IP Library Granted Patent US 11,298,341
Granted Patent B2
US 11,298,341 · App. 16/507,713 · Granted Apr 12, 2022

PSMA binding ligand-linker conjugates and methods for using

Inventors: Philip S. Low (West Lafayette, IN); Sumith A. Kularatne (West Lafayette, IN)
Assignee: Purdue Research Foundation
A61K31/426A61K31/475A61K31/4745A61K47/54A61K47/542A61K47/547A61K47/548A61K47/64A61K49/0041A61K49/0043A61K49/0052A61K49/0056A61K51/04A61K51/0402A61K51/0489A61K51/088C07C323/52C07D207/416C07K5/08
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Quick Facts
Patent No.
US 11,298,341
App. No.
16/507,713
Granted
Apr 12, 2022
Kind
B2
Abstract

Described herein are prostate specific membrane antigen (PSMA) binding conjugates that are useful for delivering therapeutic, diagnostic and imaging agents. Also described herein are pharmaceutical composition containing them and methods of using the conjugates and compositions. Also described are processes for manufacture of the conjugates and the compositions containing them.

Claims (20)

1. A compound of the formula:

B-L-IA

or a pharmaceutically acceptable salt thereof, wherein:

B is of the formula

wherein * represents the point of attachment to L;

L is a divalent linker of at least 14 atoms in length, the divalent linker comprising one or more of a divalent cycloalkyl, cycloalkane diradical, cycloalkylene, alkylenecycloalkyl, cycloalkylenecarbonyl, heterocyclyl, aryl, arylalkylene, heteroaryl, a divalent amino alkylene carbonyl group, arylene, or cyclo-imide group and at least one group:

—N(H)—(CR′R″) q —C(O)—

wherein q is 1, R′ is hydrogen, and R″ is the side chain of glutamic acid;

and L does not comprise an arylalkyl side chain; and

IA is an optical imaging agent selected from the group consisting of fluorescein, BODIPY F1, BODIPY 505, tetramethylrhodamine, ALEXA FLUOR™ 488, ALEXA FLUOR™ 647, DYLIGHT™ 680, DYLIGHT™ 800, IR800CW, indocyanine green, OREGON GREEN™ 488, OREGON GREEN™ 514, Texas Red, and phycoerythrin.

2. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises a divalent cycloalkylenecarbonyl group, a divalent amino alkylene carbonyl group, and at least one group —N(H)—(CR′R″) q C(O)—.

3. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L is between about 14 and about 31 atoms in length.

4. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises a cycloalkyl group selected from the group consisting of cyclopropyl, cyclohexyl, 3-ethylcyclopent-1-yl, cyclopropylethyl, and cyclohexylmethyl.

5. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises a cycloalkylene group selected from the group consisting of cycloprop-1,1-diyl, cycloprop-1,2-diyl, cyclohex-1,4-diyl, 3-ethylcyclopent-1,2-diyl, and 1-methylenecyclohex-4-yl.

6. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises a heterocyclyl group selected from the group consisting alkylheterocyclyl, heteroalkylheterocyclyl, heterocyclylalkyl, and heterocyclylheteroalkyl.

7. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises a heterocyclyl group selected from the group consisting of aziridine, pyrrolidine, oxazolidine, 3-methoxypyrrolidine, and 3-methylpiperazine.

8. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises a heterocyclyl group selected from the group consisting of tetrahydrofuran-2-yl, piperidin-1-yl, piperidin-4-yl, piperazin-1-yl, morpholin-1-yl, tetrahydrofuran-2-ylmethyl, piperidin-1-ylethyl, piperidin-4-ylmethyl, piperazin-1-ylpropyl, and morpholin-1-ylethyl.

9. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises an aryl group selected from the group consisting of phenyl and naphthyl.

10. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein L comprises a heteroaryl group selected from the group consisting of pyridinyl, pyrimidinyl, indolyl, and benzoxazolyl.

11. A pharmaceutical composition comprising a compound of claim 1 or a pharmaceutically acceptable salt thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 13, 2020
From: LOW, PHILIP STEWART; KULARATNE, SUMITH A.
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 053485/0451 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 10, 2019
From: LOW, PHILIP STEWART; KULARATNE, SUMITH A.
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 051224/0323 →
Continuity (7)
Continuation 15959110 · Apr 20, 2018
Continuation 15606913 · May 26, 2017
Continuation 14794482 · Jul 8, 2015
Continuation 12673931
Provisional Application 60956489 · Aug 17, 2007
Provisional Application 61074358 · Jun 20, 2008
Related Publication 20200155695A1 · May 21, 2020
Cited By (4)
US 12,208,102 US 12,473,265 US 12,496,292 US 12,655,115