IP Library Granted Patent US 11,104,873
Granted Patent B2
US 11,104,873 · App. 16/534,165 · Granted Aug 31, 2021

Systems and methods for stillage fractionation

Inventor: Jason Alan Bootsma (Sioux Falls, SD)
Assignee: POET Research, Inc.
C12F3/10A23K10/38A23K20/163A23K50/10C10L1/026C11B1/00C12M41/26C12M43/00C12M47/10C12M47/14Y02P60/87
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Quick Facts
Patent No.
US 11,104,873
App. No.
16/534,165
Granted
Aug 31, 2021
Kind
B2
Abstract

Systems and methods for fractionating whole stillage from an ethanol production facility are provided. Whole stillage undergoes a separation of its liquid portion (thin stillage) from the solid portion (fiber cake). In some embodiments, the solids and liquids in whole stillage may be separated utilizing a screening centrifuge. The fiber cake may be dried to generate a high fiber animal feed. The thin stillage may be provided to a three-phase separator for separation into an oil emulsion, an aqueous clarified stillage, and a protein paste. The protein paste may be dried to generate a high protein animal feed with greater than about 45% protein content. The clarified thin stillage is condensed to yield a syrup with greater than around 60% solids. The oil emulsion is subjected to a pH adjustment to liberate the oil from the emulsion, which is then separated.

Claims (30)

1. A method for processing whole stillage in an ethanol plant, comprising:

a) separating a thin stillage liquid from the whole stillage via a first centrifuge system;

b) separating a protein paste and a clarified liquid stillage output from the thin stillage liquid via a second centrifuge system, wherein separating the protein paste and the clarified liquid stillage output from the thin stillage liquid comprises separating the thin stillage liquid into the clarified stillage output, an oil emulsion and the protein paste; and

c) sending at least a portion of the clarified liquid stillage output to an evaporation system to concentrate the clarified liquid stillage output into a concentrated, clarified liquid stillage having at least 60% solids; and

d) separating oil from the oil emulsion.

2. The method of claim 1 , wherein separating the thin stillage liquid from the whole stillage produces a fiber cake.

3. The method of claim 2 further comprising: drying the fiber cake to provide a high fiber animal feed product.

4. The method of claim 1 further comprising:

drying the protein paste to provide a high protein animal feed product.

5. The method of claim 1 , wherein the concentrated, clarified liquid stillage is used as an animal feed supplement.

6. The method of claim 1 , further comprising recycling a portion of the clarified liquid stillage output upstream for utilization as fermentation backset.

7. A method for processing whole stillage in an ethanol plant, comprising:

a) separating a thin stillage liquid from the whole stillage via a first centrifuge system;

b) separating a protein paste output and an oil emulsion output from the thin stillage liquid via a second centrifuge system;

c) drying protein paste output via a dryer system to form a protein animal feed product;

d) separating oil from the oil emulsion output via a third centrifuge system to form a residual aqueous layer, wherein the residual aqueous layer comprises protein; and

e) forming an animal feed product with at least a portion of the residual aqueous layer.

8. The method of claim 7 , wherein the protein animal feed product has at least 45% protein.

9. The method of claim 7 , wherein separating a protein paste output from the thin stillage liquid comprises separating the thin stillage liquid into a clarified stillage, an oil emulsion and the protein paste output.

10. The method of claim 9 , further comprising sending at least a portion of the clarified liquid stillage to an evaporation system to concentrate the clarified liquid stillage output into a concentrated, clarified liquid stillage.

11. The method of claim 9 , further comprising recycling a portion of the clarified liquid stillage upstream for utilization as fermentation backset.

12. The method of claim 7 , wherein the at least a portion of the residual aqueous layer and protein paste output are dried in a dryer system to form an animal feed product.

13. The method of claim 7 , wherein separating a thin stillage liquid from the whole stillage via a first centrifuge system comprises separating a thin stillage liquid and fiber cake from the whole stillage, wherein the at least a portion of the residual aqueous layer is combined with the fiber cake.

14. A method for processing whole stillage in an ethanol plant, comprising:

a) separating a thin stillage liquid and fiber cake from the whole stillage via a first centrifuge system;

b) separating a protein paste and an oil emulsion output from the thin stillage liquid via a second centrifuge system;

c) separating oil from the oil emulsion output via a third centrifuge system to form a residual aqueous layer, wherein the residual aqueous layer comprises protein; and

d) forming an animal feed product with at least a portion of the residual aqueous layer and at least a portion of the protein paste.

15. The method of claim 14 , wherein the at least a portion of the residual aqueous layer and the at least a portion of the protein paste are dried in a dryer system to form the animal feed product.

16. The method of claim 14 , wherein the at least a portion of the residual aqueous layer is combined with the fiber cake.

Assignments (3)
SECURITY INTEREST Recorded Apr 3, 2020
From: POET RESEARCH, INC.
To: COBANK, ACB, AS ADMINISTRATIVE AGENT
Reel/Frame 052312/0801 →
SECURITY INTEREST Recorded Apr 2, 2020
From: POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 052295/0712 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 7, 2019
From: BOOTSMA, JASON ALAN
To: POET RESEARCH, INC.
Reel/Frame 049988/0872 →
Continuity (4)
Division 15015355 · Feb 4, 2016
Division 14112897
Provisional Application 61476702 · Apr 18, 2011
Related Publication 20190390146A1 · Dec 26, 2019
Cited By (2)
US 12,480,142 US 12,486,481