IP Library Granted Patent US 11,667,884
Granted Patent B2
US 11,667,884 · App. 16/487,769 · Granted Jun 6, 2023

Bead beating tube and method for extracting deoxyribonucleic acid and/or ribonucleic acid from microorganisms

Inventors: Holger Klapproth (Freiburg, DE); Nicolaas Smit (Welland, CA)
Assignee: Safeguard Biosystems Holdings Ltd.
C12N1/066B01L3/5082C12N15/1006G01N1/286C12N2509/10G01N2001/2866
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Quick Facts
Patent No.
US 11,667,884
App. No.
16/487,769
Granted
Jun 6, 2023
Kind
B2
Abstract

The present disclosure provides improved methods for bead beating and a bead beating system useful therefor. The present disclosure further provides methods of using the bead beating system to extract nucleic acids from cells containing the nucleic acids.

Claims (28)

1. A method for producing and recovering a lysate from cells contained in blood containing an anticoagulant, and analyzing one or more nucleic acids from the lysate, comprising:

a) agitating the blood within a bead beating system in the absence of any additive other than the anticoagulant, under conditions sufficient to lyse both a fungal pathogen and a bacterial pathogen and provide a lysate suitable for PCR amplification of DNA from the fungal pathogen, when present, and the bacterial pathogen, when present, said bead beating system comprising (i) a sample tube or blood collection tube and (ii) beads;

b) recovering the lysate from the sample tube or blood collection tube; and

c) analyzing one or more nucleic acids from the lysate, wherein the analyzing comprises PCR to amplify DNA from the fungal pathogen, when present, and DNA from the bacterial pathogen, when present.

2. The method of claim 1 , wherein the beads are adapted to lyse yeast or filamentous fungi.

3. The method of claim 1 , which comprises agitating the blood under conditions sufficient to (i) lyse Candida albicans and (ii) provide a lysate suitable for PCR amplification of DNA from Candida albicans , when the Candida albicans is present.

4. The method of claim 3 , which comprises agitating the blood under conditions sufficient to (i) lyse Staphylococcus aureus and (ii) provide a lysate suitable for PCR amplification of DNA from Staphylococcus aureus , when the Staphylococcus aureus is present.

5. The method of claim 4 , which comprises agitating the blood under conditions sufficient to (i) lyse Escherichia coli and (ii) provide a lysate suitable for PCR amplification of DNA from Escherichia coli , when the Escherichia coli is present.

6. The method of claim 3 , which comprises agitating the blood under conditions sufficient to (i) lyse Escherichia coli and (ii) provide a lysate suitable for PCR amplification of DNA from Escherichia coli , when the Escherichia coli is present.

7. The method of claim 1 , which comprises agitating the blood under conditions sufficient to (i) lyse Staphylococcus aureus and (ii) provide a lysate suitable for PCR amplification of DNA from Staphylococcus aureus , when the Staphylococcus aureus is present.

8. The method of claim 7 , which comprises agitating the blood under conditions sufficient to (i) lyse Escherichia coli and (ii) provide a lysate suitable for PCR amplification of DNA from Escherichia coli , when the Escherichia coli is present.

9. The method of claim 1 , which comprises agitating the blood under conditions sufficient to (i) lyse Escherichia coli and (ii) provide a lysate suitable for PCR amplification of DNA from Escherichia coli , when the Escherichia coli is present.

10. The method of claim 1 , wherein the agitating comprises subjecting the bead beating system to an oscillating motion.

11. The method of claim 1 , wherein the agitating is performed with a vortexer or a homogenizer.

12. The method of claim 1 , wherein the agitating comprises subjecting the bead beating system to 2000 or more oscillations per minute.

13. The method of claim 1 , wherein the agitating is performed for 25-60 seconds.

14. The method of claim 1 , wherein the agitating is performed for 1-2 minutes.

15. The method of claim 1 , wherein the anticoagulant is EDTA, citrate, oxalate or heparin.

16. The method of claim 1 , wherein the cells comprise one or more pathogens.

17. The method of claim 16 , wherein the cells comprise one or more bacterial pathogens, viral pathogens, fungal pathogens, or a combination thereof.

18. The method of claim 17 , wherein the cells comprise one or more fungal pathogens.

19. The method of claim 18 , wherein the one or more fungal pathogens comprise Candida albicans.

20. The method of claim 17 , wherein the cells comprise one or more bacterial pathogens.

21. The method of claim 20 , wherein the one or more bacterial pathogens comprise Staphylococcus aureus.

22. The method of claim 20 , wherein the one or more bacterial pathogens comprise Escherichia coli.

23. The method of claim 1 , wherein the blood comprises cells from multiple species.

24. The method of claim 1 , further comprising purifying one or more nucleic acids from the lysate prior to PCR.

25. The method of claim 1 , further comprising using a microarray to analyze the one or more nucleic acids or sequencing the one or more nucleic acids following PCR.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Oct 31, 2024
From: IP SUCCESSOR FUND 21 L.P.
To: SAFEGUARD BIOSYSTEMS HOLDINGS LIMITED
Reel/Frame 069084/0644 →
RELEASE OF SECURITY INTEREST Recorded Oct 31, 2024
From: MLC50 LP INC.
To: SAFEGUARD BIOSYSTEMS HOLDINGS LIMITED
Reel/Frame 069084/0649 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 31, 2024
From: SAFEGUARD BIOSYSTEMS HOLDING LIMITED
To: SAFEGUARD DX LIMITED
Reel/Frame 069088/0245 →
SECURITY INTEREST Recorded Aug 16, 2024
From: SAFEGUARD BIOSYSTEMS HOLDINGS LIMITED
To: MLC50 LP INC.
Reel/Frame 068317/0453 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2024
From: SAFEGUARD BIOSYSTEMS HOLDINGS LTD.
To: IP SUCCESSOR FUND 21 L.P.
Reel/Frame 066668/0727 →
SECURITY INTEREST Recorded Feb 25, 2021
From: SAFEGUARD BIOSYSTEMS HOLDINGS LIMITED
To: IP SUCCESSOR FUND 21 L.P.
Reel/Frame 055411/0940 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 29, 2020
From: KLAPPROTH, HOLGER; SMIT, NICOLAAS
To: SAFEGUARD BIOSYSTEMS HOLDINGS LTD.
Reel/Frame 051662/0584 →
Priority Claims (1)
EP 2017051902 · Jan 30, 2017 · regional
Continuity (2)
Provisional Application 62538073 · Jul 28, 2017
Related Publication 20210284951A1 · Sep 16, 2021