IP Library Granted Patent US 11,253,528
Granted Patent B2
US 11,253,528 · App. 16/448,838 · Granted Feb 22, 2022

Stabilized modified release Vitamin D formulation and method of administering same

Inventors: Jay A. White (Newmarket, CA); Samir P. Tabash (Whitby, CA); Sammy A. Agudoawu (Mississauga, CA); Joel Z. Melnick (Evanston, IL)
Assignee: EIRGEN PHARMA LTD.
A61K31/593A61K9/2054A61K9/2866A61K9/4866A61K31/592A61K47/38A61K47/44
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Quick Facts
Patent No.
US 11,253,528
App. No.
16/448,838
Granted
Feb 22, 2022
Kind
B2
Abstract

A stabilized formulation for controlled release of a vitamin D compound is disclosed. The formulation comprises one or both of 25-hydroxyvitamin D 2 and 25-hydroxyvitamin D 3 and a cellulosic compound. The stabilized formulations exhibit a stable dissolution profile following exposure to storage conditions and demonstrate improved pharmacokinetic parameters compared to unstabilized formulations.

Claims (12)

1. A pharmaceutical composition comprising a storage-stabilized formulation for sustained release of a vitamin D compound, wherein the storage-stabilized formulation comprises a mixture of: a vitamin D compound; and a stabilizing agent comprising a cellulose ether in an amount of about 5 wt % to about 30 wt % of the storage-stabilized formulation, wherein the stabilizing agent maintains a difference of less than 30% between the amount of vitamin D compound released at any given time point after four hours during in vitro dissolution after two months exposure to storage conditions of 25° C. and 60% relative humidity and the amount released at the same dissolution time point during in vitro dissolution conducted prior to exposing the formulation to the storage conditions,

wherein the storage-stabilized formulation comprises a lipophilic matrix comprising the vitamin D compound.

2. The pharmaceutical composition of claim 1 , wherein the lipophilic matrix comprises a wax.

3. The pharmaceutical composition of claim 1 , wherein the storage-stabilized formulation is an oral formulation for sustained release of the vitamin D compound in the gastrointestinal tract of a subject which ingests the formulation.

4. The pharmaceutical composition of claim 1 , wherein the storage-stabilized formulation comprises a matrix that releasably binds and controllably releases the vitamin D compound.

5. The pharmaceutical composition according to claim 1 , wherein the cellulose ether comprises one or more of methylcellulose, hydroxyl propyl methylcellulose, hydroxyl ethyl methylcellulose, hydroxyl ethyl cellulose, and hydroxyl propyl cellulose.

6. The pharmaceutical composition according to claim 4 , wherein the cellulose ether comprises hydroxyl propyl methylcellulose.

7. The pharmaceutical composition according to claim 1 , wherein the vitamin D compound is one or more of vitamin D 3 (cholecalciferol), vitamin D 2 (ergocalciferol), 25-hydroxyvitamin D 3 , 25-hydroxyvitamin D 2 , 25-hydroxyvitamin D 4 , 25-hydroxyvitamin D 5 , 25-hydroxyvitamin D 7 , 1α,25-dihydroxyvitamin D 3 , 1α,25-dihydroxyvitamin D 2 , 1α,25-dihydroxyvitamin D 4 , 1,25-dihydroxy-19-nor-vitamin D 2 , and 1α-hydroxyvitamin D 3 .

8. The pharmaceutical composition according to claim 7 , wherein the vitamin D compound comprises one or both of 25-hydroxyvitamin D 2 and 25-hydroxyvitamin D 3 .

9. The pharmaceutical composition according to claim 1 , wherein the vitamin D compound comprises 25-hydroxyvitamin D 3 .

10. The pharmaceutical composition of claim 1 , wherein the storage-stabilized formulation is in the form of a capsule, tablet, sachet, dragee, or suppository.

11. The pharmaceutical composition of claim 10 , wherein the storage-stabilized formulation is in the form of a capsule.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 30, 2021
From: OPKO IRELAND GLOBAL HOLDINGS, LTD.
To: EIRGEN PHARMA LTD.
Reel/Frame 055765/0953 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 27, 2020
From: WHITE, JAY A.; TABASH, SAMIR P.; AGUDOAWU, SAMMY A.; MELNICK, JOEL Z.
To: OPKO IP HOLDINGS II, INC.
Reel/Frame 054182/0497 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 27, 2020
From: OPKO IP HOLDINGS II, INC.
To: OPKO IRELAND GLOBAL HOLDINGS, LTD.
Reel/Frame 054182/0554 →
Continuity (4)
Division 15720948 · Sep 29, 2017
Continuation 14213285 · Mar 14, 2014
Provisional Application 61801896 · Mar 15, 2013
Related Publication 20190374555A1 · Dec 12, 2019
Cited By (1)
US 12,478,631