IP Library › Granted Patent US 10,744,482
Granted Patent B2
US 10,744,482 · App. 16/434,472 · Granted Aug 18, 2020

Highly stable [MaMbF6-n(O/H2O)n(ligand)2(solvent)x]n metal organic frameworks

Inventors: Mohamed Eddaoudi (Thuwal, SA); Karim Adil (Thuwal, SA); Youssef Belmabkhout (Thuwal, SA); Osama Shekhah (Thuwal, SA); Prashant M. Bhatt (Thuwal, SA); Amandine Cadiau (Thuwal, SA)
Assignee: KING ABDULLAH UNIVERSITY OF SCIENCE AND TECHNOLOGY
B01J20/226B01D53/02B01J20/2808B01J20/28061B01J20/28071B01J20/3078B01J20/3085C07D241/10C07F19/005B01D2253/204B01D2256/245B01D2257/304B01D2257/504B01D2258/05Y02C10/08Y02P20/152
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Quick Facts
Patent No.
US 10,744,482
App. No.
16/434,472
Granted
Aug 18, 2020
Kind
B2
Abstract

Embodiments of the present disclosure describe metal-organic framework compositions comprising a pillar characterized by the formula (M b F 5 (O/H 2 O)), where M b is selected from periodic groups IIIA, IIIB, IVB, VB, VIB, and VIII; and a square grid characterized by the formula (M a (ligand) x ), where M a is selected from periodic groups IB, IIA, IIB, IIIA, IVA, IVB, VIB, VIIB, and VIII, ligand is a polyfunctional organic ligand, and x is 1 or more; wherein the pillaring of the square grid with the pillars forms the metal-organic framework.

Claims (11)

1. A metal-organic framework, comprising:

a pillar characterized by the formula (M b F 5 (O/H 2 O)), where M b is selected from periodic groups IIIA, IIIB, IVB, VB, VIB, and VIII; and

a square grid characterized by the formula (M a (ligand) x ), where M a is selected from periodic groups IB, IIA, IIB, IIIA, IVA, IVB, VIB, VIIB, and VIII, where the ligand is selected from pyrimidine, pyridazine, triazine, thiazole, oxazole, pyrrole, imidazole, pyrazole, triazole, oxadiazole, thiadiazole, quinoline, benzoxazole, and benzimidazole, where x is 1 or more;

wherein the square grid and pillar associate to form the metal-organic framework and wherein the metal-organic framework includes open metal sites.

2. The metal-organic framework of claim 1 , wherein M b is selected from Al′, Ga 3+ , Fe +2 , Fe +3 , Cr 2+ , Cr 3+ , Ti 3+ , V 3+ , V 5+ , Sc 3+ , In 3+ , Nb 5+ , and Y 3+ .

3. The metal-organic framework of claim 1 , wherein M a is selected from Cu 2+ , Zn 2+ , Co 2+ , Ni 2+ , Mn 2+ , Zr 2+ , Fe 2+ , Ca 2+ , Ba 2+ , Pb 2+ , Pt 2+ , Pd 2+ , Ru 2+ , Rh 2+ , Cd 2+ , Mg 2+ , Al +3 , Fe 2+ , Fe +3 , Cr 2+ , Cr 3+ , Ru 2+ , Ru 3+ , and Co 3+ .

4. The metal-organic framework of claim 1 , wherein the pillar is (NbOF 5 ) 2− , (AlF 5 (H 2 O)) 2− , or FeF 5 ((H 2 O)) 2− .

5. A metal-organic framework, comprising:

a pillar characterized by the formula (M b F 5 (O/H 2 O)), where M b is selected from periodic groups IIIA, IIIB, IVB, VB, VIB, and VIII; and

a square grid characterized by the formula (M a (ligand) x ), where M a is selected from periodic groups IB, IIA, IIB, IIIA, IVA, IVB, VIB, VIIB, and VIII, where the ligand is selected from pyrimidine, pyridazine, triazine, thiazole, oxazole, pyrrole, imidazole, pyrazole, triazole, oxadiazole, thiadiazole, quinoline, benzoxazole, and benzimidazole, where x is 1 or more;

wherein the square grid and pillar associate to form the metal-organic framework and wherein the metal-organic framework includes a double-bonded oxygen.

Continuity (3)
Continuation 15564909
Provisional Application 62144156 · Apr 7, 2015
Related Publication 20190282998A1 · Sep 19, 2019
Cited By (3)
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