IP Library › Granted Patent US 11,479,661
Granted Patent B2
US 11,479,661 · App. 16/477,747 · Granted Oct 25, 2022

Rubber composition, aging-resistant rubber product using the same

Inventors: Tao Xu (Hangzhou, CN); Zhi Sheng Fu (Hangzhou, CN); An Yang Wu (Hangzhou, CN)
Assignee: HANGZHOU XINGLU TECHNOLOGIES CO., LTD.
C08L23/06B60C1/00B60S1/38C08L23/16E01D19/041E01D19/06F16F1/3605F16G1/06B60S2001/3829C08L2205/025C08L2205/03C08L2205/06C08L2207/07C08L2207/322C08L2312/00
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Quick Facts
Patent No.
US 11,479,661
App. No.
16/477,747
Granted
Oct 25, 2022
Kind
B2
Abstract

The present invention discloses a rubber composition, a processing method thereof, and an aging resistant rubber product using the rubber composition. The rubber composition comprises a rubber matrix and essential components, wherein, based on 100 parts by weight of the rubber matrix, the rubber matrix comprises a branched polyethylene with a content represented as A, in which 0<A≤100 parts, and an EPM and an EPDM with a content represented as B, in which 0≤B<100 parts; and the essential components comprise 1.5-10 parts of a crosslinking agent, 30-200 parts of a reinforcing filler, and 5-250 parts of a plasticizer. The rubber composition provided by present invention has good processability and can be used for producing rubber products with high aging resistance and compression set resistance.

Claims (23)

1. A rubber composition, comprising a rubber matrix and essential components, wherein the rubber matrix comprises, based on 100 parts by weight of the rubber matrix, a branched polyethylene with a content represented as A, in which 0<A≤100 parts, and an ethylene-propylene rubber with a content represented as B, in which 0≤b<100 parts; and based on 100 parts by weight of the rubber matrix, the essential components comprise 1.5-10 parts of a crosslinking agent, 30-200 parts of a reinforcing filler, and 5-250 parts of a plasticizer, wherein the branched polyethylene comprises an ethylene homopolymer having a degree of branching of from 60 to 105 branches/1000 carbon atoms, a weight average molecular weight of from 268,000 to 518,000, and a Mooney viscosity ML(1+4) at 125° C. of from 42 to 102.

2. The rubber composition according to claim 1 , wherein based on 100 parts by weight of the rubber matrix, the content of the branched polyethylene is A, in which 10≤A≤100 parts; said ethylene-propylene rubber is consisted of EPM and EPDM, and the content of EPM and EPDM is B, in which 0≤B≤90 parts, wherein the branched polyethylene is an ethylene homopolymer having a degree of branching of from 82 to 105 branches/1000 carbon atoms, a weight average molecular weight of from 268,000 to 401,000, and a Mooney viscosity ML(1+4) at 125° C. of from 42 to 101.

3. The rubber composition according to claim 1 , comprising a rubber matrix and essential components, wherein the rubber matrix comprises, in parts by weight, 100 parts of a branched polyethylene; and based on 100 parts by weight of the rubber matrix, the essential components comprise 1.5-10 parts of a crosslinking agent, 30-200 parts of a reinforcing filler, and 8-150 parts of a plasticizer.

4. The rubber composition according to claim 1 , wherein the crosslinking agent comprises at least one of a peroxide crosslinking agent and sulfur, wherein the peroxide crosslinking agent comprises at least one of di-tert-butyl peroxide, dicumyl peroxide, tert-butyl cumyl peroxide, 1,1-di-tert-butyl peroxide-3,3,5-trimethylcyclohexane, 2,5-dimethyl-2,5-di(tert-butylperoxy)hexane, 2,5-dimethyl-2,5-di(tert-butylperoxy)hexyne-3, bis(tert-butylperoxyisopropyl)benzene, 2,5-dimethyl-2,5-bis(benzoylperoxy)hexane, tert-butyl peroxybenzoate, and tert-butylperoxy-2-ethylhexyl carbonate; the reinforcing filler comprises at least one of carbon black, silica, calcium carbonate, talc, calcined clay, magnesium silicate, and magnesium carbonate; the plasticizer comprises at least one of pine tar, motor oil, naphthenic oil, paraffin oil, coumarone, RX-80, stearic acid, paraffin, and liquid polyisobutene.

