IP Library Granted Patent US 11,014,873
Granted Patent B2
US 11,014,873 · App. 16/483,341 · Granted May 25, 2021

Anti-fibrotic compounds

Inventors: Thomas Miller (Wakefield, MA); Nikolaos Papaioannou (Newton, MA)
Assignee: CERTA THERAPEUTICS PTY LTD.
C07C235/38C07C255/60C07D213/06C07D215/08C07D231/56C07D233/58C07D241/42C07D249/08C07D257/04C07D265/34C07D271/10C07D305/08C07D307/06
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Quick Facts
Patent No.
US 11,014,873
App. No.
16/483,341
Granted
May 25, 2021
Kind
B2
Abstract

Provided herein are anti-fibrotic compounds, in particular those of Formula (I), that inhibit the TGF-beta signaling pathway. Also provided are pharmaceutical compositions comprising the anti-fibrotic compounds, and methods of treating diseases or conditions associated with fibrosis, inflammation, and benign or malignant neoplastic diseases in a subject by administering a compound or composition described herein. (Formula (I))

Claims (47)

1. A compound of Formula I-i:

or a pharmaceutically acceptable salt thereof; wherein

X is O or NR 10 ;

Y is O or NR 10 ; provided that at least one of X and Y is NR 10 ;

each occurrence of R g and R h is, independently, hydrogen or alkyl, or R g and R h together with the carbon atom to which they are attached form a carbonyl;

t is 1 or 2;

each occurrence of R 10 is, independently, hydrogen or C 1-4 alkyl optionally substituted with oxo.

2. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein each occurrence of R 10 is, independently, hydrogen or C 1-4 alkyl.

3. The compound of claim 2 , wherein R 10 is methyl.

4. The compound of claim 2 , wherein R 10 is hydrogen.

5. The compound of claim 2 , or a pharmaceutically acceptable salt thereof, wherein

X is O;

Y is NR 10 ; and

R 10 is C 1-4 alkyl.

6. The compound of claim 2 , or a pharmaceutically acceptable salt thereof, wherein

X is NR 10 ;

Y is O; and

R 10 is C 1-4 alkyl.

7. The compound of claim 2 , or a pharmaceutically acceptable salt thereof, wherein t is 2.

8. The compound of claim 7 , wherein each occurrence of R g and R h is hydrogen.

9. The compound of claim 7 , wherein one occurrence of R g and R h is hydrogen, and the other occurrence of R g and R h is that R g and R h together with the carbon atom to which they are attached form a carbonyl.

10. The compound of claim 2 , wherein the compound is of Formula I-j:

or a pharmaceutically acceptable salt thereof, wherein:

X is O;

Y is NR 10 ; and

R 10 is C 1-4 alkyl.

11. The compound of claim 2 , wherein the compound is of Formula I-j:

or a pharmaceutically acceptable salt thereof, wherein:

X is NR 10 ;

Y is O; and

R 10 is C 1-4 alkyl.

12. A compound selected from the group consisting of:

2-[[(E)-3-(4-methyl-2,3-dihydro-1,4-benzoxazin-6-yl)prop-2-enoyl]amino]benzoic acid (107);

(E)-2-(3-(4-methyl-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-7-yl)acrylamido)benzoic acid (109);

(E)-2-(3-(4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazin-7-yl)acrylamido)benzoic acid (110);

(E)-2-(3-(3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)acrylamido)benzoic acid (111);

(E)-2-(3-(4-methyl-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)acrylamido)benzoic acid (112);

and pharmaceutically acceptable salts thereof.

13. The compound of claim 12 , wherein the compound is:

2-[[(E)-3-(4-methyl-2,3-dihydro-1,4-benzoxazin-6-yl)prop-2-enoyl]amino]benzoic acid (107);

(E)-2-(3-(4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazin-7-yl)acrylamido)benzoic acid (110); or

(E)-2-(3-(4-methyl-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)acrylamido)benzoic acid (112);

or a pharmaceutically acceptable salt thereof.

14. The compound of claim 13 , wherein the compound is:

(E)-2-(3-(4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazin-7-yl)acrylamido)benzoic acid (110); or a pharmaceutically acceptable salt thereof.

15. A pharmaceutical composition comprising the compound of claim 1 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

16. A pharmaceutical composition comprising the compound of claim 12 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 5, 2022
From: MILLER, THOMAS A.; PAPAIOANNOU, NIKOLAOS
To: SHIRE HUMAN GENETIC THERAPIES, INC.
Reel/Frame 059502/0854 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 20, 2020
From: SHISEIDO AMERICAS CORPORATION
To: SHISEIDO COMPANY, LIMITED
Reel/Frame 052203/0245 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2019
From: MILLER, THOMAS A.; PAPAIOANNOU, NIKOLAOS
To: SHIRE HUMAN GENETIC THERAPIES, INC.
Reel/Frame 050403/0693 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2019
From: SHIRE HUMAN GENETIC THERAPIES, INC.
To: CERTA THERAPEUTICS PTY LTD.
Reel/Frame 050403/0761 →
Continuity (2)
Provisional Application 62454358 · Feb 3, 2017
Related Publication 20200055814A1 · Feb 20, 2020