IP Library Granted Patent US 10,894,751
Granted Patent B2
US 10,894,751 · App. 16/514,247 · Granted Jan 19, 2021

Ethylene-to-liquids systems and methods

Inventors: Greg Nyce (Pleasanton, CA); Peter Czerpak (San Francisco, CA); Carlos Faz (Hayward, CA); Jarod McCormick (San Carlos, CA); William Michalak (Redwood City, CA); Bipinkumar Patel (Richmond, TX); Guido Radaelli (South San Francisco, CA); Tim A. Rappold (San Francisco, CA); Ron Runnebaum (Sacramento, CA); Erik C. Scher (San Francisco, CA); Aihua Zhang (Daly City, CA); Joel Cizeron (Redwood City, CA)
Assignee: Lummus Technology LLC
C07C2/84B01J19/24B01J19/245B01J29/40C07C1/0425C07C1/0435C07C1/06C07C1/12C07C2/12C07C2/58C07C4/02C07C5/05C07C5/09C07C5/327C10G9/00C10G11/00C10G50/00C10G57/02C10L3/10F25J3/0209F25J3/0219F25J3/0233F25J3/0238F25J3/0247F25J3/0257B01J2219/00074B01J2219/00103B01J2219/24C07C2523/46C07C2523/755C07C2529/08C07C2529/18C07C2529/40C07C2529/70C07C2529/85C10G2400/20C10G2400/30F25J2200/02F25J2200/74F25J2205/04F25J2210/02F25J2210/04F25J2210/12F25J2230/08F25J2240/02F25J2245/02F25J2260/20F25J2260/60F25J2270/04F25J2270/06F25J2270/12F25J2270/60F25J2270/90F25J2290/80Y02P20/52Y02P20/582Y02P30/40
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Quick Facts
Patent No.
US 10,894,751
App. No.
16/514,247
Granted
Jan 19, 2021
Kind
B2
Abstract

Integrated systems are provided for the production of higher hydrocarbon compositions, for example liquid hydrocarbon compositions, from methane using an oxidative coupling of methane system to convert methane to ethylene, followed by conversion of ethylene to selectable higher hydrocarbon products. Integrated systems and processes are provided that process methane through to these higher hydrocarbon products.

Claims (30)

1. A method of producing a plurality of hydrocarbon products including hydrocarbon compounds with two or more carbon atoms (C 2+ compounds), comprising:

(a) directing methane and an oxidant to an oxidative coupling of methane (OCM) reactor that is upstream of a post-bed cracking (PBC) unit, wherein the OCM reactor is configured to facilitate an OCM reaction using the methane and the oxidant to generate the C 2+ compounds including ethylene and one or more alkanes, and wherein the PBC unit is configured to convert the one or more alkanes, including ethane, to one or more alkenes, including ethylene;

(b) in the OCM reactor, reacting the methane and the oxidant in the OCM reaction to generate an OCM product stream and heat, wherein the OCM product stream comprises ethylene and one or more alkanes;

(c) directing the OCM product stream to the PBC unit;

(d) in the PBC unit, subjecting the OCM product stream to thermal cracking under conditions that crack ethane to ethylene, wherein the thermal cracking is conducted at least in part with the heat from (b), thereby producing a PBC product stream comprising ethylene;

(e) directing the PBC product stream to a separations module, and, in the separations module, separating ethane from the PBC product stream to generate an ethane stream; and

(f) directing the ethane stream to the PBC unit.

2. The method according to claim 1 , wherein the PBC unit is a section of the OCM reactor.

3. The method according to claim 1 , wherein the PBC unit is separate from the OCM reactor.

4. The method according to claim 3 , wherein the PBC unit is in thermal communication with the OCM reactor.

5. The method according to claim 1 , wherein an inlet temperature of the OCM reactor is from about 400° C. to about 600° C. and a pressure of the OCM reactor is from about 15 psig to 150 psig.

6. The method according to claim 5 , wherein the OCM reaction has a C 2+ selectivity of at least 50%.

7. The method according to claim 1 , wherein the separations module comprises a de-methanizer, and in the de-methanizer, separating C 1 compounds contained in the PBC product stream from C 2+ compounds contained in the PBC product stream, directing the C 1 compounds to a methanator to form methane, and directing at least a portion of the methane formed in the methanator to the OCM reactor.

