IP Library Granted Patent US 11,474,169
Granted Patent B2
US 11,474,169 · App. 16/647,884 · Granted Oct 18, 2022

Magnetic material observation method, and magnetic material observation apparatus

Inventors: Toshiya Inami (Hyogo, JP); Tetsu Watanuki (Hyogo, JP); Tetsuro Ueno (Hyogo, JP); Ryo Yasuda (Hyogo, JP)
Assignee: National Institutes for Quantum Science and Technology
G01R33/12G01N23/2252G01R33/032H01J37/222H01J37/266
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Quick Facts
Patent No.
US 11,474,169
App. No.
16/647,884
Granted
Oct 18, 2022
Kind
B2
Abstract

A magnetic material observation method in accordance with the present invention includes: an irradiating step including irradiating a region of a sample with an excitation beam and thereby allowing a magnetic element contained in the sample to radiate a characteristic X-ray; a detecting step including detecting intensities of a right-handed circularly polarized component and a left-handed circularly polarized component contained in the characteristic X-ray; and a calculating step including calculating the difference between the intensity of the right-handed circularly polarized component and the intensity of the left-handed circularly polarized component. Reference to such a difference enables precise measurement of the direction or magnitude of magnetization without strict limitations as to the sample.

Claims (24)

1. A magnetic material observation method for observing a direction of magnetization or a magnitude of magnetization of a sample that contains a magnetic material, the method comprising:

an irradiating step comprising irradiating a region of the sample with an excitation beam, the excitation beam being a beam that allows an element included in the magnetic material to radiate a characteristic X-ray upon irradiation of the sample with the beam;

a detecting step comprising recognizing, as intensities of two circularly polarized components in respective rotation directions, the characteristic X-ray radiated from the element upon irradiation of the sample with the excitation beam; and

a calculating step comprising calculating a difference between the intensities of the two circularly polarized components recognized in the detecting step.

2. The method according to claim 1 , wherein the excitation beam is an electromagnetic wave beam.

3. The method according to claim 2 , wherein the excitation beam is an electromagnetic wave beam which is other than X-rays.

4. The method according to claim 1 , wherein the excitation beam is a charged particle beam.

5. A magnetic material observation apparatus for observing a direction of magnetization or a magnitude of magnetization of a sample that contains a magnetic material, the magnetic material observation apparatus comprising:

an excitation beam source configured to emit an excitation beam, the excitation beam being a beam that allows an element included in the magnetic material to radiate a characteristic X-ray upon irradiation of the sample with the beam;

a detecting section configured to detect the characteristic X-ray, radiated by the element upon irradiation of the sample with the excitation beam, as circularly polarized components different in direction of rotation, the circularly polarized components being a right-handed circularly polarized component and a left-handed circularly polarized component; and

a data processing section configured to carry out output of values each calculated from a difference between an intensity of the right-handed circularly polarized component and an intensity of the left-handed circularly polarized component.

6. The magnetic material observation apparatus according to claim 5 , wherein:

the excitation beam source is configured to irradiate the sample with the excitation beam such that a position, irradiated with the excitation beam, of the sample sweeps; and

the data processing section is configured to (i) recognize the values as the position irradiated with the excitation beam sweeps and (ii) carries out output of an image in which the values correspond to regions, irradiated with the excitation beam, of the sample.

7. The magnetic material observation apparatus according to claim 5 , wherein the detecting section includes a quarter-wave plate for the characteristic X-ray.

8. The magnetic material observation apparatus according to claim 7 , wherein the detecting section includes a polarizer configured to impart, to the characteristic X-ray that has passed through the quarter-wave plate and that contains a linearly polarized component, an intensity that differs according to a polarization direction.

9. The magnetic material observation apparatus according to claim 5 , wherein the excitation beam is an electromagnetic wave beam.

10. The magnetic material observation apparatus according to claim 9 , wherein the excitation beam is an electromagnetic wave beam which is other than X-rays.

11. The magnetic material observation apparatus according to claim 5 , wherein the excitation beam is a charged particle beam.

12. The magnetic material observation apparatus according to claim 11 , wherein the excitation beam is an electron beam,

the magnetic material observation apparatus further comprising an image acquiring section configured to acquire a microscope image which is a scanning electron microscope image or a transmission electron microscope image,

the data processing section being configured to carry out output of an image in which the microscope image and a region irradiated with the excitation beam are displayed such that the microscope image and the region correspond to each other.

13. The magnetic material observation apparatus according to claim 5 , wherein a collimating optical system is provided between the sample and the detecting section, the collimating optical system being configured to collimate the characteristic X-ray.

14. The magnetic material observation apparatus according to claim 13 , wherein the collimating optical system is comprised of a Montel multilayer mirror.

Assignments (2)
CHANGE OF NAME Recorded Aug 19, 2022
From: NATIONAL INSTITUTES FOR QUANTUM AND RADIOLOGICAL SCIENCE AND TECHNOLOGY
To: NATIONAL INSTITUTES FOR QUANTUM SCIENCE AND TECHNOLOGY
Reel/Frame 061254/0716 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 17, 2020
From: INAMI, TOSHIYA; WATANUKI, TETSU; UENO, TETSURO; YASUDA, RYO
To: NATIONAL INSTITUTES FOR QUANTUM AND RADIOLOGICAL SCIENCE AND TECHNOLOGY
Reel/Frame 052133/0983 →
Priority Claims (1)
JP JP2018-054701 · Mar 22, 2018 · national
Continuity (1)
Related Publication 20200249288A1 · Aug 6, 2020