IP Library Granted Patent US 11,052,076
Granted Patent B2
US 11,052,076 · App. 16/619,573 · Granted Jul 6, 2021

Spirocyclic indolines as IL-17 modulators

Inventors: Gareth Neil Brace (Abingdon, GB); Rose Elizabeth Chappell (Abingdon, GB); Hervé Jean Claude Deboves (Abingdon, GB); Anne Marie Foley (Slough, GB); Gregory Foulkes (Abingdon, GB); Elizabeth Pearl Jones (Bracknell, GB); Fabien Claude Lecomte (Slough, GB); Joanna Rachel Quincey (Slough, GB); Monika-Sarah Elisabeth Dorothea Schulze (Slough, GB); Matthew Duncan Selby (Slough, GB); Adam Peter Smalley (Slough, GB); Richard David Taylor (Slough, GB); Robert James Townsend (Abingdon, GB); Zhaoning Zhu (Slough, GB)
Assignee: UCB Biopharma SRL
A61K31/4439A61K31/407A61K31/4155A61K31/4192A61K31/4196A61K31/422A61K31/427A61K31/433A61K31/437A61K31/501A61K31/502A61K31/506C07D471/10C07D487/10C07D491/107C07D491/20C07D495/10C07D519/00
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Quick Facts
Patent No.
US 11,052,076
App. No.
16/619,573
Granted
Jul 6, 2021
Kind
B2
Abstract

A series of substituted spirocyclic 2-oxoindoline derivatives, and analogues thereof, being potent modulators of human IL-17 activity, are accordingly of benefit in the treatment and/or prevention of various human ailments, including inflammatory and autoimmune disorders.

Claims (50)

1. A compound of formula (I), or a pharmaceutically acceptable salt thereof:

wherein

ring A represents C 3-9 cycloalkyl, C 3-7 heterocycloalkyl or C 4-9 heterobicycloalkyl, any of which groups may be optionally substituted by one or more substituents;

B represents C—R 2 or N;

D represents C—R 3 or N;

E represents C—R 4 or N;

R 0 represents hydrogen or C 1-6 alkyl;

R 1 represents —COR a ;

R a represents —CH(R 5 )N(H)C(O)R 6 , —CH(R 5 )N(H)S(O) 2 R 6 , —C(═CR 5a R 5b )N(H)C(O)R 6 , —CH(R 5 )R 7 , —CH(R 5 )N(H)R 7 or —CH(R 5 )C(O)N(H)R 7 ;

R 2 represents hydrogen, halogen, cyano, C 1-6 alkyl, fluoromethyl, difluoromethyl, trifluoromethyl, hydroxy, C 1-6 alkoxy, difluoromethoxy, trifluoromethoxy, C 1-6 alkyl-sulphinyl or C 1-6 alkylsulphonyl;

R 3 represents hydrogen, halogen, cyano, C 1-6 alkyl, fluoromethyl, difluoromethyl, trifluoromethyl, hydroxy, C 1-6 alkoxy, difluoromethoxy, trifluoromethoxy, C 1-6 alkyl-sulphinyl or C 1-6 alkylsulphonyl;

R 4 represents hydrogen, halogen, cyano, C 1-6 alkyl, fluoromethyl, difluoromethyl, trifluoromethyl, hydroxy, C 1-6 alkoxy, difluoromethoxy, trifluoromethoxy, C 1-6 alkyl-sulphinyl or C 1-6 alkylsulphonyl;

R 5 represents hydrogen; or R 5 represents C 1-5 alkyl, C 3-9 cycloalkyl, C 3-9 cyclo-alkyl(C 1-5 )alkyl, C 4-9 bicycloalkyl, C 4-9 bicycloalkyl(C 1-5 )alkyl, C 5-9 spirocycloalkyl, C 5-9 spirocycloalkyl(C 1-5 )alkyl, C 9-11 tricycloalkyl, C 9-11 tricycloalkyl(C 1-5 )alkyl, aryl, aryl-(C 1-5 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-5 )alkyl, heteroaryl or heteroaryl(C 1-5 )alkyl, any of which groups may be optionally substituted by one or more substituents;

