IP Library Granted Patent US 11,026,941
Granted Patent B2
US 11,026,941 · App. 16/540,552 · Granted Jun 8, 2021

Concentrated, inhalable ciprofloxacin formulation

Inventors: David C. Cipolla (San Ramon, CA); James Blanchard (El Granada, CA)
Assignee: GRIFOLS, S.A.
A61K31/496A61K9/0043A61K9/0073A61K9/0078A61K9/12A61K9/127A61K45/06A61K47/22A61K9/5084
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Quick Facts
Patent No.
US 11,026,941
App. No.
16/540,552
Granted
Jun 8, 2021
Kind
B2
Abstract

A concentrated inhalable formulation of an antibiotic drug such as ciprofloxacin is disclosed. The antibiotic is formulated with sodium acetate and liposome which incorporate antibiotic. The formulation is aerosolized and inhaled for treatment of respiratory tract infections and other medical conditions.

Claims (24)

1. A method of treating bronchiectasis in a patient, comprising:

administering to lungs of the patient an aerosolized formulation comprising:

free unencapsulated ciprofloxacin;

a pharmaceutically acceptable excipient; and

liposome-encapsulated ciprofloxacin wherein the liposomes are unilamellar, have an average particle size of 1 nanometer to 10 microns, and comprise cholesterol and hydrogenated soy phosphatidyl-choline (HSPC);

wherein the liposomes maintain integrity when aerosolized and provide a ciprofloxacin release rate of 0.5% to 20% per hour over a period of time of 1-12 hours.

2. The method of claim 1 , wherein the liposomes have a diameter in a range from 20 nanometers to 1 micron.

3. The method of claim 2 , wherein the free unencapsulated ciprofloxacin comprises between about 1 and about 75% of the total free unencapsulated and liposome-encapsulated ciprofloxacin.

4. The method of claim 1 , wherein the liposomes provide a ciprofloxacin release rate of 2% to 10% per hour over a period of time of 1-6 hours.

5. The method of claim 1 , wherein the aerosolized formulation further comprises an isotonic histidine buffer.

6. The method of claim 1 , wherein the aerosolized formulation has a pH of 6.0.

7. The method of claim 1 , wherein the aerosolized formulation has an osmolarity of 300 mOsm/kg.

8. The method of claim 1 , wherein the aerosolized formulation further comprises an isotonic histidine buffer at pH 6.0, and an osmolarity of 300 mOsm/kg.

9. A method of treating bronchiectasis in a patient, comprising:

administering to lungs of the patient an aerosolized formulation comprising: free unencapsulated ciprofloxacin;

a pharmaceutically acceptable excipient; and

liposome-encapsulated ciprofloxacin wherein the liposomes comprise cholesterol and hydrogenated soy phosphatidyl-choline (HSPC), are unilamellar, 90% or more of the liposomes maintain integrity when aerosolized, and provide a ciprofloxacin release rate of 0.5% to 20% per hour over a period of time of 1-12 hours.

10. The method of claim 9 , wherein the liposomes provide a ciprofloxacin release rate of 2% to 10% per hour over a period of time of 1-6 hours.

11. The method of claim 9 , wherein the liposomes have a diameter in a range from 20 nanometers to 1 micron.

12. The method of claim 9 , wherein the free unencapsulated ciprofloxacin comprises between about 1 and about 75% of the total free unencapsulated and liposome-encapsulated ciprofloxacin.

13. The method of claim 9 , wherein the aerosolized formulation further comprises an isotonic histidine buffer.

14. The method of claim 9 , wherein the aerosolized formulation has a pH of 6.0.

15. The method of claim 9 , wherein the aerosolized formulation has an osmolarity of 300 mOsm/kg.

16. The method of claim 9 , wherein the aerosolized formulation further comprises an isotonic histidine buffer at pH 6.0, and an osmolarity of 300 mOsm/kg.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 10, 2020
From: ARADIGM CORPORATION
To: GRIFOLS, S.A.
Reel/Frame 052619/0884 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2019
From: CIPOLLA, DAVID C.; BLANCHARD, JAMES
To: ARADIGM CORPORATION
Reel/Frame 051000/0729 →
Continuity (8)
Continuation 15299284 · Oct 20, 2016
Continuation 13036904 · Feb 28, 2011
Continuation 12888275 · Sep 22, 2010
Continuation In Part 12437765 · May 8, 2009
Continuation In Part 12261946 · Oct 30, 2008
Continuation In Part 11876539 · Oct 22, 2007
Provisional Application 60862753 · Oct 24, 2006
Related Publication 20190388416A1 · Dec 26, 2019