IP Library Granted Patent US 11,629,053
Granted Patent B2
US 11,629,053 · App. 16/623,891 · Granted Apr 18, 2023

Optoelectronically-active two-dimensional indium selenide and related layered materials via surfactant-free deoxygenated co-solvent processing

Inventors: Mark C. Hersam (Wilmette, IL); Joohoon Kang (Evanston, IL)
Assignee: NORTHWESTERN UNIVERSITY
C01B19/007H01L31/032H01L31/035227H01L31/18C01P2002/72C01P2002/77C01P2002/82C01P2002/85C01P2004/04C01P2004/24C01P2006/40
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Quick Facts
Patent No.
US 11,629,053
App. No.
16/623,891
Granted
Apr 18, 2023
Kind
B2
Abstract

Preparation of two-dimensional indium selenide, other two-dimensional materials and related compositions via surfactant-free deoxygenated co-solvent systems.

Claims (17)

1. A composition, comprising:

a layered nanomaterial comprising at least one of mono-, bi- and n-layer nanosheets of said nanomaterial, where n is an integer selected from 3 to 6; and

a deoxygenated medium comprising ethanol and water,

wherein said nanomaterial is selected from Group III monochalcogenides and Group IV monochalcogenides.

2. The composition of claim 1 , being absent of a surfactant.

3. A composition, comprising:

a layered nanomaterial comprising at least one of mono-, bi- and n-layer nanosheets of said nanomaterial, where n is an integer selected from 3 to 6; and

a deoxygenated medium comprising ethanol and water,

wherein said nanomaterial is indium selenide.

4. The composition of claim 3 , wherein said deoxygenated medium is 60:40 (v/v) ethanol:water.

5. The composition of claim 1 , wherein said deoxygenated medium is 60:40 (v/v) ethanol:water.

6. The composition of claim 1 , wherein said deoxygenated medium comprises an Ar-purged co-solvent mixture of ethanol and water.

7. A composition, comprising:

a layered nanomaterial comprising at least one of mono-, bi- and n-layer nanosheets of said nanomaterial, where n is an integer selected from 3 to 6; and

a deoxygenated medium comprising ethanol and water,

wherein said nanomaterial is selected from a transition metal dichalcogenide, hexagonal boron nitride, graphene, and black phosphorus.

8. The composition of claim 6 , wherein said transition metal dichalcogenide is selected from MoS2, MoSe2, MoTe2, WS2 and WSe2.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jun 11, 2025
From: NORTHWESTERN UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 071511/0167 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2020
From: HERSAM, MARK C.; KANG, JOOHOON
To: NORTHWESTERN UNIVERSITY
Reel/Frame 051953/0189 →
Continuity (2)
Provisional Application 62604274 · Jun 29, 2017
Related Publication 20210147235A1 · May 20, 2021