R 5a represents C 3-7 cycloalkyl, C 4-9 bicycloalkyl, aryl, C 3-7 heterocycloalkyl or heteroaryl, any of which groups may be optionally substituted by one or more substituents; and

R 5b represents hydrogen or C 1-6 alkyl; or

R 5a and R 5b , when taken together with the carbon atom to which they are both attached, represent C 3-7 cycloalkyl, C 4-9 bicycloalkyl or C 3-7 heterocycloalkyl, any of which groups may be optionally substituted by one or more substituents;

R 6 represents —NR 6a R 6b or —OR 6c ; or R 6 represents C 1-9 alkyl, C 3-9 cycloalkyl, C 3-9 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl-(C 1-6 )alkyl, heteroaryl, heteroaryl(C 1-6 )alkyl or spiro[(C 3-7 )heterocycloalkyl][heteroaryl], any of which groups may be optionally substituted by one or more substituents;

R 6a represents hydrogen; or R 6a represents C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cyclo-alkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )-alkyl, heteroaryl, heteroaryl(C 1-6 )alkyl or spiro[(C 3-7 )heterocycloalkyl][heteroaryl], any of which groups may be optionally substituted by one or more substituents;

R 6b represents hydrogen or C 1-6 alkyl;

R 6c represents C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, heteroaryl or heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents; and

R 7 represents aryl, heteroaryl or spiro[(C 3-7 )heterocycloalkyl][heteroaryl], any of which groups may be optionally substituted by one or more substituents.

2. A compound as claimed in claim 1 represented by formula (I-1), (I-2), (I-3), (I-4) or (I-5), or a pharmaceutically acceptable salt thereof:

wherein A, R 0 , R 1 , R 2 , R 3 and R 4 are as defined in claim 1 .

3. A compound as claimed in claim 1 represented by formula (IIA), or a pharmaceutically acceptable salt thereof:

wherein

W represents O, S, S(O), S(O) 2 , S(O)(NH) or N—R 17 ;

R 17 represents hydrogen or C 1-6 alkyl;

R 0 , R 3 ,

R 5 and R 6 are as defined in claim 1 .

4. A compound as claimed in claim 1 represented by formula (IIB), or a pharmaceutically acceptable salt thereof:

wherein

W represents O, S, S(O), S(O) 2 , S(O)(NH) or N—R 17 ;

R 17 represents hydrogen or C 1-6 alkyl; and

R 0 , R 5 and R 6 are as defined in claim 1 .

5. A compound as claimed in claim 1 wherein R 5 represents C 1-5 alkyl, C 3-9 cycloalkyl, C 3-9 cycloalkyl(C 1-5 )alkyl, C 4-9 bicycloalkyl, C 4-9 bicycloalkyl(C 1-5 )-alkyl, C 5-9 spirocycloalkyl, C 9-11 tricycloalkyl, C 9-11 tricycloalkyl(C 1-5 )alkyl, aryl, aryl-(C 1-5 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-5 )alkyl or heteroaryl(C 1-5 )alkyl, any of which groups may be optionally substituted by one, two or three substituents independently selected from halogen, C 1-6 alkyl, trifluoromethyl, phenyl and C 1-6 alkoxy.

6. A compound as claimed in claim 1 wherein R 6 represents —NR 6a R 6b or —OR 6c ; or R 6 represents C 1-9 alkyl, aryl, C 3-7 heterocycloalkyl, heteroaryl, heteroaryl(C 1-6 )alkyl or spiro[(C 3-7 )heterocycloalkyl][heteroaryl], any of which groups may be optionally substituted by one, two or three substituents independently selected from halogen, C 1-6 alkyl, difluoromethyl, trifluoromethyl, difluoroethyl, trifluoroethyl, trifluoropropyl, cyclopropyl, cyclobutyl, cyclopropylmethyl, hydroxy, hydroxy(C 1-6 )alkyl, oxo, C 1-6 alkoxy(C 1-6 )alkyl, C 1-6 alkylsulfonyl, amino, amino(C 1-6 )alkyl, di(C 1-6 )alkyl-amino(C 1-6 )alkyl and tetrahydropyranyl.