8. The method according to claim 1 , wherein directing the ethane stream to the PBC unit results in a cracking capacity of the PBC unit being at least 70% saturated.

9. The method according to claim 1 , wherein a molar ratio of methane to ethane in the PBC unit is from 1:1 to 15:1.

10. The method according to claim 1 , wherein the OCM reactor comprises a nanowire OCM catalyst material.

11. The method according to claim 1 , further comprising:

directing a stream comprising at least one of C 3 compounds or C 4 compounds to a downstream region of the PBC unit.

12. The method according to claim 1 , wherein the amount of ethane converted to ethylene is at least about 50% of a maximum amount of ethane that can be converted to ethylene in the PBC unit.

13. The method according to claim 1 , further comprising:

(i) directing a natural gas stream having a methane to ethane ratio of 1:1 to 40:1 to a process gas compressor downstream of the PBC unit; and

(ii) directing the PBC product stream to the process gas compressor prior to (e).

14. A system for producing a plurality of hydrocarbon products including hydrocarbon compounds with two or more carbon atoms (C 2+ compounds), comprising:

(a) an oxidative coupling of methane (OCM) reactor comprising an OCM catalyst and fluidly connected at one or more reactor inlets to a source of methane and a source of oxidant, wherein the OCM reactor is configured to generate an OCM product stream and heat from the source of methane and the source of oxidant, wherein the OCM product stream comprises C 2+ compounds including ethylene and one or more alkanes, including ethane;

(b) a post-bed cracking (PBC) unit fluidly connected to the OCM reactor and downstream of the OCM catalyst, wherein the PBC unit is configured to thermally crack the one or more alkanes, including ethane, contained in the OCM product stream to one or more alkenes, including ethylene, using heat generated in the OCM reactor, to thereby produce a PBC product stream comprising ethylene and ethane; and

(c) a separations module downstream of and fluidly connected to the PBC unit, wherein the separations module comprises a de-ethanizer configured to produce an ethane stream from the ethane contained in the PBC product stream and to feed the ethane stream to the PBC unit.

15. The system according to claim 14 , wherein the separations module comprises a de-methanizer configured to separate C 1 compounds contained in the PBC product stream from C 2+ compounds contained in the PBC product stream.

16. The system according to claim 15 , wherein the separations module comprises a methanator fluidly connected to the de-methanizer and to the OCM reactor, wherein the methanator is configured to receive C 1 compounds from the de-methanizer, to produce a methane stream from the C 1 compounds, and to feed at least a portion of the methane stream to the OCM reactor.

17. The system according to claim 14 , wherein the PBC unit is a section of the OCM reactor.

18. The system according to claim 14 , wherein the PBC unit is separate from the OCM reactor.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 2, 2020
From: SILURIA TECHNOLOGIES, INC.
To: SILURIA (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
Reel/Frame 053673/0607 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNOR'S NAME PREVIOUSLY RECORDED ON REEL 050161 FRAME 0416. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Sep 2, 2020
From: SILURIA (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
To: LUMMUS TECHNOLOGY LLC
Reel/Frame 053675/0520 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 26, 2019
From: SILURIA TECHNOLOGIES, INC.
To: LUMMUS TECHNOLOGY LLC
Reel/Frame 050161/0416 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 23, 2019
From: NYCE, GREG; CZERPAK, PETER; FAZ, CARLOS; MCCORMICK, JAROD; MICHALAK, WILLIAM; PATEL, BIPINKUMAR; RADAELLI, GUIDO; RAPPOLD, TIM A.; RUNNEBAUM, RON; SCHER, ERIK C.; ZHANG, AIHUA; CIZERON, JOEL
To: SILURIA TECHNOLOGIES, INC.
Reel/Frame 050144/0023 →
Continuity (9)
Continuation 16197984 · Nov 21, 2018
Continuation 15335183 · Oct 26, 2016
Continuation 15076512 · Mar 21, 2016
Continuation 14789917 · Jul 1, 2015
Continuation 14591850 · Jan 7, 2015
Provisional Application 61925200 · Jan 8, 2014
Provisional Application 62010986 · Jun 11, 2014
Provisional Application 62050729 · Sep 15, 2014
Related Publication 20200207685A1 · Jul 2, 2020
Cited By (1)
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