IP Library Granted Patent US 10,822,968
Granted Patent B2
US 10,822,968 · App. 16/435,484 · Granted Nov 3, 2020

Microstructure geometry for thermal barrier coatings to mitigate CMAS attack

Inventors: Eric Jordan (Storrs, CT); Rishi Kumar (Ashford, CT)
Assignee: University of Connecticut
F01D5/288C23C4/134C23C14/28F05D2220/32F05D2230/90
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Quick Facts
Patent No.
US 10,822,968
App. No.
16/435,484
Granted
Nov 3, 2020
Kind
B2
Abstract

Thermal barrier coatings and methods to make such coatings present improved resistance to CMAS infiltration. The method for forming a thermal barrier coating includes applying a layer of the thermal barrier coating to a component having a surface, forming a plurality of first channels in the thermal barrier coating, and forming a plurality of second channels in the thermal barrier coating. The first channels extend through a thickness of the thermal barrier coating from an interface with the surface of the component to a free surface opposite the interface. The second channels are disposed between the free surface and the interface and extending lengthwise generally parallel to the free surface of the thermal barrier coating.

Claims (31)

1. A method for forming a thermal barrier coating, the method comprising:

applying a layer of the thermal barrier coating to a component having a surface; and

forming a plurality of first channels in the thermal barrier coating, wherein the first channels extend through a thickness of the thermal barrier coating from an interface with the surface of the component and a free surface opposite the interface; and

forming a plurality of second channels disposed between the free surface and the interface and extending lengthwise generally parallel to the free surface of the thermal barrier coating;

wherein forming the plurality of second channels further comprises forming the plurality of second channels to have an average cross-sectional span in a range of about 1 micron to 50 microns.

2. The method of claim 1 , further comprising forming the plurality of second channels to have an average cross-sectional span in a range of about 4 microns to 15 microns.

3. The method of claim 1 , further comprising forming the plurality of second channels by a solution precursor plasma spray process.

4. The method of claim 1 , further comprising forming the plurality of second channels by a thermal spray of powders and suspensions.

5. The method of claim 1 , further comprising forming the plurality of second channels by an electron beam physical vapor deposition process.

6. The method of claim 1 , further comprising forming the plurality of first channels and the plurality of second channels at locations for reactive blocking of calcium magnesium aluminum silicates (CMAS) infiltration.

7. The method of claim 1 , wherein forming the plurality of first channels further comprises spacing the plurality of first channels about 33 microns to 400 microns apart.

8. The method of claim 1 , wherein forming the plurality of first channels further comprises forming openings in the free surface of the thermal barrier coating.

9. The method of claim 1 , wherein forming the plurality of second channels further comprises forming openings in at least some of the first channels and connecting some of the second channels to some of the first channels.

10. A method for forming a thermal barrier coating, the method comprising:

applying a layer of the thermal barrier coating to a component having a surface; and

forming a plurality of first channels in the thermal barrier coating, wherein the first channels extend through a thickness of the thermal barrier coating from an interface with the surface of the component and a free surface opposite the interface, wherein forming the plurality of first channels further comprises spacing the plurality of first channels about 33 microns to 400 microns apart; and

forming a plurality of second channels disposed between the free surface and the interface and extending lengthwise generally parallel to the free surface of the thermal barrier coating.

11. The method of claim 10 , further comprising forming the plurality of second channels to have an average cross-sectional span in a range of about 4 microns to 15 microns.

12. The method of claim 10 , further comprising forming the plurality of second channels by a solution precursor plasma spray process.

13. The method of claim 10 , further comprising forming the plurality of first channels and the plurality of second channels at locations for reactive blocking of calcium magnesium aluminum silicates (CMAS) infiltration.

14. The method of claim 10 , wherein forming the plurality of first channels further comprises forming openings in the free surface of the thermal barrier coating.

15. The method of claim 10 , wherein forming the plurality of second channels further comprises forming openings in at least some of the first channels and connecting some of the second channels to some of the first channels.

16. A method for forming a thermal barrier coating, the method comprising:

applying a layer of the thermal barrier coating to a component having a surface; and

forming a plurality of first channels in the thermal barrier coating, wherein the first channels extend through a thickness of the thermal barrier coating from an interface with the surface of the component and a free surface opposite the interface; and

forming a plurality of second channels disposed between the free surface and the interface and extending lengthwise generally parallel to the free surface of the thermal barrier coating;

wherein forming the plurality of second channels further comprises forming openings in at least some of the first channels and connecting some of the second channels to some of the first channels.

17. The method of claim 16 , further comprising forming the plurality of second channels to have an average cross-sectional span in a range of about 4 microns to 15 microns.

18. The method of claim 16 , further comprising forming the plurality of second channels by a solution precursor plasma spray process.

19. The method of claim 16 , further comprising forming the plurality of first channels and the plurality of second channels at locations for reactive blocking of calcium magnesium aluminum silicates (CMAS) infiltration.

20. The method of claim 16 , wherein forming the plurality of first channels further comprises forming openings in the free surface of the thermal barrier coating.

Assignments (2)
CONFIRMATORY LICENSE Recorded Nov 4, 2020
From: UNIVERSITY OF CONNECTICUT SCH OF MED/DNT
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 054299/0711 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 31, 2020
From: JORDAN, ERIC; KUMAR, RISHI
To: UNIVERSITY OF CONNECTICUT
Reel/Frame 053651/0203 →
Continuity (2)
Provisional Application 62682635 · Jun 8, 2018
Related Publication 20200024979A1 · Jan 23, 2020