7. A pharmaceutical composition comprising a compound of formula (I) as defined in claim 1 , or a pharmaceutically acceptable salt thereof, in association with a pharmaceutically acceptable carrier.

8. A method for the treatment of psoriasis, psoriatic arthritis, ankylosing spondylitis, chronic obstructive pulmonary disease, atopic dermatitis, arthritis, rheumatoid arthritis, systemic onset juvenile idiopathic arthritis, systemic lupus erythematosus, asthma, scleroderma, systemic sclerosis, lung fibrosis, Crohn's disease, ulcerative colitis and pain, which comprises administering to a patient in need of such treatment an effective amount of a compound of formula (I) as defined in claim 1 , or a pharmaceutically acceptable salt thereof.

9. A compound as claimed in claim 1 represented by formula (IA), or a pharmaceutically acceptable salt thereof:

wherein A, B, D, E, R 0 , R 5 and R 6 are as defined in claim 1 .

10. A compound as claimed in claim 1 represented by formula (IB), or a pharmaceutically acceptable salt thereof:

wherein A, B, D, E, R 0 , R 5 and R 6 are as defined in claim 1 .

11. A compound as claimed in claim 1 represented by formula (IC), or a pharmaceutically acceptable salt thereof:

wherein A, B, D, E, R 0 , R 5 and R 7 are as defined in claim 1 .

12. A compound as claimed in claim 1 represented by formula (ID), or a pharmaceutically acceptable salt thereof:

wherein A, B, D, E, R 0 , R 5 and R 7 are as defined in claim 1 .

13. A compound as claimed in claim 1 represented by formula (IE), or a pharmaceutically acceptable salt thereof:

wherein A, B, D, E, R 0 , R 5 and R 7 are as defined in claim 1 .

14. A compound as claimed in claim 1 represented by formula (IF), or a pharmaceutically acceptable salt thereof:

wherein A, B, D, E, R 0 , R 5a , R 5b and R 6 are as defined in claim 1 .

Assignments (7)
CHANGE OF NAME Recorded May 19, 2020
From: UCB BIOPHARMA SPRL
To: UCB BIOPHARMA SRL
Reel/Frame 052706/0243 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE'S NAME. PREVIOUSLY RECORDED AT REEL: 052678 FRAME: 0467. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 19, 2020
From: BRACE, GARETH NEIL; CHAPPELL, ROSE ELIZABETH; DEBOVES, HERVE JEAN CLAUDE; FOULKES, GREGORY; TOWNSEND, ROBERT JAMES
To: EVOTEC (UK) LTD
Reel/Frame 052706/0397 →
CORRECTIVE ASSIGNMENT TO CORRECT THE SPELLING OF THE ASSIGNOR EVOTEK (UK) LTD TO EVOTEC (UK) LTD PREVIOUSLY RECORDED ON REEL 052678 FRAME 0504. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 19, 2020
From: EVOTEC (UK) LTD
To: UCB BIOPHARMA SPRL
Reel/Frame 052707/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2020
From: BRACE, GARETH NEIL; CHAPPELL, ROSE ELIZABETH; DEBOVES, HERVE JEAN CLAUDE; FOULKES, GREGORY; TOWNSEND, ROBERT JAMES
To: EVOTEK (UK) LTD
Reel/Frame 052678/0467 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2020
From: CELLTECH R&D LIMITED
To: UCB BIOPHARMA SPRL
Reel/Frame 052678/0791 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2020
From: EVOTEK (UK) LTD
To: UCB BIOPHARMA SPRL
Reel/Frame 052678/0504 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2020
From: FOLEY, ANNE MARIE; JONES, ELIZABETH PEARL; LECOMTE, FABIEN CLAUDE; QUINCEY, JOANNA RACHEL; SCHULZE, MONIKA-SARAH ELISABETH DORTHEA; SELBY, MATTHEW; SMALLEY, ADAM PETER; TAYLOR, RICHARD DAVID; ZHU, ZHAONING
To: CELLTECH R&D LIMITED
Reel/Frame 052678/0567 →
Priority Claims (1)
GB 1709456 · Jun 14, 2017 · national
Continuity (1)
Related Publication 20200138797A1 · May 7, 2020