IP Library › Granted Patent US 10,494,501
Granted Patent B2
US 10,494,501 · App. 16/395,397 · Granted Dec 3, 2019

Nanocomposite hemp

Inventor: Ronald Kander (Philadelphia, PA)
Assignee: Thomas Jefferson University
C08K3/04B33Y10/00B33Y70/00C08G63/08C08J3/203B29C64/118B29K2055/02B29K2067/046B29K2511/10C08K2201/001C08K2201/005H01B1/24
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Quick Facts
Patent No.
US 10,494,501
App. No.
16/395,397
Granted
Dec 3, 2019
Kind
B2
Abstract

A composite material comprising a polymer and a carbonized hemp filler, wherein the carbonized hemp filler is produced by carbonizing hemp at a temperature of at least 1100 C to produce a char; and milling the char to produce a particle size, wherein the filler comprises 95% of particles of less than 10 microns in size; and wherein the hemp filler comprises between 1 and 50% of the total mass of the composite.

Claims (15)

1. A composite material comprising a polymer and a hemp char filler, wherein the hemp char filler is produced by carbonizing a portion of hemp at a temperature of at least 1100° C. to produce a hemp char; and milling the hemp char to produce the hemp char filler having an average particle size of between 0.001 and 10 microns; adding into hemp char filler a portion of polymer and milling the hemp char filler and polymer together to form the composite material, wherein the hemp char filler comprises 95% of particles of between 0.001 and 10 microns in size; and wherein the hemp char filler comprises between 1% and 50% of the total mass of the composite material; and wherein the composite does not contain silanes or a dispersing agent to disperse the hemp particles into the polymer before forming the composite material.

2. The composite of claim 1 , wherein the hemp particle filler comprises an average particle size of less than 2 microns.

3. The composite of claim 1 , wherein the milling comprises a cryomilling process.

4. The composite of claim 1 , wherein the hemp char filler is included at a sufficient density in the composite material wherein the resistance of the composite is less than 100Ω.

5. The composite material of claim 1 , wherein the composite material is extruded into a composite article.

6. A method of manufacturing a hemp based composite particles comprising: processing a portion of polymer to generate a polymer particle having an average particle size of between 0.001 and 10 microns, using a 30 Hz processing in an oscillating mill; processing a portion of hemp by cryomilling said hemp under liquid nitrogen at 30 Hz; and combining a portion of the polymer particle and a portion of the cryomilled hemp and milling them together at 30 Hz to form composite particles.

7. The method of claim 6 , wherein the composite particles are further processed by extrusion or molding to form a composite article.

8. The method of claim 6 , wherein the average particle size of the polymer particle is no more than 2 microns.

9. The method of claim 6 , wherein the average particle size of the cryomilled hemp is no more than 2 microns.

10. The method of claim 6 , wherein a composite particle comprises between 1 and 50% of the cryomilled hemp.

11. The method of claim 10 , wherein the composite material has a resistance of less than 100Ω.

12. The method of claim 6 , wherein the polymer is selected from a biodegradable polymer, a non-biodegradable polymer, or combinations thereof.

13. The method of claim 6 , wherein the portion of hemp is a carbonized hemp.

14. The method of claim 13 , wherein the carbonized hemp is charred at a temperature of greater than 600° C. under an inert gas.

15. The method of claim 6 , wherein the polymer is acrylonitrile butadiene styrene, polylactic acid, polyethylene terephthalate, polypropylene, or combinations thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 30, 2019
From: KANDER, RONALD
To: THOMAS JEFFERSON UNIVERSITY
Reel/Frame 049035/0869 →
Continuity (2)
Provisional Application 62663674 · Apr 27, 2018
Related Publication 20190330443A1 · Oct 31, 2019
Cited By (2)
US 12,466,971 US 12,728,592