IP Library Granted Patent US 11,225,624
Granted Patent B2
US 11,225,624 · App. 16/643,989 · Granted Jan 18, 2022

Fluorine-containing ether compound, lubricant for magnetic recording medium, and magnetic recording medium

Inventors: Tsuyoshi Kato (Ichihara, JP); Daisuke Yagyu (Ichihara, JP); Naoya Fukumoto (Ichihara, JP); Yuta Yamaguchi (Kawasaki, JP)
Assignee: SHOWA DENKO K.K.
C10M105/54C10M107/38G11B5/7257G11B5/82C10M2213/043C10N2020/04C10N2030/06C10N2040/18C10N2050/02C10N2050/025
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Quick Facts
Patent No.
US 11,225,624
App. No.
16/643,989
Granted
Jan 18, 2022
Kind
B2
Abstract

A fluorine-containing ether compound represented by Formula (1) is provided, R 1 —R 2 —CH 2 —R 3 —CH 2 —R 4   (1) (In Formula (1), R 1 is an alkyl group that may have a substituent, R 2 is a divalent linking group bonded to R 1 via an ethereal oxygen, R 3 is a perfluoropolyether chain, and R 4 is an end group which is different from R 1 -R 2 and includes two or three polar groups, in which each of the polar groups is bonded to a different carbon atom, and the carbon atoms bonded to the polar groups are bonded to each other via a linking group containing a carbon atom not bonded to the polar groups.).

Claims (51)

1. A fluorine-containing ether compound represented by Formula (1)

R 1 —R 2 —CH 2 —R 3 —CH 2 —R 4   (1)

(in Formula (1), R 1 is an alkyl group that may have a substituent, R 2 is represented by —O— or Formula (6)

(in Formula (6), w represents 1 to 4), R 3 is a perfluoropolyether chain, and R 4 is an end group which is different from R 1 -R 2 and includes two or three polar groups, in which each of the polar groups is bonded to a different carbon atom, and the carbon atoms bonded to the polar groups are bonded to each other via a linking group containing a carbon atom not bonded to the polar groups).

2. The fluorine-containing ether compound according to claim 1 ,

wherein the polar groups of R 4 in Formula (1) are hydroxyl groups.

3. A fluorine-containing ether compound represented by Formula (1),

R 1 —R 2 —CH 2 —R 3 —CH 2 —R 4   (1)

(in Formula (1), R 1 is an alkyl group that may have a substituent, R 2 is a divalent linking group bonded to R 1 via an ethereal oxygen, R 3 is a perfluoropolyether chain, and

R 4 is an end group represented by any one of Formulas (2-1) to (2-4)

(in Formula (2-1), p1 represents 1 to 2 and p2 represents 1 to 5),

(in Formula (2-2), s represents 2 to 5),

(in Formula (2-3), t represents 1 to 5),

(in Formula (2-4), q represents 2 to 5).

4. A fluorine-containing ether compound represented by Formula (1),

R 1 —R 2 —CH 2 —R 3 —CH 2 —R 4   (1)

in Formula (1), R 1 is an alkyl group that may have a substituent, R 2 is a divalent linking group bonded to R 1 via an ethereal oxygen, R 3 is represented by Formula (3), (4) or (5),

(in Formula (3), m and n represent average polymerization degrees, m represents 1 to 30, and n represents 0 to 30),

in Formula (4), u represents an average polymerization degree and represents 1 to 30),

in Formula (5), v represents an average polymerization degree and represents 1 to 30), and R 4 is an end group which is different from R 1 -R 2 and includes two or three polar groups, in which each of the polar groups is bonded to a different carbon atom, and the carbon atoms bonded to the polar groups are bonded to each other via a linking group containing a carbon atom not bonded to the polar groups).

5. A fluorine-containing ether compound represented by Formula (1),

R 1 —R 2 —CH 2 —R 3 —CH 2 —R 4   (1)

in Formula (1) R 1 is an alkyl group in which a part or all of hydrogen atoms are substituted with halogen and an alkoxy group or with either halogen or an alkoxy group, R 2 is a divalent linking group bonded to R 1 via an ethereal oxygen, R 3 is a perfluoropolyether chain, and R 4 is an end group which is different from R 1 -R 2 and includes two or three polar groups, in which each of the polar groups is bonded to a different carbon atom, and the carbon atoms bonded to the polar groups are bonded to each other via a linking group containing a carbon atom not bonded to the polar groups).

6. The fluorine-containing ether compound according to claim 1 , wherein R 4 in Formula (1) includes three polar groups.

7. The fluorine-containing ether compound according to claim 1 , wherein a number-average molecular weight thereof is in a range of 500 to 10000.

8. A lubricant for a magnetic recording medium, comprising:

the fluorine-containing ether compound according to claim 1 .

9. A magnetic recording medium, comprising:

a substrate; and

at least a magnetic layer, a protective layer, and a lubricating layer in this order on the substrate,

wherein the lubricating layer includes the fluorine-containing ether compound according to claim 1 .

10. The magnetic recording medium according to claim 9 ,

wherein an average film thickness of the lubricating layer is 0.5 nm to 3 nm.

11. A lubricant for a magnetic recording medium, comprising:

the fluorine-containing ether compound according to claim 3 .

12. A magnetic recording medium, comprising:

a substrate; and

at least a magnetic layer, a protective layer, and a lubricating layer in this order on the substrate,

wherein the lubricating layer includes the fluorine-containing ether compound according to claim 3 .

13. A lubricant for a magnetic recording medium, comprising:

the fluorine-containing ether compound according to claim 4 .

14. A magnetic recording medium, comprising:

a substrate; and

at least a magnetic layer, a protective layer, and a lubricating layer in this order on the substrate,

wherein the lubricating layer includes the fluorine-containing ether compound according to claim 4 .

15. A lubricant for a magnetic recording medium, comprising:

the fluorine-containing ether compound according to claim 5 .

16. A magnetic recording medium, comprising:

a substrate; and

at least a magnetic layer, a protective layer, and a lubricating layer in this order on the substrate,

wherein the lubricating layer includes the fluorine-containing ether compound according to claim 5 .

Assignments (3)
CHANGE OF ADDRESS Recorded Feb 14, 2024
From: RESONAC CORPORATION
To: RESONAC CORPORATION
Reel/Frame 066599/0037 →
CHANGE OF NAME Recorded Jun 23, 2023
From: SHOWA DENKO K.K.
To: RESONAC CORPORATION
Reel/Frame 064082/0513 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 3, 2020
From: KATO, TSUYOSHI; YAGYU, DAISUKE; FUKUMOTO, NAOYA; YAMAGUCHI, YUTA
To: SHOWA DENKO K.K.
Reel/Frame 051995/0953 →