA; L'BASSI, MICHAEL
To: MKS INSTRUMENTS, INC.
Reel/Frame 048809/0719 →
Continuity (1)
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Cited By (1)
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