Cell assemblies and methods of using the same
Embodiments disclosed herein relate to cell assemblies for fabricating superhard materials (e.g., used in a high-pressure cubic press) and methods of using the same. The disclosed cell assemblies include a plurality of internal anvils, at least some of which are positioned internally relative to a cell pressure medium of the cell assembly. Such a configuration for the cell assemblies may enable one or more of intensifying cell pressure, reducing processing time, or reducing costs for fabricating such superhard materials.
1. A method of making a superabrasive compact, the method comprising:
disposing a refractory metal canister assembly including a superabrasive compact assembly disposed therein, at least partially within a cell assembly;
wherein the cell assembly includes:
a pressure transmitting medium that at least partially surrounding the refractory metal canister assembly;
a cell pressure medium at least partially surrounding the pressure transmitting medium and the refractory metal canister assembly;
a heating element; and
a plurality of anvils, at least some of the plurality of anvils being positioned at least partially within the cell pressure medium; and
subjecting the cell assembly, including the refractory metal canister assembly, to a high-pressure/high-temperature process at a pressure of about 9 GPa to about 15 GPa.
2. The method of claim 1 , wherein subjecting the cell assembly, including the refractory metal canister assembly, to a high-pressure/high-temperature process at a pressure of about 9 GPa to about 15 GPa includes causing at least some of the cell pressure medium to extrude out of the cell assembly through one or more gaps between adjacent anvils of the plurality of anvils.
3. The method of claim 1 , wherein the superabrasive compact assembly includes a cemented carbide substrate and a plurality of superhard particles.
4. The method of claim 1 , wherein the superabrasive compact assembly includes a cemented tungsten-carbide substrate and a plurality of diamond particles.
5. The method of claim 1 , wherein the superabrasive compact assembly includes a carbide substrate and a plurality of diamond particles having a bimodal size distribution.
6. The method of claim 5 , wherein the bimodal size distribution includes a first plurality of diamond particles having a first average particle size between 2 μm and 12 μm and a second plurality of diamond particles having a second average particles size between 15 μm and 40 μm.
7. The method of claim 1 , wherein:
the refractory metal canister assembly includes an upper surface, a lower surface, and at least one lateral surface extending therebetween; and
the plurality of anvils includes:
a first anvil disposed adjacent to the upper surface;
a second anvil disposed adjacent to the lower surface;
a plurality of lateral anvils disposed circumferentially around at least a portion of the at least one lateral surface of the refractory metal canister assembly; and
wherein each of the plurality of lateral anvils includes an inner surface adjacent to the refractory metal canister assembly, an outer surface generally opposite the inner surface, and at least one lateral surface therebetween, the inner surface having a smaller surface area than the outer surface and exhibiting a geometry that is substantially complementary with at least a portion of the at least one lateral surface of the refractory metal canister assembly.
8. The method of claim 1 , wherein subjecting the cell assembly, including the refractory metal canister assembly, to a high-pressure/high-temperature process at a pressure of about 9 GPa to about 15 GPa includes heating the cell assembly to a temperature of 1200° C. to 2200° C.
9. A method of making a superabrasive compact, the method comprising:
disposing a refractory metal canister assembly including a superabrasive compact assembly disposed therein, at least partially within a cell assembly;
wherein the cell assembly includes:
a pressure transmitting medium that at least partially surrounding the refractory metal canister assembly;
a cell pressure medium at least partially surrounding the pressure transmitting medium and the refractory metal canister assembly;
a heating element; and
a plurality of anvils, at least some of the plurality of anvils being positioned at least partially within the cell pressure medium;
wherein the superabrasive compact assembly includes a carbide substrate and a plurality of diamond particles; and
subjecting the cell assembly, including the refractory metal canister assembly with the superabrasive compact assembly therein, to a high-pressure/high-temperature process.
10. The method of claim 9 , wherein disposing a refractory metal canister assembly at least partially within a cell assembly includes positioning the refractory metal canister assembly in a central cavity of the cell pressure medium.
11. The method of claim 9 , wherein subjecting the cell assembly, including the refractory metal canister assembly, to a high-pressure/high-temperature process includes causing at least some of the cell pressure medium to extrude out of the cell assembly through one or more gaps between adjacent anvils of the plurality of anvils.
12. The method of claim 9 , wherein the carbide substrate includes a cemented tungsten-carbide substrate.
13. The method of claim 9 , wherein the plurality of diamond particles have a bimodal size distribution including a first plurality of diamond particles having a first average particle size between 2 μm and 12 μm and a second plurality of diamond particles having a second average particles size between 15 μm and 40 μm.
14. The method of claim 9 , wherein:
the refractory metal canister assembly includes an upper surface, a lower surface, and at least one lateral surface extending therebetween; and
the plurality of anvils includes:
a first anvil disposed adjacent to the upper surface;
a second anvil disposed adjacent to the lower surface;
a plurality of lateral anvils disposed circumferentially around at least a portion of the at least one lateral surface of the refractory metal canister assembly; and
wherein each of the plurality of lateral anvils includes an inner surface adjacent to the refractory metal canister assembly, an outer surface generally opposite the inner surface, and at least one lateral surface therebetween, the inner surface having a smaller surface area than the outer surface and exhibiting a geometry that is substantially complementary with at least a portion of the at least one lateral surface of the refractory metal canister assembly.
15. The method of claim 9 , wherein subjecting the cell assembly, including the refractory metal canister assembly, to a high-pressure/high-temperature process includes subjecting the cell assembly to a pressure between 9 GPa to 15 GPa and heating the cell assembly to a temperature of 1200° C. to 2200° C.
16. The method of claim 15 , wherein the heating element is positioned adjacent to the refractory metal canister assembly.
17. The method of claim 9 , further comprising positioning the at least some of the plurality of anvils at least partially within the cell pressure medium.
18. A method of making a superabrasive compact, the method comprising:
making a cell assembly, the cell assembly including:
a pressure transmitting medium;
a cell pressure medium at least partially surrounding the pressure transmitting medium;
a heating element; and
a plurality of anvils, at least some of the plurality of anvils being positioned at least partially within the cell pressure medium;
disposing a refractory metal canister assembly including a superabrasive compact assembly disposed therein, at least partially within the cell assembly; and
subjecting the cell assembly, including the refractory metal canister assembly with the superabrasive compact assembly therein, to a high-pressure/high-temperature process at a pressure of about 9 GPa to about 15 GPa.
19. The method of claim 18 , wherein:
the pressure transmitting medium at least partially surrounds the refractory metal canister assembly; and
disposing a refractory metal canister assembly including a superabrasive compact assembly disposed therein, at least partially within the cell assembly includes disposing the refractory metal canister assembly within a body of the cell pressure medium.
20. The method of claim 18 , wherein the superabrasive compact assembly includes a carbide substrate and a plurality of superabrasive particles.