5. The rubber composition according to claim 1 , further comprising auxiliary components, which comprise, based on 100 parts by weight of the rubber matrix, 0.2 to 10 parts of an auxiliary crosslinking agent, 0.5 to 3 parts of a stabilizer, 2 to 15 parts of a metal oxide, and 0 to 3 parts of a vulcanization accelerator; the auxiliary crosslinking agent comprises at least one of triallyl cyanurate, triallyl isocyanurate, ethylene glycol dimethacrylate, ethyl dimethacrylate, triethylene glycol dimethacrylate, triallyl trimellitate, trimethylolpropane trimethacrylate, ethylene glycol dimethacrylate, N,N′-m-phenylene bismaleimide, N,N′-bis(furfurylidene) acetone, 1,2-polybutadiene, paraquinonedioxime, sulfur, and a metal salt of an unsaturated carboxylic acid; the metal oxide comprises at least one of zinc oxide, magnesia, calcium oxide, lead monoxide, and lead tetroxide; the stabilizer comprises at least one of 2,2,4-trimethyl-1,2-dihydroquinoline polymer, 6-ethoxy-2,2,4-trimethyl-1,2-dihydroquinoline, and 2-mercaptobenzimidazole; the vulcanization accelerator comprises at least one of 2-mercaptobenzothiazole, dibenzothiazyl disulfide, tetramethyl thiuram monosulfide, tetramethyl thiuram disulfide, tetraethyl thiuram disulfide, N-cyclohexyl-2-benzothiazole sulfenamide, N,N-dicyclohexyl-2-benzothiazole sulfenamide, bismaleimide, and ethylene thiourea.

6. A rubber support, wherein, a rubber compound used for the rubber support comprises a rubber composition comprising a rubber matrix and essential components, wherein the rubber matrix comprises, based on 100 parts by weight of the rubber matrix, a branched polyethylene with a content represented as A, in which 0<A≤100 parts, and an ethylene-propylene rubber with a content represented as B, in which 0≤B<100 parts; and based on 100 parts by weight of the rubber matrix, the essential components comprise 1.5-10 parts of a crosslinking agent, 30-200 parts of a reinforcing filler, and 5-250 parts of a plasticizer, wherein the branched polyethylene comprises an ethylene homopolymer having a degree of branching of not less than 50 branches/1000 carbon atoms, a weight average molecular weight of not less than 50,000, and a Mooney viscosity ML(1+4) at 125° C. of not less than 2; and

wherein either:

the rubber support is a plate-type rubber support of bridge and comprises a steel plate and a rubber sheet, wherein the rubber sheet comprises the rubber compound;

the rubber support is a basin-type rubber support and comprises a rubber bearing plate comprising the rubber compound; or

the rubber support is a vehicle shock-absorbing support.

7. An aging resistant rubber product, wherein, a rubber compound used for the aging resistant rubber product comprises a rubber composition comprising a rubber matrix and essential components, wherein the rubber matrix comprises, based on 100 parts by weight of the rubber matrix, a branched polyethylene with a content represented as A, in which 0<A≤100 parts, and an ethylene-propylene rubber with a content represented as B, in which 0≤B<100 parts; and based on 100 parts by weight of the rubber matrix, the essential components comprise 1.5-10 parts of a crosslinking agent, 30-200 parts of a reinforcing filler, and 5-250 parts of a plasticizer, wherein the branched polyethylene comprises an ethylene homopolymer having a degree of branching of not less than 50 branches/1000 carbon atoms, a weight average molecular weight of not less than 50,000, and a Mooney viscosity ML(1+4) at 125° C. of not less than 2.

8. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a rubber expansion and contraction installation for bridge, which comprises a rubber expansion and contraction body, the rubber compound used for said rubber expansion and contraction body comprises said rubber composition.

9. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a rubber and steel plate composite expansion and contraction installation, which comprises a rubber expansion and contraction body, the rubber compound used for said rubber expansion and contraction body comprises said rubber composition.

10. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a rubber railway pad.

11. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a rubber fender.

12. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a rubber water stop.

13. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a rubber roller.

14. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a high temperature-resistant ribbed belt.

15. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a windshield wiper.

16. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is a waterproof coil.

17. The aging resistant rubber product according to claim 7 , wherein, said aging resistant rubber product is an inner tire.

18. The rubber composition according to claim 1 , wherein the ethylene homopolymer has a degree of branching of from 60 to 102 branches/1000 carbon atoms.

19. The rubber composition according to claim 1 , wherein the ethylene homopolymer has a degree of branching of from 82 to 102 branches/1000 carbon atoms.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2024
From: HANGZHOU XINGLU TECHNOLOGY CO., LTD.; ZHEJIANG UNIVERSITY
To: HANGZHOU XINGLU TECHNOLOGY CO., LTD.; SHAOXING PINGHE NEW MATERIAL TECHNOLOGY CO., LTD.
Reel/Frame 066734/0595 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2023
From: HANGZHOU XINGLU TECHNOLOGY CO., LTD.
To: HANGZHOU XINGLU TECHNOLOGY CO., LTD.; ZHEJIANG UNIVERSITY
Reel/Frame 063461/0701 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 18, 2022
From: XU, TAO; FU, ZHI SHENG; WU, AN YANG
To: HANGZHOU XINGLU TECHNOLOGIES CO., LTD.
Reel/Frame 059724/0278 →
Priority Claims (2)
CN 201710025140.8 · Jan 13, 2017 · national
CN 201810020850.6 · Jan 10, 2018 · national
Continuity (1)
Related Publication 20190359806A1 · Nov 28, 2019
Cited By (2)
US 12,679,963 US 12,715,987