IP Library › Granted Patent US 11,377,586
Granted Patent B2
US 11,377,586 · App. 16/528,183 · Granted Jul 5, 2022

Use of a borate-acid buffer in oil and gas operations

Inventors: Nabijan Nizamidin (Emeryville, CA); Gayani W. Pinnawala (Katy, TX); Guo-Qing Tang (Mountain View, CA); Varadarajan Dwarakanath (Houston, TX); Gregory A. Winslow (Houston, TX); Jordan Taylor Isbell (Houston, TX); Taimur Malik (Houston, TX)
Assignee: Chevron U.S.A. Inc.
C09K8/584C09K8/588C09K8/602C09K8/665C09K8/68C09K8/80E21B43/20E21B43/26E21B47/11
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Quick Facts
Patent No.
US 11,377,586
App. No.
16/528,183
Granted
Jul 5, 2022
Kind
B2
Abstract

Provided herein are compositions comprising borate-acid buffers, as well as methods of using these compositions in oil and gas operations, including enhanced oil recovery (EOR) operations, fracturing operations, stimulation operations, etc.

Claims (44)

1. A method for improving hydrocarbon recovery from a subterranean formation containing hydrocarbons therewithin, the method comprising:

injecting an aqueous composition comprising (i) a borate-acid buffer, (ii) a surfactant package; (iii) water; and (iv) optionally a water-soluble polymer into the subterranean formation through a wellbore in fluid communication with the subterranean formation;

wherein the borate-acid buffer exhibits a capacity to buffer at a pH of from 6.0 to 8.5;

wherein the borate-acid buffer is present in an effective amount to chelate divalent metal ions present in the water or in water present in the subterranean formation.

2. The method of claim 1 , wherein the wellbore is an injection wellbore; and

wherein injection of the aqueous composition into the subterranean formation through the wellbore increases a flow of hydrocarbons to a production wellbore in fluid communication with the subterranean formation.

3. The method of claim 1 , wherein the method for hydrocarbon recovery comprises an enhanced oil recovery (EOR) operation.

4. The method of claim 1 , further comprising:

adding a tracer to the aqueous composition prior to introducing or along with the aqueous composition or through the wellbore into the subterranean formation;

recovering the tracer from fluids produced from the subterranean formation through the wellbore, fluids recovered from a different wellbore in fluid communication with the subterranean formation, or any combination thereof; and

comparing the quantity of tracer recovered from the fluids produced to the quantity of tracer introduced.

5. The method of claim 1 , wherein the hydrocarbons further comprise CO 2 , H 2 S, or any combination thereof.

6. The method of claim 1 , wherein the borate-acid buffer is present in the aqueous composition in an amount of from 0.05% to 5% by weight, based on the total weight of the aqueous composition.

7. The method of claim 1 , wherein the borate-acid buffer exhibits a capacity to buffer at a pH of from 6.0 to 8.0.

8. The method of claim 1 , wherein the borate-acid buffer comprises a borate compound and a conjugate base of an acid.

9. The method of claim 8 , wherein the borate compound comprises sodium tetraborate, calcium tetraborate, sodium borate, sodium metaborate, or any combination thereof.

10. The method of claim 8 , wherein the conjugate base comprises acetate, citrate, tartrate, succinate, or any combination thereof.

11. The method of claim 8 , wherein the borate compound and the conjugate base of the organic acid are present at a weight ratio of from 1:1 to 5:1.

12. The method of claim 1 , wherein the borate-acid buffer comprises a boric acid and an alkali.

13. The method of claim 1 , wherein the aqueous composition comprises a surfactant package, and wherein the surfactant package comprises a primary surfactant and optionally one or more secondary surfactants.

14. The method of claim 13 , wherein the primary surfactant comprises an anionic surfactant, such as a sulfonate, a disulfonate, a sulfate, a disulfate, a sulfosuccinate, a disulfosuccinate, a carboxylate, a dicarboxylate, or any combination thereof.

15. The method of claim 14 , wherein the anionic surfactant comprises one of the following:

a branched or unbranched C6-C32:PO(0-65):EO(0-100)-carboxylate;

a C10-C30 internal olefin sulfonate;

a C8-C30 alkyl benzene sulfonate (ABS);

a sulfosuccinate surfactant;

a surfactant defined by the formula below

R 1 —R 2 —R 3

wherein

R 1 comprises a branched or unbranched, saturated or unsaturated, cyclic or non-cyclic, hydrophobic carbon chain having 6-32 carbon atoms and an oxygen atom linking R 1 and R 2 ;

R 2 comprises an alkoxylated chain comprising at least one oxide group selected from the group consisting of ethylene oxide, propylene oxide, butylene oxide, and combinations thereof; and

R 3 comprises a branched or unbranched hydrocarbon chain comprising 2-12 carbon atoms and from 2 to 5 carboxylate groups; or

a surfactant defined by the formula below

wherein

R 4 is, individually for each occurrence, a branched or unbranched, saturated or unsaturated, cyclic or non-cyclic, hydrophobic carbon chain having 6-32 carbon atoms; and

M represents a counterion.

16. The method of claim 13 , wherein the primary surfactant comprises a non-ionic surfactant, such as a branched or unbranched C6-C32:PO(0-65):EO(0-100).

17. The method of claim 13 , wherein the primary surfactant has a concentration within the composition of from 0.05% to 5% by weight, based on the total weight of the aqueous composition.

18. The method of claim 1 , wherein the composition further comprises a polymer, a friction reducer, a gelling agent, a crosslinker, a breaker, a pH adjusting agent, a non-emulsifier agent, an iron control agent, a corrosion inhibitor, a scale inhibitor, a biocide, a clay stabilizing agent, a chelating agent, a proppant, a wettability alteration chemical, a co-solvent, or any combination thereof.

19. The method of claim 1 , wherein the borate-acid buffer is present in the aqueous composition in an amount of from 0.1% to 5% by weight, based on the total weight of the aqueous composition.

20. The method of claim 1 , wherein when present the water-soluble polymer comprises a synthetic polymer.

21. The method of claim 1 , wherein when present the water-soluble polymer comprises polyacrylamide or a copolymer thereof.

22. The method of claim 1 , wherein the surfactant package comprises a primary surfactant comprising a branched or unbranched C6-C32:PO(0-65):EO(0-100)-carboxylate, a dicarboxylate, or any combination thereof.

23. The method of claim 1 , wherein the divalent metal ions comprise Mg 2+ , Ca 2+ , or any combination thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 22, 2019
From: NIZAMIDIN, NABIJAN; PINNAWALA, GAYANI W.; TANG, GUO-QING; DWARAKANATH, VARADARAJAN; WINSLOW, GREGORY A.; ISBELL, JORDAN TAYLOR; MALIK, TAIMUR
To: CHEVRON U.S.A. INC.
Reel/Frame 050135/0284 →
Continuity (2)
Provisional Application 62712944 · Jul 31, 2018
Related Publication 20200056087A1 · Feb 20, 2020