IP Library Granted Patent US 11,331,722
Granted Patent B2
US 11,331,722 · App. 16/583,710 · Granted May 17, 2022

Apparatus and method for production and encapsulation of small particles and thin wires

Inventors: Jingzhou Zhao (East Longmeadow, MA); Max Aaron Martel (Fairfield, CT); Yuri Andrew Gulak (Woodbury, CT)
Assignee: WESTERN NEW ENGLAND UNIVERSITY
B22F1/16B22F9/08C03B23/073B22F2302/256
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Quick Facts
Patent No.
US 11,331,722
App. No.
16/583,710
Granted
May 17, 2022
Kind
B2
Abstract

A method of forming one of a plurality of encapsulated crystalline particles includes feeding a coaxial feed wire downwardly such that a first wire end of the coaxial feed wire is positioned at a heating source. The coaxial feed wire includes a crystalline wire core, and an amorphous shell surrounding the crystalline wire core. The first end of the coaxial feed wire is heated at the heating source, thereby forming a molten pendant drop at the first wire end. The plurality of encapsulated crystalline particles are emitted from the molten pendant drop onto a collector located below the molten pendant drop.

Claims (26)

1. A method of forming one of a plurality of particles, comprising:

feeding a microwire such that a first wire end of the microwire is disposed at a heating source;

heating the first end of the microwire at the heating source, thereby forming a molten pendant drop at the first wire end;

positioning a flow of sheath gas around the microwire upstream of the heating source; and

emitting the plurality of particles from the molten pendant drop;

wherein the microwire includes:

a crystalline wire core; and

an amorphous shell surrounding the crystalline wire core.

2. The method of claim 1 , wherein the plurality of particles are one or more encapsulated crystalline core particles.

3. The method of claim 2 , wherein the one or more encapsulated crystalline core particles are less than 1 mm in diameter.

4. The method of claim 1 , wherein the heating source heats the microwire by one or more of resistive heating, induction heating, torch heating, laser heating, microwave heating, electron beam heating, or plasma heating.

5. The method of claim 1 , further comprising positioning an electrode beneath the molten pendant drop.

6. The method of claim 5 , further comprising connecting a second wire end of the microwire opposite the first wire end to a voltage source.

7. The method of claim 6 , wherein the voltage source applies a voltage in a range of −100 kV˜100 kV across the microwire and the electrode.

8. A method of forming one of a plurality of wires, comprising:

feeding a microwire such that a first wire end of the microwire is disposed at a heating source;

heating the first end of the microwire at the heating source, thereby forming a molten pendant drop at the first wire end; and

positioning a flow of sheath gas around the microwire upstream of the heating source; and

emitting the plurality of wires from the molten pendant drop.

9. The method of claim 8 , wherein the microwire has a crystalline wire core; and an amorphous shell surrounding the crystalline wire core.

10. The method of claim 8 , further comprising positioning an electrode beneath the molten pendant drop.

11. The method of claim 10 , further comprising connecting a second wire end of the microwire opposite the first wire end to a voltage source.

12. The method of claim 11 , wherein the voltage source applies a voltage in a range of −100 kV˜100 kV across the microwire and the electrode.

13. The method of claim 8 , wherein the plurality of wires are one or more encapsulated thin crystalline core wires.

14. The method of claim 13 , wherein the encapsulated thin crystalline core wires are less than 100 μm in diameter.

15. The method of claim 8 , wherein the heating source heats the microwire by one or more of resistive heating, induction heating, torch heating, laser heating, microwave heating, electron beam heating, or plasma heating.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 26, 2019
From: ZHAO, JINGZHOU; MARTEL, MAX AARON; GULAK, YURI ANDREW
To: WESTERN NEW ENGLAND UNIVERSITY
Reel/Frame 050503/0502 →
Continuity (2)
Provisional Application 62738071 · Sep 28, 2018
Related Publication 20200114421A1 · Apr 16, 2020