IP Library Granted Patent US 11,467,094
Granted Patent B2
US 11,467,094 · App. 16/611,745 · Granted Oct 11, 2022

Methods and sensors for detection

Inventors: Sin Yen Leo (Gainesville, FL); Peng Jiang (Gainesville, FL); Tianwei Xie (Gainesville, FL)
Assignee: University of Florida Research Foundation, Inc.
G01N21/78C08G18/6755C08G18/81C08J9/26G01N21/25G01N21/255G01N21/272G01N33/2852C08G2101/00C08G2280/00C08J2201/0442C08J2205/044C08J2375/14G01N2021/7723G01N2021/7773G02B1/005
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Quick Facts
Patent No.
US 11,467,094
App. No.
16/611,745
Granted
Oct 11, 2022
Kind
B2
Abstract

Embodiments of the present disclosure provide for methods of detecting, sensors (e.g., chromogenic sensor), kits, compositions, and the like that related to or use tunable macroporous polymer. In an aspect, tunable macroporous materials as described herein can be used to determine the presence of a certain type(s) and quantity of liquid in a liquid mixture.

Claims (15)

1. A method of measuring the presence of a first liquid in a liquid mixture, comprising:

providing a tunable shape memory polymer membrane wherein the tunable shape memory polymer membrane is an optically transparent glassy polymer having a glass transition temperature higher than room temperature, wherein the glassy polymer is selected from poly(urethane), polyethylene terephthalate (PET), polyethyleneoxide (PEO), epoxy, polyarylates, block copolymers containing polystyrene and poly(1,4-butadiene), poly(2-methyl-2-oxazoline), and polytetrahydrofuran, and polynorbornene, wherein the tunable shape memory polymer membrane is a macroporous photonic crystal membrane having a three-dimensional polymer framework separating macropores; and

exposing an area of the tunable shape memory polymer membrane to the liquid mixture, wherein the area of the tunable shape memory polymer membrane exposed to the liquid mixture changes color if the liquid mixture includes the first liquid;

wherein the color change is correlated to a concentration of the first liquid in the liquid mixture or pressure of vapor of the first liquid in the liquid mixture;

wherein the area changes color depending upon the concentration of the first liquid in the liquid mixture, wherein the color changes from a greenish color to a bluish color in response to a first concentration, yellowish color in response to a second concentration, and orange color in response to a third concentration, and

wherein the first concentration, the second concentration, and the third concentration are different from one another.

2. The method of claim 1 , wherein the color change is detectable.

3. The method of claim 1 , wherein the first liquid is an organic solvent.

4. The method of claim 3 , wherein the organic solvent is ethanol.

5. The method of claim 4 , wherein the liquid mixture is gasoline.

6. A method of measuring the presence of an organic solvent in gasoline, comprising:

providing a tunable shape memory polymer membrane wherein the tunable shape memory polymer membrane is an optically transparent glassy polymer having a glass transition temperature higher than room temperature, wherein the tunable shape memory polymer membrane is a macroporous photonic crystal membrane having a three-dimensional polymer framework separating macropores; and

exposing an area of the tunable shape memory polymer membrane to the gasoline, wherein the area of the tunable shape memory polymer membrane exposed to the gasoline changes color if the liquid mixture includes the organic solvent;

wherein the color change is correlated to a concentration of the organic solvent in the gasoline or pressure of vapor of the organic solvent in the gasoline;

wherein the organic solvent is ethanol, and wherein the area changes color depending upon the concentration of organic solvent in the gasoline, wherein the color changes from a greenish color to a bluish color in response to a first concentration, yellowish color in response to a second concentration, and orange color in response to a third concentration, and wherein the first concentration, the second concentration, and the third concentration are different from one another.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 2, 2021
From: LEO, SIN YEN; JIANG, PENG; XIE, TIANWEI
To: UNIVERSITY OF FLORIDA RESEARCH FOUNDATION, INC.
Reel/Frame 056746/0803 →
CONFIRMATORY LICENSE Recorded Dec 4, 2019
From: UNIVERSITY OF FLORIDA
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 051181/0009 →
Continuity (2)
Provisional Application 62507294 · May 17, 2017
Related Publication 20200110037A1 · Apr 9, 2020