IP Library Granted Patent US 11,014,920
Granted Patent B2
US 11,014,920 · App. 16/461,825 · Granted May 25, 2021

Factor XIIa inhibitors

Inventors: Jacqueline D. Hicks (Watchung, NJ); Brian Alexander McKittrick (New Vernon, NJ); Brent R. Whitehead (Morristown, NJ); Matthew Lombardo (Flemington, NJ); Xiaoqing Han (Edison, NJ); Jerry A. Taylor (Trenton, NJ); Hong Dong Chu (Livingston, NJ); Sung-Sau So (Verona, NJ); Peter Orth (Pittstown, NJ); Zhicai Wu (Montvale, NJ)
Assignee: Merck Sharp & Dohme Corp.
C07D417/14A61P7/02C07D401/12C07D409/12C07D409/14C07D417/12
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Quick Facts
Patent No.
US 11,014,920
App. No.
16/461,825
Granted
May 25, 2021
Kind
B2
Abstract

The present invention provides a compound of Formula I and pharmaceutical compositions comprising one or more said compounds, and methods for using said compounds for treating or preventing thromboses, embolisms, hypercoagulability or fibrotic changes. The compounds are selective Factor XIIa inhibitors.

Claims (31)

1. A compound of the formula:

wherein R 1 is aryl or heteroaryl, wherein said aryl and heteroaryl groups are optionally substituted with one to three substituents independently selected from the group consisting of hydroxyl, cyano, halo, C 1-3 alkyl, O(C 1-3 alkyl), NH 2 , CH 2 NH 2 , (C═O)NH 2 or heteroaryl;

R 2 is aryl, heteroaryl,

wherein said aryl and heteroaryl groups are optionally substituted with one to three substituents independently selected from the group consisting of hydroxyl, oxo, cyano, halo, C 1-3 alkyl, C 1-3 haloalkyl, O(C 1-3 alkyl) and NH 2 ;

R 3 is hydrogen, C 1-3 alkyl,

or C 3-7 cycloalkyl;

R 4 is hydrogen or C 1-4 alkyl;

R 5 is

(a) hydrogen,

(b) CH 2 —C 3-6 cycloalkyl;

(c) piperidinyl, which is optionally substituted with hydroxyl, oxo, cyano, halo or C 1-3 alkyl, or

(d) C 1-4 alkyl which is optionally substituted with NR 6 R 7 , N + (CH 3 ) 3 , NH(C═O)R 6 , O(C═O)R 6 , NR 6 SO 2 R 7 , NHSO 2 cyclopropyl or heterocyclyl, wherein said heterocyclyl is optionally substituted with R 6 ;

R 6 is hydrogen or C 1-4 alkyl, which is optionally substituted with one to three substituents independently selected from the group consisting of halo and hydroxyl;

R 7 is hydrogen or C 1-3 alkyl, which is optionally substituted with one to three substituents independently selected from the group consisting of halo and hydroxyl;

or a pharmaceutically acceptable salt thereof.

2. The compound of claim 1 wherein R 1 is indolyl, phenyl or thiazolyl, wherein said groups are optionally substituted with one to three substituents independently selected from the group consisting of halo, C 1-3 alkyl, NH 2 , and CH 2 NH 2 ,(C═O)NH 2 ; or a pharmaceutically acceptable salt thereof.

3. The compound of claim 2 wherein R 1 is thiazolyl, which is optionally substituted with C 1-3 alkyl, or a pharmaceutically acceptable salt thereof.

4. The compound of claim 1 wherein R 2 is thiazolyl, phenyl, dihydroquinolinyl,

wherein said thiazolyl and phenyl, groups are optionally substituted with one to three substituents independently selected from the group consisting of halo and C 1-3 alkyl; or a pharmaceutically acceptable salt thereof.

5. The compound of claim 1 wherein R 3 is cyclohexyl or

or a pharmaceutically acceptable salt thereof.

6. The compound of claim 1 wherein R 4 is hydrogen or methyl, or a pharmaceutically acceptable salt thereof.

7. The compound of claim 1 wherein R 5 is C 1-4 alkyl which is optionally substituted with NR 6 R 7 , NH(C═O)R 6 , NHSO 2 R 7 , NHSO 2 cyclopropyl or heterocyclyl, wherein said heterocyclyl is optionally substituted with R 7 ; or a pharmaceutically acceptable salt thereof.

8. A compound selected from

or a pharmaceutically acceptable salt thereof.

9. A pharmaceutical composition comprising a compound of claim 1 or a pharmaceutically acceptable salt thereof and a pharmaceutically acceptable carrier.

10. A method for inhibiting thrombus formation in blood or treating thrombus formation in blood comprising administering a composition of claim 9 to a mammal in need of thereof.

11. A method for preventing thrombus formation in blood comprising administering a composition of claim 9 to a mammal in need thereof.

12. A method of treating venous thromboembolism and pulmonary embolism in a mammal comprising administering a composition of claim 9 to a mammal in need thereof.

13. A method of treating deep vein thrombosis in a mammal comprising administering a composition of claim 9 to a mammal in need thereof.

14. A method of treating thromboembolic stroke in a human comprising administering a composition of claim 9 to a mammal in need thereof.

Assignments (2)
MERGER Recorded Aug 8, 2022
From: MERCK SHARP & DOHME CORP.
To: MERCK SHARP & DOHME LLC
Reel/Frame 061102/0145 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 17, 2019
From: HICKS, JACQUELINE D.; WHITEHEAD, BRENT R.; LOMBARDO, MATTHEW; HAN, XIAOQING; SO, SUNG-SAU; ORTH, PETER; WU, ZHICAI; TAYLOR, JERRY; MCKITTRICK, BRIAN ALEXANDER; CHU, HONG DONG
To: MERCK SHARP & DOHME CORP
Reel/Frame 049217/0914 →