IP Library Granted Patent US 11,658,336
Granted Patent B2
US 11,658,336 · App. 16/550,777 · Granted May 23, 2023

Lithium-ion solid state conductor containing a compound of Li

Inventors: Yan Wang (Brookline, MA); Lincoln Miara (Lincoln, MA); Yan-Yan Hu (Tallahassee, FL); Xuyong Feng (Tallahassee, FL)
Assignees: SAMSUNG ELECTRONICS CO., LTD.; THE FLORIDA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
H01M10/0562C01B25/372C01G27/006H01M4/366H01M4/485H01M4/5815H01M4/5825H01M10/0525H01M50/451H01M50/454H01M50/437H01M50/489H01M50/491H01M2300/0068
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Quick Facts
Patent No.
US 11,658,336
App. No.
16/550,777
Granted
May 23, 2023
Kind
B2
Abstract

A compound of Formula 1 Li 1+(4−a)α Hf 2−α M a α (PO 4−δ ) 3   (1) is disclosed, wherein M is at least one cationic element having a valence of a, wherein 0<α≤⅔, 1≤a≤4, and 0≤δ≤0.1. Also described are an electrolyte composition, a separator, a protected positive electrode, a protected negative electrode, and a lithium battery, each including the compound of Formula 1.

Claims (47)

1. A compound of the formula

Li 1α Hf 2−α La α (PO 4−δ ) 3

wherein 0<α≤⅔, and 0≤δ≤0.1.

2. A protected negative electrode, comprising:

a negative active material; and

the compound of claim 1 on a surface of the negative active material.

3. An electrolyte composition, the composition comprising the compound of claim 1 .

4. A separator, comprising:

a microporous film, and

the compound of claim 1 on the microporous film.

5. A protected positive active material comprising:

positive active material a lithium transition metal oxide, a lithium transition metal phosphate, a sulfide, or a combination thereof, and

the compound of claim 1 on a surface of the positive active material.

6. A lithium battery, comprising:

a negative electrode;

an electrolyte; and

a positive electrode,

wherein the electrolyte is between the negative electrode and the positive electrode, and

wherein the negative electrode comprises the protected negative electrode of claim 2 .

7. A lithium battery, comprising:

a negative electrode;

an electrolyte; and

a positive electrode,

wherein the electrolyte is between the negative electrode and the positive electrode, and

wherein the positive electrode comprises the protected positive active material of claim 5 .

8. A lithium battery, comprising:

a negative electrode;

an electrolyte; and

a positive electrode,

wherein the electrolyte is between the negative electrode and the positive electrode, and

wherein the electrolyte comprises the compound of claim 1 .

9. A lithium battery, comprising:

a negative electrode;

a separator comprising a microporous film; and

a positive electrode,

wherein the electrolyte is between the negative electrode and the positive electrode, and

wherein the separator comprises the compound of claim 1 .

10. A method of manufacturing the compound of claim 1 , the method comprising:

contacting a compound comprising lithium, a compound comprising hafnium, and a compound comprising element La to form a mixture; and

heat-treating the mixture to manufacture the compound of the formula

Li 1α Hf 2−α La α (PO 4−δ ) 3

wherein 0<α<⅔, and 0≤δ≤0.1.

11. A method of manufacturing a lithium battery, the method comprising:

providing a negative electrode;

providing a positive electrode; and

disposing a solid electrolyte between the positive electrode and the negative electrode,

wherein at least one of the negative electrode, the positive electrode, and the solid electrolyte comprises the compound of claim 1 .

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 26, 2019
From: WANG, YAN; MIARA, LINCOLN
To: SAMSUNG ELECTRONICS CO., LTD.
Reel/Frame 050167/0438 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 26, 2019
From: HU, YAN-YAN; FENG, XUYONG
To: THE FLORIDA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
Reel/Frame 050167/0468 →
Continuity (3)
Provisional Application 62820670 · Mar 19, 2019
Provisional Application 62773375 · Nov 30, 2018
Related Publication 20200176812A1 · Jun 4, 2020