IP Library Granted Patent US 11,295,869
Granted Patent B2
US 11,295,869 · App. 16/564,552 · Granted Apr 5, 2022

Methods of preserving a nuclear fuel element

Inventor: Aleksey Rezvoi (Idaho Falls, ID)
Assignee: Battelle Energy Alliance, LLC
G21C3/20C23C22/07C08K2003/327C23C22/00C25D11/08G21C13/087G21C19/32G21C21/02G21F5/008
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Quick Facts
Patent No.
US 11,295,869
App. No.
16/564,552
Granted
Apr 5, 2022
Kind
B2
Abstract

A method of preserving a nuclear fuel includes exposing a surface of a fuel element comprising aluminum to a phosphorus-containing acid and reacting the phosphorus-containing acid with the aluminum to form aluminum phosphate (AlPO 4 ). A nuclear fuel element includes a nuclear fuel and a shell surrounding the nuclear fuel. The shell comprises aluminum phosphate.

Claims (20)

1. A method of preserving a nuclear fuel element, the method comprising:

removing corrosion from a surface of a corroded nuclear fuel element; and

after removing the corrosion from the nuclear fuel element, exposing the surface of the nuclear fuel element to a phosphorus-containing acid, the nuclear fuel element comprising a nuclear fuel and a cladding material on the nuclear fuel, one of the nuclear fuel and the cladding material comprising aluminum, exposing the surface of the nuclear fuel element

comprising reacting the phosphorus-containing acid with the aluminum to form aluminum phosphate (AlPO 4 ) on a surface of one or both of the nuclear fuel and the cladding material.

2. The method of claim 1 , wherein exposing the surface of the nuclear fuel element to a phosphorus-containing acid comprises exposing the surface of the nuclear fuel element to phosphoric acid.

3. The method of claim 1 , wherein exposing the surface of the nuclear fuel element to a phosphorus-containing acid comprises exposing the surface of the nuclear fuel element to hypophosphoric acid.

4. The method of claim 1 , wherein exposing the surface of the nuclear fuel element to a phosphorus-containing acid comprises exposing the surface of the nuclear fuel element to phosphorous acid.

5. The method of claim 1 , wherein exposing the surface of the nuclear fuel element to a phosphorus-containing acid comprises exposing the surface of the nuclear fuel element to hypophosphorous acid.

6. The method of claim 1 , wherein exposing the surface of the nuclear fuel element to a phosphorus-containing acid comprises applying an electrical potential to the surface of the nuclear fuel element while exposing the surface of the nuclear fuel element to the phosphorus-containing acid.

7. The method of claim 1 , wherein exposing the surface of the nuclear fuel element comprising aluminum to a phosphorus-containing acid comprises exposing a surface of a cladding material to the phosphorus-containing acid.

8. The method of claim 7 , wherein reacting the phosphorus-containing acid with the aluminum comprises sealing at least one hole through the cladding material.

9. The method of claim 1 , wherein reacting the phosphorus-containing acid with the aluminum comprises forming a barrier impermeable to oxygen.

10. The method of claim 1 , wherein reacting the phosphorus-containing acid with the aluminum comprises forming the aluminum phosphate directly contacting each of the cladding material and the nuclear fuel.

11. The method of claim 1 , wherein reacting the phosphorus-containing acid with the aluminum to form aluminum phosphate comprises forming the aluminum phosphate directly contacting elemental aluminum.

12. The method of claim 1 , wherein exposing the surface of the nuclear fuel element comprising aluminum to a phosphorus-containing acid comprises exposing a surface of a cladding material comprising least one material selected from the group consisting of aluminum, zirconium, and stainless steel to the phosphorus-containing acid.

13. The method of claim 1 , wherein exposing the surface of the nuclear fuel element comprising aluminum to a phosphorus-containing acid comprises exposing a surface of a cladding material comprising aluminum to the phosphorus-containing acid.

14. The method of claim 1 , wherein exposing the surface of the nuclear fuel element comprising aluminum to a phosphorus-containing acid comprises exposing a surface of a cladding material comprising aluminum oxide to the phosphorus-containing acid.

15. The method of claim 1 , wherein reacting the phosphorus-containing acid with the aluminum to form aluminum phosphate (AlPO 4 ) comprises reacting the phosphorus-containing acid with the aluminum through at least one orifice in a cladding material and forming the aluminum phosphate (AlPO 4 ) in contact with the fuel element.

16. The method of claim 1 , wherein exposing the surface of the nuclear fuel element to a phosphorus-containing acid comprises exposing, to the phosphorus-containing acid, a surface of a nuclear fuel comprising U x Al y , wherein x and y are integers.

17. The method of claim 1 , wherein exposing the surface of the nuclear fuel element to a phosphorus-containing acid comprises exposing a surface of a nuclear fuel element comprising spent nuclear fuel to the phosphorus-containing acid.

Assignments (1)
CONFIRMATORY LICENSE Recorded Nov 25, 2019
From: BATTELLE ENERGY ALLIANCE/IDAHO NAT'L LAB
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 051109/0098 →
Continuity (2)
Provisional Application 62730139 · Sep 12, 2018
Related Publication 20200082951A1 · Mar 12, 2020
Cited By (1)
US 12,360,016