IP Library Granted Patent US 10,695,316
Granted Patent B2
US 10,695,316 · App. 16/459,771 · Granted Jun 30, 2020

Methods of heating cannabis plant material

Inventors: Virgil Macaluso (Independence, KS); Corey Lowdon (Independence, KS); Shih-Shin Chou (Independence, KS)
Assignees: Virgil Macaluso; William G. Bale; Catalytic Industrial Group, Inc.
A61K31/352A61K36/185A01G7/00A61K31/05A61K45/06A61K2236/37C07C37/68
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Quick Facts
Patent No.
US 10,695,316
App. No.
16/459,771
Granted
Jun 30, 2020
Kind
B2
Abstract

The present invention includes a method of drying Cannabis plant material generally comprising exposing the Cannabis plant material to infrared radiation emitted from an infrared heater, such as a catalytic gas heater, the radiation having a wavelength of from about 3 to about 10 microns; and heating the Cannabis plant material to a temperature of from about 100° F. to about 400° F.

Claims (34)

1. A method of drying a cannabis plant material comprising an untrimmed, freshly harvested cannabis plant or at least one of an intact leaf, stalk, stem, flower, or bud of a freshly harvested cannabis plant, the method comprising:

exposing the cannabis plant material to infrared radiation emitted from an infrared heater, the radiation having a wavelength of from about 3 to about 10 microns; and

heating the cannabis plant material to a temperature of from about 100° F. to about 400° F.

2. The method of claim 1 , wherein the cannabis plant material is exposed to the infrared radiation for a period of time such that less than 25% of a cannabinoid compound in the cannabis plant material is decarboxylated.

3. The method of claim 2 , wherein the cannabinoid compound comprises cannabidiolic acid (CBDA).

4. The method of claim 2 , wherein the cannabinoid compound comprises tetrahydrocannabinolic acid (THCA).

5. The method of claim 1 , further including a step of circulating air over the cannabis plant material.

6. The method of claim 1 , wherein the infrared heater is a catalytic gas heater operating at a gas pressure allowing heater output from 50% to 100% of rated power.

7. The method of claim 1 , wherein the method does not comprise actively controlling the humidity of the air around the cannabis plant material while being exposed to the infrared radiation.

8. The method of claim 1 , wherein the cannabis plant material does not exceed 180° F. during the heating step.

9. The method of claim 1 , wherein the heating step comprises removing at least 10% of the moisture content from the cannabis plant material.

10. The method of claim 1 , wherein the cannabis plant material is exposed to the infrared radiation for a period of time such that more than 75% of a cannabinoid compound in the cannabis plant material is decarboxylated.

11. The method of claim 10 , wherein the cannabis plant material reaches a temperature of at least 285° F. during the heating step.

12. The method of claim 10 , wherein the cannabis plant material is exposed to the infrared radiation for at least 3 minutes.

13. The method of claim 10 , wherein the infrared heater is a catalytic gas heater operating at a gas pressure that allows heater output to vary from 50% to 100% of rated power.

14. The method of claim 1 , wherein, prior to exposing the cannabis plant material to infrared radiation, the cannabis plant material is water cured for about 1 to about 10 hours.

15. The method of claim 1 , wherein heating the cannabis plant material volatilizes water and terpenes from the cannabis plant material, the method further comprising condensing at least a portion of the water and terpenes.

16. The method of claim 15 , further comprising extracting and recovering the terpenes from the water.

17. The method of claim 1 , wherein the cannabis plant material is heated while in a cool or refrigerated environment having a temperature below about 70° F.

18. The method of claim 1 , further comprising cooling the cannabis plant material to a temperature of from about 40° F. to about 90° F. and subsequently heating the cannabis plant material to a temperature of from about 100° F. to about 400° F.

19. The method of claim 1 , wherein the method is capable of reducing the levels of E. Coli, Salmonella , Aflatoxin, and/or Ochratoxin below the detectable limits.

20. A method of decarboxylating a cannabinoid compound contained within a cannabis plant material comprising an untrimmed cannabis plant or at least one of an intact leaf, stalk, stem, flower, or bud of a cannabis plant, the method comprising:

exposing the cannabis plant material to infrared radiation emitted from an infrared heater, the radiation having a wavelength of from about 3 to about 10 microns; and

heating the cannabis plant material to a temperature of at least 200° F. for a sufficient time so as to decarboxylate at least 50% of the cannabinoid compound contained within the cannabis plant material.

21. The method of claim 20 , wherein the cannabinoid compound comprises cannabidiolic acid (CBDA).

22. The method of claim 21 , wherein at least 75% of the CBDA present within the cannabis plant material is decarboxylated into cannabidiol (CBD).

23. The method of claim 20 , wherein the cannabinoid compound comprises tetrahydrocannabinolic acid (THCA).

24. The method of claim 23 , wherein at least 75% of the THCA within the cannabis plant material is decarboxylated into tetrahydrocannabinol (THC).

25. A method of drying a cannabis plant material comprising an untrimmed, freshly harvested cannabis plant or at least one of an intact leaf, stalk, stem, flower, or bud of a freshly harvested cannabis plant while reducing the incidence of decarboxylation of a cannabinoid compound contained within the cannabis plant material, the method comprising:

exposing the cannabis plant material to infrared radiation emitted from an infrared heater, the radiation having a wavelength of from about 3 to about 10 microns; and

heating the cannabis plant material to a temperature of from about 100° F. to about 160° F. to produce a dried cannabis plant material,

wherein the dried cannabis plant material has a ratio of the cannabinoid compound to the decarboxylated cannabinoid compound of at least 2:1.

26. The method of claim 25 , further including a step of circulating air over the cannabis plant material and not requiring a step of actively controlling the humidity of the air around the cannabis plant material.

27. The method of claim 25 , wherein the cannabis plant material is exposed for a duration of time such that a moisture water content loss is at least 7.5%.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 24, 2021
From: BALE, WILLIAM G.
To: CATALYTIC INDUSTRIAL GROUP, INC.
Reel/Frame 058204/0518 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 9, 2021
From: MACALUSO, VIRGIL
To: CATALYTIC INDUSTRIAL GROUP, INC.
Reel/Frame 058057/0219 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2019
From: MACALUSO, VIRGIL
To: MACALUSO, VIRGIL; BALE, WILLIAM G.
Reel/Frame 049712/0738 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2019
From: LOWDON, COREY; CHOU, SHIH-SHIN
To: CATALYTIC INDUSTRIAL GROUP, INC.
Reel/Frame 049712/0837 →
Continuity (2)
Provisional Application 62693651 · Jul 3, 2018
Related Publication 20200009109A1 · Jan 9, 2020
Cited By (3)
US 1,117,976 US 1,122,511 US 1,138,114