IP Library Granted Patent US 12,091,390
Granted Patent B2
US 12,091,390 · App. 16/442,770 · Granted Sep 17, 2024

Rosuvastatin calcium and process for producing intermediate thereof

Inventors: Naoyuki Watanabe (Fukuoka, JP); Tomoko Maeda (Kanagawa, JP); Yasumasa Dekishima (Kanagawa, JP); Hiroshi Kawabata (Kanagawa, JP); Masaki Nagahama (Fukuoka, JP)
Assignee: API CORPORATION
C07D239/42C12N9/0006C12P17/12C12Y101/01184
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Quick Facts
Patent No.
US 12,091,390
App. No.
16/442,770
Granted
Sep 17, 2024
Kind
B2
Abstract

An object of the present invention is to provide a novel method capable of producing rosuvastatin calcium and intermediates therefor efficiently, inexpensively and with high purity. The present invention provides a method of efficiently producing rosuvastatin calcium and intermediates therefor having a high purity at an industrial scale, without using an extremely low temperature reaction or a special asymmetric catalyst.

Claims (9)

1. A production method of a compound represented by the following formula (1a):

wherein R is a n-propyl group or an isopropyl group, comprising

(iia) condensing a compound represented by the following formula (3):

and a compound represented by the following formula (4a):

wherein R 2 is a tert-butyl group, in the presence of a base to obtain a compound represented by the following formula (5):

wherein R 2 is as defined for R 2 in said formula (4a); and

(iib) reacting the compound represented by formula (5) with an alcohol represented by R—OH wherein R is a n-propyl group or an isopropyl group.

2. The production method of claim 1 , wherein R is the isopropyl group.

3. The production method of claim 1 , wherein R is the n-propyl group.

Assignments (3)
MERGER Recorded Sep 23, 2025
From: API CORPORATION
To: UBE CORPORATION
Reel/Frame 072344/0161 →
CHANGE OF ADDRESS Recorded Jun 21, 2023
From: API CORPORATION
To: API CORPORATION
Reel/Frame 064103/0580 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 17, 2019
From: WATANABE, NAOYUKI; MAEDA, TOMOKO; DEKISHIMA, YASUMASA; KAWABATA, HIROSHI; NAGAHAMA, MASAKI
To: API CORPORATION
Reel/Frame 049486/0904 →
Priority Claims (3)
JP 2014-021769 · Feb 6, 2014 · national
JP 2014-209142 · Oct 10, 2014 · national
JP 2014-209480 · Oct 10, 2014 · national
Continuity (3)
Division 15600196 · May 19, 2017
Division 15116861
Related Publication 20190315696A1 · Oct 17, 2019