IP Library Granted Patent US 10,971,635
Granted Patent B2
US 10,971,635 · App. 16/443,065 · Granted Apr 6, 2021

Conductive polymer nanowires—graphene hybrids with improved optoelectronic properties

Inventors: Mircea Cotlet (Rocky Point, NY); Mingxing Li (Huntington Station, NY)
Assignee: BROOKHAVEN SCIENCE ASSOCIATES, LLC
H01L31/02167H01L51/0036H01L51/0045H01L51/428H01L51/4213H01L31/028H01L2031/0344
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Quick Facts
Patent No.
US 10,971,635
App. No.
16/443,065
Granted
Apr 6, 2021
Kind
B2
Abstract

A photodetector including graphene and poly(3-hexylthiopene) (P3HT) nanowires is claimed. A method of making the hybrid photodetector is also claimed.

Claims (12)

1. A hybrid photodetector comprising atomically thin graphene and a conductive polymer wherein the conductive polymer is poly (3-hexylthiophene) (P3HT) nanowires self-assembled from regioregular P3HT and a mesh-like mesostructure is formed on top of the atomically thin graphene with voids between nanowires in the range of the wavelength of light.

2. The photodetector of claim 1 , wherein the P3HT nanowires are about 2-4 μm in length.

3. The photodetector of claim 1 , wherein the photodetector comprises no planar P3HT thin film.

4. The photodetector of claim 1 , wherein the graphene has a thickness of about 0.33 nm.

5. The photodetector of claim 1 , wherein the graphene has a thickness of 0.33 nm and the P3HT nanowires have a thickness of 11 nm.

6. A method of making a hybrid photodetector comprising (1) providing regioregular poly (3-hexylthiophene) (P3HT) and atomically thin graphene; (2) either using a Whiskers method or a mixed solvent method to make the regioregular P3HT self-assemble into P3HT nanowires; and (3) either dropping or spin-casting the P3HT nanowires onto the graphene to form a conductive nanowire mesh hybrid photodetector.

7. The method of claim 6 , wherein the mixed solvent method is used and the solvents are chlorobenzene and acetone.

8. The method of claim 7 , wherein the regioregular P3HT is dissolved in chlorobenzene to form a solution then heated for at least 3 hours; acetone is added to the solution with stirring to form a mixed solution; and the mixed solution is stirred and heated for at least 10 hours then cooled to room temperature.

9. The method of claim 8 , wherein the ratio of chlorobenzene to acetone is about 3:1.

10. The method of claim 8 , wherein the solution is heated to about 95° C. and the mixed solution is heated to about 90° C.

11. The method of claim 7 , wherein the P3HT nanowires are present in the solvents in a concentration of about 0.5 to about 2.5 mg/ml.

12. The method of claim 6 , wherein spin-casting is used and the spin-casting occurs at about 1500 rpm to about 2500 rpm.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jun 18, 2020
From: BROOKHAVEN SCIENCE ASSOC-BROOKHAVEN LAB
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 052977/0128 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 1, 2019
From: COTLET, MIRCEA; LI, MINGXING
To: BROOKHAVEN SCIENCE ASSOCIATES, LLC
Reel/Frame 049934/0595 →
Continuity (2)
Provisional Application 62688734 · Jun 22, 2018
Related Publication 20190393436A1 · Dec 26, 2019