IP Library Granted Patent US 10,941,117
Granted Patent B2
US 10,941,117 · App. 16/653,668 · Granted Mar 9, 2021

5-[(piperazin-l-yl)-3-oxo-propyl]-imidazolidine-2,4-dione derivatives as ADAMTS inhibitors for the treatment of osteoarthritis

Inventors: Franck Laurent Brebion (Romainville, FR); Luke Jonathan Alvey (Romainville, FR); David Amantini (Romainville, FR); Frédéric André De Ceuninck (Paris, FR); Pierre Marc Marie Joseph Deprez (Romainville, FR); Romain Luc Marie Gosmini (Romainville, FR); Hélène Marie Jary (Romainville, FR); Christophe Peixoto (Romainville, FR); Iuliana Ecaterina Pop-Botez (Houilles, FR); Marie Laurence Claire Varin (Romainville, FR)
Assignees: GALAPAGOS NV; LES LABORATORIES SERVIER
C07D233/78A61K31/496A61K31/5377A61K31/55A61P19/02A61P19/04C07D401/04C07D401/12C07D401/14C07D403/06C07D403/14C07D405/12C07D417/12
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Quick Facts
Patent No.
US 10,941,117
App. No.
16/653,668
Granted
Mar 9, 2021
Kind
B2
Abstract

The present invention discloses compounds according to Formula I: Wherein R 1 , R 2 , R 3a , R 3b , and Cy are as defined herein. The present invention relates to compounds inhibiting ADAMTS, methods for their production, pharmaceutical compositions comprising the same, and methods of treatment using the same, for the prophylaxis and/or treatment of inflammatory conditions, and/or diseases involving degradation of cartilage and/or disruption of cartilage homeostasis by administering a compound of the invention.

Claims (34)

1. A pharmaceutical composition comprising a pharmaceutically acceptable carrier and a pharmaceutically effective amount of a compound, wherein the compound is

5-[3-[(3S)-4-(3-chloro-4-fluoro-phenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-cyclopropyl-imidazolidine-2,4-dione,

5-[3-[(3S)-4-(3-chloro-5-fluoro-phenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-cyclopropyl-imidazolidine-2,4-dione,

(5S)-5-cyclopropyl-5-[3-[(3S)-4-(3,4-dichlorophenyl)-3-methyl-piperazin-1-yl]-3-oxo-propyl]imidazolidine-2,4-dione,

(5S)-5-cyclopropyl-5-[(2S)-3-[(3S)-4-(3,4-difluorophenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]imidazolidine-2,4-dione,

5-[3-[(3S)-4-(4-chlorophenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-cyclopropyl-imidazolidine-2,4-dione,

5-[3-[4-(3,4-difluorophenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(methoxymethyl)imidazolidine-2,4-dione,

5-[2-[4-(3,5-dichlorophenyl)piperazine-1-carbonyl]butyl]-5-methyl-imidazolidine-2,4-dione,

(S)-5-((S)-3-((S)-4-(3-chloro-4-fluorophenyl)-3-methylpiperazin-1-yl)-2-methyl-3-oxopropyl)-5-(methoxymethyl)imidazolidine-2,4-dione,

5-[3-[4-(3-chlorophenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-cyclopropyl-imidazolidine-2,4-dione,

5-[3-[4-(3-chloro-2-methyl-phenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-cyclopropyl-imidazolidine-2,4-dione,

tert-butyl N-[2-[4-[3-[4-(3,4-difluorophenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]-2,5-dioxo-imidazolidin-4-yl]ethyl]carbamate,

(5S)-5-cyclopropyl-5-[3-[(3S)-4-(3,5-dichlorophenyl)-3-methyl-piperazin-1-yl]-3-oxo-propyl]imidazolidine-2,4-dione,

5-[3-[(3S)-4-(3-chloro-4-fluoro-phenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(2-pyridyl)imidazolidine-2,4-dione,

5-cyclopropyl-5-[3-[4-(3,5-dichlorophenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]imidazolidine-2,4-dione,

(5R)-5-[(2S)-3-[(3S)-4-(3-chloro-4-fluoro-phenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-methyl-imidazolidine-2,4-dione,

5-cyclopropyl-5-[3-[(3S)-4-[3-fluoro-5-(1H-pyrazol-4-yl)phenyl]-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]imidazolidine-2,4-dione,

