IP Library Granted Patent US 11,376,566
Granted Patent B2
US 11,376,566 · App. 16/469,885 · Granted Jul 5, 2022

Catalyst and method for removing NOX from combustion exhaust gas

Inventors: Katsumi Nochi (Yokohama, JP); Koji Higashino (Yokohama, JP); Tomotsugu Masuda (Yokohama, JP)
Assignee: MITSUBISHI HEAVY INDUSTRIES, LTD.
B01J23/30B01D53/8628B01D53/90B01J35/1061B01J35/1066F01N3/10B01J2523/47B01J2523/55B01J2523/68B01J2523/69
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Quick Facts
Patent No.
US 11,376,566
App. No.
16/469,885
Granted
Jul 5, 2022
Kind
B2
Abstract

Provided is a catalyst for removing NOx from a combustion exhaust gas, in particular, a low-NOx combustion exhaust gas, wherein the catalyst has a ratio of a pore volume in a range of not less than 500 Å and not more than 3000 Å in a pore diameter relative to a total pore volume of not less than 15% and not more than 40% and preferably a ratio of a pore volume in a range of not less than 1000 Å in the pore diameter relative to the total pore volume of not less than 10% and not more than 45% in a pore volume distribution in a range of not more than 10 5 Å in the pore diameter, and where SILICA is unlikely to be deposited and even when the amount of SILICA deposited is increased, denitration performance is hardly lowered.

Claims (14)

1. A catalyst for removing NOx from a combustion exhaust gas, wherein the catalyst comprises an oxide of titanium, an oxide of molybdenum and/or tungsten, and an oxide of vanadium, wherein a ratio of V element to Ti element is not more than 2% by weight in terms of a weight percentage of V 2 O 5 /TiO 2 ,

the catalyst has a ratio of a pore volume in a range of pore diameter of not less than 500 A and not more than 3000 Å relative to a total pore volume of not less than 15% and not more than 40%, a ratio of a pore volume in a range of pore diameter of not less than 500 Å relative to the total pore volume of not less than 25% and not more than 50% and a ratio of a pore volume in a range of pore diameter of not less than 1000 Å relative to the total pore volume of not less than 10% and not more than 45% in a pore volume distribution in a range of pore diameter of not more than 10 5 Å.

2. The catalyst according to claim 1 , wherein the catalyst has a ratio of a pore volume in a range of pore diameter of not less than 40 Å and not more than 3000 Å relative to the total pore volume of not less than 80% in the pore volume distribution in the range of pore diameter of not more than 10 5 Å.

3. The catalyst according to claim 2 , wherein the catalyst has a ratio of a pore volume in a range of pore diameter of not less than 40 Å relative to the total pore volume of not less than 90% in the pore volume distribution in the range of pore diameter of not more than 10 5 Å.

4. The catalyst according to claim 2 , wherein a ratio of Mo element and/or W element to Ti element is not more than 5% by weight in terms of a weight percentage of (MoO 3 +WO 3 )/TiO 2 .

5. The catalyst according to claim 2 , wherein the catalyst has a ratio of a pore volume in a range of pore diameter of not less than 3000 Å relative to the total pore volume of not more than 10% in the pore volume distribution in the range of pore diameter of not more than 10 5 Å.

6. The catalyst according to claim 1 , wherein the catalyst has a ratio of a pore volume in a range of pore diameter of not less than 40 Å relative to the total pore volume of not less than 90% in the pore volume distribution in the range of pore diameter of not more than 10 5 Å.

7. The catalyst according to claim 6 , wherein a ratio of Mo element and/or W element to Ti element is not more than 5% by weight in terms of a weight percentage of (MoO 3 +WO 3 )/TiO 2 .

8. The catalyst according to claim 6 , wherein the catalyst has a ratio of a pore volume in a range of pore diameter of not less than 3000 Å relative to the total pore volume of not more than 10% in the pore volume distribution in the range of pore diameter of not more than 10 5 Å.

9. The catalyst according to claim 1 , wherein a ratio of Mo element and/or W element to Ti element is not more than 5% by weight in terms of a weight percentage of (MoO 3 +WO 3 )/TiO 2 .

10. The catalyst according to claim 1 , wherein the catalyst has a ratio of a pore volume in a range of pore diameter of not less than 3000 Å relative to the total pore volume of not more than 10% in the pore volume distribution in the range of pore diameter of not more than 10 5 Å.

11. A method comprising bringing a combustion exhaust gas into contact with the catalyst according to claim 1 , in the presence of ammonia to remove NOx from the combustion exhaust gas.

12. The method according to claim 11 , wherein the combustion exhaust gas is a low concentration-NOx combustion exhaust gas.

13. The method according to claim 12 , wherein the combustion exhaust gas has a NOx concentration of not more than 350 ppm.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2022
From: MITSUBISHI POWER, LTD.
To: MITSUBISHI HEAVY INDUSTRIES, LTD.
Reel/Frame 059944/0715 →
CHANGE OF NAME Recorded Sep 21, 2020
From: MITSUBISHI HITACHI POWER SYSTEMS, LTD.
To: MITSUBISHI POWER, LTD.
Reel/Frame 053838/0787 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2019
From: NOCHI, KATSUMI; HIGASHINO, KOJI; MASUDA, TOMOTSUGU
To: MITSUBISHI HITACHI POWER SYSTEMS, LTD.
Reel/Frame 049517/0867 →
Priority Claims (1)
JP JP2016-243167 · Dec 15, 2016 · national
Continuity (1)
Related Publication 20190314789A1 · Oct 17, 2019