Self-healing insulation fluid for repairing damaged fluid filled cables
The disclosure describes a method of purifying a self-healing fluid (SHF) comprising a drying oil and dielectric fluid. The method comprises (a) filtering the SHF through an absorbent material; and (b) subsequently filtering the SHF through a micropore filter system.
1. A method of purifying a self-healing fluid (SHF) comprising a drying oil and dielectric fluid, the method comprising:
a) filtering the SHF through an absorbent material; and
b) subsequently filtering the SHF through a micropore filter system.
2. The method according to claim 1 , wherein the absorbent material comprises Fuller's Earth.
3. The method according to claim 1 , wherein the method comprises recovering the SHF from the absorbent material.
4. The method according to claim 1 , wherein the micropore filter system comprises a membrane filter with a pore size of less than 50 μm, less than 40 μm, less than 30 μm, less than 20 μm, less than 15 μm, less than 12.5 μm, less than 10 μm, or less than 9 μM.
5. The method according to claim 1 , wherein the method comprises repeating steps (a) and (b) consecutively at least once, optionally wherein the oil is continuously recirculated through a purification system.
6. A method of producing a purified self-healing fluid (SHF), the method comprising:
contacting one or more drying oils and a dielectric fluid to produce a SHF; and
purifying the SHF as defined in claim 1 .
7. The method according to claim 1 , wherein the weight ratio of the drying oil to the dielectric fluid is between 5:95 and 35:65, between 10:90 and 30:70, or between 15:85 and 25:75.
8. The method according to claim 1 , wherein the dielectric fluid is an insulating cable oil.
9. The method according to claim 1 , wherein the drying oil is tung oil.
10. The method according to claim 1 , wherein the drying oil is selected by assessment of composition through spectroscopic analysis, with respect to the level of:
average unsaturation per triglyceride unit; and
mole fraction of residues containing doubly allylic CH 2 groups.
11. The method according to claim 1 , wherein a further drying oil or small molecule is added to the SHF formulation to increase the mole fraction of residues containing doubly allylic CH 2 groups.
12. The method according to claim 1 , wherein subsequent to purifying the SHF, the method comprises adding a catalyst to the purified SHF.