5-cyclopropyl-5-[3-[(3S)-4-(3,4-difluorophenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]imidazolidine-2,4-dione,

5-[3-[4-(3,5-dichlorophenyl) piperazin-1-yl]-2-(hydroxymethyl)-3-oxo-propyl]-5-methyl-imidazolidine-2,4-dione,

5-[3-[(3S)-4-(3,4-difluorophenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(2-pyridyl)imidazolidine-2,4-dione,

5-[3-[(3S)-4-(3-chlorophenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(2-pyridyl)imidazolidine-2,4-dione,

5-[3-[(3S)-4-(4-chloro-3,5-difluoro-phenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-methyl-imidazolidine-2,4-dione,

5-cyclopropyl-5-[3-[(3S)-4-(3,4-dichlorophenyl)-3-methyl-piperazin-1-yl]-3-oxo-propyl]imidazolidine-2,4-dione,

5-[3-[4-(3,5-dichlorophenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(2-methylsulfonylethyl)imidazolidine-2,4-dione,

5-[3-[4-(3,5-dichlorophenyl) piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(2-pyridyl) imidazolidine-2,4-dione,

(5S)-cyclopropyl-5-[3-[(3S)-4-(3,5-difluorophenyl)-3-methyl-piperazin-1-yl]-3-oxo-propyl]imidazolidine-2,4-dione,

5-[3-[(3S)-4-(3-fluorophenyl)-3-methyl-piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(2-pyridyl)imidazolidine-2,4-dione,

5-[3-[4-(4-chloro-3,5-difluoro-phenyl) piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(methoxymethyl) imidazolidine-2,4-dione,

5-cyclopropyl-5-[3-[4-(5-fluoro-2-methyl-phenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]imidazolidine-2,4-dione,

5-[3-[4-(3,5-dichlorophenyl)piperazin-1-yl]-2-methyl-3-oxo-propyl]-5-(methoxymethyl)imidazolidine-2,4-dione, or

5-[3-[(3S)-4-(3,4-dichlorophenyl)-3-methyl-piperazin-1-yl]-3-oxo-propyl]-5-(2-pyridyl)imidazolidine-2,4-dione.

2. The pharmaceutical composition according to claim 1 , further comprising a second therapeutic agent.

3. A method of treating and/or preventing an inflammatory condition, and/or disease involving degradation of cartilage and/or disruption of cartilage homeostasis comprising administering to a subject in need thereof, the pharmaceutical composition according to claim 1 .

4. The method according to claim 3 , further comprising administering to the subject in need thereof, a second therapeutic agent effective in preventing and/or treating an inflammatory condition, and/or disease involving degradation of cartilage and/or disruption of cartilage homeostasis.

Assignments (6)
CHANGE OF NAME Recorded Jun 4, 2026
From: GALAPAGOS
To: LAKEFRONT BIOTHERAPEUTICS
Reel/Frame 074845/0068 →
RELEASE OF SECURITY INTEREST Recorded Feb 15, 2022
From: GILEAD SCIENCES, INC.
To: GALAPAGOS NV
Reel/Frame 059020/0871 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 10, 2021
From: LES LABORATOIRES SERVIER
To: GALAPAGOS NV
Reel/Frame 057442/0384 →
SECURITY INTEREST Recorded Nov 23, 2020
From: GALAPAGOS NV
To: GILEAD SCIENCES, INC.
Reel/Frame 054503/0967 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 15, 2019
From: BREBION, FRANCK LAURENT; AMANTINI, DAVID; ALVEY, LUKE JONATHAN; DEPREZ, PIERRE MARC MARIE JOSEPH; GOSMINI, ROMAIN LUC MARIE; JARY, HÉLÈNE MARIE; PEIXOTO, CHRISTOPHE; VARIN, MARIE LAURENCE CLAIRE
To: GALAPAGOS NV
Reel/Frame 050723/0107 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 15, 2019
From: DE CEUNINCK, FRÉDÉRIC ANDRÉ; POP-BOTEZ, IULIANA ECATERINA
To: LES LABORATOIRES SERVIER
Reel/Frame 050723/0139 →
Priority Claims (1)
EP 14307129 · Dec 22, 2014 · regional
Continuity (3)
Continuation 15896779 · Feb 14, 2018
Continuation 15538393
Related Publication 20200216397A1 · Jul 9, 2020