IP Library Granted Patent US 11,408,096
Granted Patent B2
US 11,408,096 · App. 16/644,686 · Granted Aug 9, 2022

Method of producing mechanoluminescent fibers

Inventors: Karen Lozano (McAllen, TX); Yuanbing Mao (McAllen, TX); Carlos Hernandez (Hildalgo, TX); Misael E. Martinez (McAllen, TX); Mark Anthony Ruiz (McAllen, TX); Jorge Ernesto Vidal (McAllen, TX); Jose Zuniga (McAllen, TX)
Assignee: The Board of Regents of the University of Texas System
D01F1/10C09K11/025C09K11/7713C09K11/7715C09K11/7727C09K11/7728C09K11/7741D01D5/18D01F6/12B29K2027/14B29K2027/16B29K2505/00D10B2321/042
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Quick Facts
Patent No.
US 11,408,096
App. No.
16/644,686
Granted
Aug 9, 2022
Kind
B2
Abstract

Described herein is the application of centrifugal spinning to provide a flexible mechanoluminescent material composed of rare earth metal doped fibers. Rare earth metal doped fibers are formed, in one embodiment, by centrifugal spinning.

Claims (13)

1. A method of producing mechanoluminescent fibers, comprising:

placing a solution comprising a polyvinyl-difluoride polymer and a rare earth complex into a body of a fiber producing device, the body comprising one or more openings;

rotating the fiber producing device at a speed sufficient to cause the solution in the body to be passed through one or more openings to produce rare earth metal doped fibers; and

collecting at least a portion of the produced rare earth metal doped fibers, wherein the produced rare earth metal doped fibers are mechanoluminescent fibers.

2. The method of claim 1 , wherein the rare earth metal doped fibers are created without subjecting the rare earth metal doped fibers, during their creation, to an externally applied electric field.

3. The method of claim 1 , wherein rare earth metal is a cerium metal salt.

4. The method of claim 1 , wherein the rare earth metal is a europium metal salt.

5. The method of claim 1 , wherein the rare earth metal is a nitrate salt.

6. The method of claim 1 , wherein the rare earth metal is a sulfate salt.

7. The method of claim 1 , wherein the fibers are collected as a mat of the fibers.

8. The method of claim 1 , wherein the fibers are collected by depositing the fibers onto a support.

9. The method of claim 1 , wherein the rare earth metal doped fibers comprise microfibers.

10. The method of claim 1 , wherein the rare earth metal doped fibers comprise nanofibers.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 14, 2020
From: LOZANO, KAREN; MAO, YUANBING; HERNANDEZ, CARLOS; MARTINEZ, MISAEL E; RUIZ, MARK ANTHONY; VIDAL, JORGE ERNESTO; ZUNIGA, JOSE
To: THE BOARD OF REGENTS OF THE UNIVERSITY OF TEXAS SYSTEM
Reel/Frame 053196/0410 →
CONFIRMATORY LICENSE Recorded Jun 3, 2020
From: UNIVERSITY OF TEXAS, RIO GRANDE
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 052832/0050 →
Continuity (2)
Provisional Application 62555754 · Sep 8, 2017
Related Publication 20200283930A1 · Sep 10, 2020