IP Library Granted Patent US 11,034,627
Granted Patent B2
US 11,034,627 · App. 16/597,047 · Granted Jun 15, 2021

Alkane activation with single and bimetallic catalysts

Inventors: Theodore R. Krause (Naperville, IL); Adam S. Hock (Chicago, IL); Guanghui Zhang (Naperville, IL); Yunjie Xu (Chicago, IL)
Assignees: UChicago Argonne, LLC; Illinois Institute of Technology
C07C2/76B01J23/002B01J23/10B01J23/28B01J23/42B01J23/62B01J23/6525B01J23/6527B01J23/6567B01J23/75B01J23/862B01J23/8913B01J35/023B01J37/088B01J37/18B01J21/08B01J23/462B01J23/468B01J2523/00C07C2521/08C07C2523/10C07C2523/28C07C2523/46C07C2523/62C07C2523/656C07C2523/75C07C2523/86C07C2523/89
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Quick Facts
Patent No.
US 11,034,627
App. No.
16/597,047
Granted
Jun 15, 2021
Kind
B2
Abstract

Methods, compositions, and articles of manufacture for alkane activation with single- or bi-metallic catalysts on crystalline mixed oxide supports.

Claims (12)

1. A method for non-oxidative coupling of methane comprising:

synthesizing a bimetallic catalyst on a SiO 2 support by:

grafting cobalt or molybdenum on the SiO 2 support forming a grafted SiO 2 support;

impregnating platinum on the grafted support, forming the bimetallic catalyst;

exposing methane to the bimetallic catalyst; and

converting methane to ethylene with an initial conversion of 8%.

2. The method of claim 1 , wherein the bimetallic catalyst has an initial selectivity in the conversion of methane to ethylene of at least 80%.

3. The method of claim 1 , wherein the conversion of methane is at a temperature of between 550° C. and 650° C.

4. The method of claim 1 , wherein the synthesizing further comprises, prior to impregnating, calcining the grafted SiO 2 support.

5. The method of claim 4 , wherein grafting comprises sequential grafting method.

6. The method of claim 5 , wherein sequential grafting comprises strong electrostatic adsorption.

7. The method of claim 6 , wherein the impregnating comprises incipient wetness impregnation.

Assignments (3)
CONFIRMATORY LICENSE Recorded Jan 17, 2020
From: UCHICAGO ARGONNE, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 051546/0720 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 9, 2019
From: ZHANG, GUANGHUI; KRAUSE, THEODORE R.; XU, YUNJIE
To: UCHICAGO ARGONNE, LLC
Reel/Frame 050667/0347 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 9, 2019
From: HOCK, ADAM S.
To: ILLINOIS INSTITUTE OF TECHNOLOGY
Reel/Frame 050668/0201 →
Continuity (2)
Division 15691666 · Aug 30, 2017
Related Publication 20200102257A1 · Apr 2, 2020