IP Library Granted Patent US 10,994,244
Granted Patent B2
US 10,994,244 · App. 16/607,135 · Granted May 4, 2021

Apparatus and method for waste gas scrubbing

Inventors: Helmut Gehrke (Bergkamen, DE); Martina Schmitz (Essen, DE); Stephan Buss (Dortmund, DE)
Assignees: thyssenkrupp Industrial Solutions AG; thysseukrupp AG
B01D53/75B01D47/06B01D53/58B01D53/78C07C273/16
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Quick Facts
Patent No.
US 10,994,244
App. No.
16/607,135
Granted
May 4, 2021
Kind
B2
Abstract

A device for waste gas scrubbing in a urea plant may be configured such that a waste gas passes along a transportation direction in the duct. The duct may include a first region for removing urea dust particles from the waste gas and a second region for removing chemical compounds from the waste gas, which can be integrated by an acid-base reaction into an aqueous liquid phase. A cross-sectional area of the duct extending perpendicular to the transportation direction in the second region may be greater than a cross-sectional area extending perpendicular to the transportation direction in the first region. Further, the device may be configured such that the duct extends horizontally at least in sections and/or the transportation direction of the waste gas through the duct extends horizontally in an installed state.

Claims (34)

1. A device for waste gas scrubbing in a urea plant, the device comprising:

a duct with an inlet opening and an outlet opening, wherein the device is configured such that a waste gas passes along a transportation direction in the duct, wherein the duct extends horizontally at least in sections and/or the transportation direction of the waste gas through the duct extends horizontally in an installed state of the device, wherein the duct comprises:

a first region comprising a first surface enlargement structure disposed in the duct for removing urea dust particles from the waste gas, and

a second region comprising a second surface enlargement structure disposed in the duct for removing chemical compounds from the waste gas, which are configured to be integrated by an acid-base reaction into an aqueous liquid phase,

wherein a cross-sectional area of the duct extending perpendicular to the transportation direction in the second region is greater than a cross-sectional area of the duct extending perpendicular to the transportation direction in the first region,

wherein the first region comprises a first spraying device for spraying a first solvent, wherein the second region comprises a second spraying device for spraying a second solvent.

2. The device of claim 1 wherein the cross-sectional area in the second region has at least one of a greater height or a greater width than the cross-sectional area of the first region.

3. The device of claim 1 wherein at least one of the first spraying device or the second spraying device comprises a distributor pipe.

4. The device of claim 3 wherein the distributor pipe comprises spray nozzles that are configured to be supplied with one of the solvents via a common feed line.

5. The device of claim 1 wherein at least one of the first spraying device or the second spraying device is disposed so as to spray into a flow of the waste gas from above transversely to the transportation direction of the flow of the waste gas upstream in front of the respective first or second surface enlargement structure.

6. The device of claim 1 wherein at least one of the first spraying device or the second spraying device is disposed upstream in front of the respective first or second surface enlargement structure such that the at least one of the first spraying device or the second spraying device sprays into the respective first or second surface enlargement structure in the transportation direction of a flow of the waste gas.

7. The device of claim 1 wherein at least one of the first surface enlargement structure or the second surface enlargement structure comprises as least one of:

Raschig rings, Pall rings, saddle elements, spring-typical bodies, or combinations thereof;

plates, corrugated plates, formed plates, or combinations thereof; or

metal, glass, plastic, carbon fibers, or combinations thereof.

8. A device for waste gas scrubbing in a urea plant, the device comprising:

a duct with an inlet opening and an outlet opening, wherein the device is configured such that a waste gas passes along a transportation direction in the duct, wherein the duct extends horizontally at least in sections and/or the transportation direction of the waste gas through the duct extends horizontally in an installed state of the device, wherein the duct comprises:

a first region comprising a first surface enlargement structure disposed in the duct for removing urea dust particles from the waste gas, and

a second region comprising a second surface enlargement structure disposed in the duct for removing chemical compounds from the waste gas, which are configured to be integrated by an acid-base reaction into an aqueous liquid phase,

wherein a cross-sectional area of the duct extending perpendicular to the transportation direction in the second region is greater than a cross-sectional area of the duct extending perpendicular to the transportation direction in the first region,

wherein at least one of:

the first region is configured to remove urea dust particles in multiple steps; or

the second region is configured to remove the chemical compounds in multiple steps, wherein one of the chemical compounds is ammonia.

9. A method for waste gas scrubbing in a urea plant, the method comprising:

guiding a waste gas through a duct having a first region for removing urea dust particles and a second region for removing chemical compounds from the waste gas, which are configured to be integrated by an acid-base reaction into an aqueous liquid phase; and

transporting the waste gas through the second region at a lesser speed than in the first region due to an enlargement of a cross-sectional area of the duct that extends perpendicular to a transportation direction in the second region,

wherein the duct extends horizontally at least in sections and/or the transportation direction of the waste gas through the duct extends horizontally.

10. The method of claim 9 comprising removing ammonia, which is one of the chemical compounds, by way of an acid washing solution in the second region.

11. The method of claim 10 wherein the acid washing solution includes an acid.

12. The method of claim 10 wherein the acid washing solution includes at least one of sulfuric acid, nitric acid, hydrochloric acid, or phosphoric acid.

13. The method of claim 9 comprising:

transporting the waste gas at a speed of greater than 1 m/s through the first region; and

transporting the waste gas at a speed of less than 1 m/s through the second region.

14. The method of claim 13 wherein the waste gas entering through an inlet opening of the duct has a temperature of at most 140° C.

Assignments (3)
CHANGE OF NAME Recorded Nov 3, 2025
From: THYSSENKRUPP UHDE GMBH
To: THYSSENKRUPP UHDE FERTILIZER TECHNOLOGY GMBH
Reel/Frame 072767/0076 →
CHANGE OF NAME Recorded Feb 26, 2025
From: THYSSENKRUPP INDUSTRIAL SOLUTIONS AG
To: THYSSENKRUPP UHDE GMBH
Reel/Frame 070340/0075 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 4, 2019
From: GEHRKE, HELMUT; SCHMITZ, MARTINA; BUSS, STEPHAN
To: THYSSENKRUPP INDUSTRIAL SOLUTIONS AG; THYSSENKRUPP AG
Reel/Frame 051177/0423 →
Priority Claims (1)
DE 10 2017 108 843.1 · Apr 25, 2017 · national
Continuity (1)
Related Publication 20200047118A1 · Feb 13, 2020